• Optoelectronic Technology
  • Vol. 44, Issue 1, 6 (2024)
Wenzhu WU, Zengzhou YANG, Zugang LIU, Jiawei JING..., Ranran HAN, Jinchen HAN, Zhijie XIA, Hong ZHAO and Xin YAO|Show fewer author(s)
Author Affiliations
  • College of Optical and Electronic Technology,China Jiliang University, Hangzhou 310018, CHN
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    DOI: 10.12450/j.gdzjs.202401002 Cite this Article
    Wenzhu WU, Zengzhou YANG, Zugang LIU, Jiawei JING, Ranran HAN, Jinchen HAN, Zhijie XIA, Hong ZHAO, Xin YAO. Method Synthesis of CuIn0.7Ga0.3S2 Nanoparticles by Injection Method and Application in CIGSSe Solar Cells[J]. Optoelectronic Technology, 2024, 44(1): 6 Copy Citation Text show less
    Schematic representation of the synthesis device
    Fig. 1. Schematic representation of the synthesis device
    Diagram of device structure
    Fig. 2. Diagram of device structure
    TEM images of nanoparticles synthesized by different oleamine volumes
    Fig. 3. TEM images of nanoparticles synthesized by different oleamine volumes
    Uv-vis absorption spectra of nanoparticles synthesized with different volumes of dibenzyl ether
    Fig. 4. Uv-vis absorption spectra of nanoparticles synthesized with different volumes of dibenzyl ether
    The XRD diffraction pattern of CuIn0.7Ga0.3S2 nanoparticles
    Fig. 5. The XRD diffraction pattern of CuIn0.7Ga0.3S2 nanoparticles
    The HRTEM and SAED images of CuIn0.7Ga0.3S2 nanoparticles
    Fig. 6. The HRTEM and SAED images of CuIn0.7Ga0.3S2 nanoparticles
    Dispersion of nanoparticles in toluene, p-xylene and cyclohexane
    Fig. 7. Dispersion of nanoparticles in toluene, p-xylene and cyclohexane
    Cross-sectional SEM images of device prepared by toluene, p-xylene and cyclohexane nanoparticle inks
    Fig. 8. Cross-sectional SEM images of device prepared by toluene, p-xylene and cyclohexane nanoparticle inks
    Device J‑V curves prepared by toluene, p-xylene, cyclohexane nanoparticle inks
    Fig. 9. Device J‑V curves prepared by toluene, p-xylene, cyclohexane nanoparticle inks
    墨水分散剂旋涂转速/rmp旋涂时间/s退火时间/s
    甲苯2 0004090
    对二甲苯2 20045100
    环己烷1 8003580
    Table 1. Preparation parameters of CuIn0.7Ga0.3S2 prefabricated layer for different dispersant inks
    二苄醚/mlCu/(Wt%)In/(Wt%)Ga/(Wt%)S/(Wt%)
    018.0223.325.6519.50
    418.0822.345.9519.46
    817.9622.126.0719.45
    Table 2. ICP results for nanoparticles prepared with different volumes of dibenzyl ether
    1‑辛硫醇/mlCu Wt%In Wt%Ga Wt%S Wt%
    1218.1223.025.9417.66
    1518.3423.106.0718.81
    1818.7323.476.1219.79
    Table 3. ICP results for nanoparticles prepared with different volumes of 1-octanethiol
    墨水 分散剂开路电压/mV短路电流密度/(mA·cm-2)填充因子/(%)转换效率/(%)
    甲苯501.7633.6957.739.76
    对二甲苯466.732.249.77.46
    环己烷407.816.739.852.71
    Table 4. Device J‑V parameters prepared by toluene, p‑xylene and cyclohexane nanoparticle inks
    Wenzhu WU, Zengzhou YANG, Zugang LIU, Jiawei JING, Ranran HAN, Jinchen HAN, Zhijie XIA, Hong ZHAO, Xin YAO. Method Synthesis of CuIn0.7Ga0.3S2 Nanoparticles by Injection Method and Application in CIGSSe Solar Cells[J]. Optoelectronic Technology, 2024, 44(1): 6
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