• Acta Optica Sinica
  • Vol. 43, Issue 13, 1305001 (2023)
Zijiang Yang1、2、3, Qiao Pan1、2、3、*, Jiacheng Zhu1、2、3, and Weimin Shen1、2、3
Author Affiliations
  • 1Key Lab of Advanced Optical Manufacturing Technologies of Jiangsu Province, Suzhou 215006, Jiangsu, China
  • 2Key Lab of Modern Optical Technologies of Education Ministry of China, Suzhou 215006, Jiangsu, China
  • 3School of Optoelectronic Science and Engineering, Soochow University, Suzhou 215006, Jiangsu, China
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    DOI: 10.3788/AOS230446 Cite this Article Set citation alerts
    Zijiang Yang, Qiao Pan, Jiacheng Zhu, Weimin Shen. Fabrication of Silicon Echelle Grating by Ultraviolet Lithography Combined with Wet Etching[J]. Acta Optica Sinica, 2023, 43(13): 1305001 Copy Citation Text show less
    Anisotropic etching of (100) monocrystalline silicon
    Fig. 1. Anisotropic etching of (100) monocrystalline silicon
    Schematics of echelle grating. (a) Traditional echelle grating; (b) silicon echelle grating
    Fig. 2. Schematics of echelle grating. (a) Traditional echelle grating; (b) silicon echelle grating
    Diffraction efficiency varying with platform duty ratio f at different working orders. (a) 47; (b) 41; (c) 36
    Fig. 3. Diffraction efficiency varying with platform duty ratio f at different working orders. (a) 47; (b) 41; (c) 36
    Tolerance analysis of grating platform duty ratio
    Fig. 4. Tolerance analysis of grating platform duty ratio
    Fabrication process of echelle gratings. (a) Substrate pre-processing; (b) oxide layer growing; (c) photoresist spinning; (d) ultraviolet exposure and development; (e) oxygen plasma etching; (f) ICP etching; (g) wet etching; (h) high-reflecting film coating
    Fig. 5. Fabrication process of echelle gratings. (a) Substrate pre-processing; (b) oxide layer growing; (c) photoresist spinning; (d) ultraviolet exposure and development; (e) oxygen plasma etching; (f) ICP etching; (g) wet etching; (h) high-reflecting film coating
    Grating after mask collapse under optical microscope
    Fig. 6. Grating after mask collapse under optical microscope
    Schematic of over-etching after reaching the self-stopping surface
    Fig. 7. Schematic of over-etching after reaching the self-stopping surface
    SEM photos of silicon echelle grating with or without crystal alignment. (a) Without crystal alignment; (b) with crystal alignment
    Fig. 8. SEM photos of silicon echelle grating with or without crystal alignment. (a) Without crystal alignment; (b) with crystal alignment
    SEM photos of 42 lp/mm silicon echelle grating. (a) Magnification of 300×; (b) magnification of 1000×
    Fig. 9. SEM photos of 42 lp/mm silicon echelle grating. (a) Magnification of 300×; (b) magnification of 1000×
    Grating photos after coating. (a) Top view; (b) dispersion diagram
    Fig. 10. Grating photos after coating. (a) Top view; (b) dispersion diagram
    Schematic of diffraction efficiency testing device of echelle grating
    Fig. 11. Schematic of diffraction efficiency testing device of echelle grating
    Measurement results of diffraction efficiency at corresponding blazed wavelength of working orders
    Fig. 12. Measurement results of diffraction efficiency at corresponding blazed wavelength of working orders
    Test results of grating sidewall surface roughness
    Fig. 13. Test results of grating sidewall surface roughness
    ParameterValue
    Wavelength /nm800-1100
    Groove density /(lp·mm-142
    Incident angle /(°)54.74
    Incident conditionQuasi Littrow mounting
    Diffraction order35-48
    Orientation angle /(°)6.4
    Table 1. Working parameters of grating
    Diffraction orderFree spectral range /nm
    48796-813
    47813-830
    46830-849
    45849-868
    44868-888
    43888-909
    42909-930
    41930-953
    40953-978
    39978-1003
    381003-1030
    371030-1058
    361058-1088
    351088-1119
    Table 2. Free spectral ranges corresponding to working diffraction orders of grating
    ParameterValue
    Groove spacing /mm23.81
    Blazed angle /(°)54.74
    Groove apex angle /(°)70.52
    High-reflecting filmAg
    High-reflecting film thickness /nm150
    Table 3. Parameters of grating groove
    ParameterRequirementMeasured value
    Maximum diffraction efficiency of each working order /%>4045-55
    Groove space /μm23.81±0.2023.80
    Blazed angle /(°)54.74±0.2054.74
    Roughness of sidewall /nm0.57
    Table 4. Measurement results of grating
    Zijiang Yang, Qiao Pan, Jiacheng Zhu, Weimin Shen. Fabrication of Silicon Echelle Grating by Ultraviolet Lithography Combined with Wet Etching[J]. Acta Optica Sinica, 2023, 43(13): 1305001
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