• Journal of Inorganic Materials
  • Vol. 37, Issue 4, 452 (2022)
Hongda WANG1、2, Qian FENG3, Xiao YOU1、2、4, Haijun ZHOU1、2、*, Jianbao HU1、2, Yanmei KAN1、2, Xiaowu CHEN1、2, and Shaoming DONG1、2
Author Affiliations
  • 11. State Key Laboratory of High Performance Ceramics and Superfine Microstructure, Shanghai Institute of Ceramics, Chinese Academy of Sciences, Shanghai 200050, China
  • 22. Structural Ceramics and Composites Engineering Research Center, Shanghai Institute of Ceramics, Chinese Academy of Sciences, Shanghai 200050, China
  • 33. Analysis and Testing center, Donghua University, Shanghai 201600, China
  • 44. University of Chinese Academy of Sciences, Beijing 100039, China
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    DOI: 10.15541/jim20210381 Cite this Article
    Hongda WANG, Qian FENG, Xiao YOU, Haijun ZHOU, Jianbao HU, Yanmei KAN, Xiaowu CHEN, Shaoming DONG. Microstructure and Corrosion Behavior of Brazed Joints of SiC/SiC Composites and Hastelloy N Alloy Using Cu-Ni Alloy[J]. Journal of Inorganic Materials, 2022, 37(4): 452 Copy Citation Text show less
    Schematic illustration of the sandwich-like structure of joint
    1. Schematic illustration of the sandwich-like structure of joint
    SEM images of brazing joints obtained at (a) 1090, (b) 1110 ℃, (c) and (d) 1130 ℃, correspoding EDS analyses (atom fraction) (e) of the point in image (d)
    2. SEM images of brazing joints obtained at (a) 1090, (b) 1110 ℃, (c) and (d) 1130 ℃, correspoding EDS analyses (atom fraction) (e) of the point in image (d)
    Elemental distribution analyses by EDS of joint obtained at 1130 ℃
    3. Elemental distribution analyses by EDS of joint obtained at 1130 ℃
    Gibbs free energy of formation of candidates calculated using HSC Chemistry 5.11 computer software and its associated databases
    4. Gibbs free energy of formation of candidates calculated using HSC Chemistry 5.11 computer software and its associated databases
    SEM image of microstructure and EDS line-scan analyses in SiC/SiC composites near joint obtained at 1150 ℃
    5. SEM image of microstructure and EDS line-scan analyses in SiC/SiC composites near joint obtained at 1150 ℃
    XRD patterns of joints before and after corrosion
    6. XRD patterns of joints before and after corrosion
    Appearance images and SEM images of microstructure of joints before and after corrosion at 800 ℃ for 100 h
    7. Appearance images and SEM images of microstructure of joints before and after corrosion at 800 ℃ for 100 h
    Elemental distribution analyses by EDS of joint obtained at 1130 ℃ after corrosion at 800 ℃ for 100 h
    8. Elemental distribution analyses by EDS of joint obtained at 1130 ℃ after corrosion at 800 ℃ for 100 h
    ElementBefore corrosionAfter corrosion
    Ni1020
    Cr20210
    Fe3040
    Mo<10<10
    Table 1.

    Content of main metal impurities in fluoride salts before and after corrosion (10-4% in mass)

    Hongda WANG, Qian FENG, Xiao YOU, Haijun ZHOU, Jianbao HU, Yanmei KAN, Xiaowu CHEN, Shaoming DONG. Microstructure and Corrosion Behavior of Brazed Joints of SiC/SiC Composites and Hastelloy N Alloy Using Cu-Ni Alloy[J]. Journal of Inorganic Materials, 2022, 37(4): 452
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