Author Affiliations
1Institute of Laser Advanced Manufacturing, Zhejiang University of Technology, Hangzhou, Zhejiang 310023, China2College of Mechanical Engineering, Zhejiang University of Technology, Hangzhou, Zhejiang 310023, China3Jiangsu Yawei Machine Tool Co., Ltd., Yangzhou, Jiangsu 225200, Chinashow less
Fig. 1. Morphological diagrams of Ti6Al4V powder. (a) Micro-morphology; (b) particle size distribution
Fig. 2. Schematic of SLD system
Fig. 3. Cross-sectional micro-morphologies of SLD-Ti6Al4V coatings. (a)(b) B1; (c)(d) B2; (e)(f) B3; (g)(h) B4; (i)(j) B5
Fig. 4. Area fraction of interfacial reaction layer in SLD-Ti6Al4V coatings
Fig. 5. EDS mapping results at particle interface of SLD-Ti6Al4V coating (sample B3). (a) Original SEM image; (b) Ti element; (c) Al element; (d) V element; (e) N element
Fig. 6. EDS analysis result of Ti6Al4V powder
Fig. 7. XRD patterns of Ti6Al4V coatings and Ti6Al4V powder
Fig. 8. Compactness comparison of coatings. (a)(c) CS-Ti6Al4V; (b)(d) SLD-Ti6Al4V
Fig. 9. Porosity comparison of SLD-Ti6Al4V coatings
Fig. 10. Schematic of particle interfacial in-situ reaction in SLD-Ti6Al4V coatings
Fig. 11. Micro-hardness of SLD-Ti6Al4V coatings. (a) B1; (b) B2; (c) B3; (d) B4; (e) B5; (f) average value of micro-hardness
Fig. 12. Micro-morphologies of worn surfaces of Ti6Al4V substrate and coatings. (a)(b) Ti6Al4V substrate; (c)(d) CS-Ti6Al4V coating; (e)(f) SLD-Ti6Al4V coating
SampleNo. | N2pressure /MPa | N2temperature /℃ | Standoffdistance /mm | Powderfeeding rate /(r·min-1) | Traversespeed /(mm·s-1) | Laserpower /W | Laser spotdiameter /mm | Overlappingrate /% |
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B1 | 5 | 1000 | 30 | 1.5 | 15 | 0 | 4 | 50 | B2 | 5 | 1000 | 30 | 1.5 | 15 | 500 | 4 | 50 | B3 | 5 | 1000 | 30 | 1.5 | 15 | 600 | 4 | 50 | B4 | 5 | 1000 | 30 | 1.5 | 15 | 700 | 4 | 50 | B5 | 5 | 1000 | 30 | 1.5 | 15 | 800 | 4 | 50 |
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Table 1. Process parameters for preparing SLD-Ti6Al4V coatings
Sample No. | Content | Ti | N | Al | V |
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B1 | Mass fraction /% | 85.2 | 8.92 | 4.77 | 1.12 | | Atomic fraction /% | 68.06 | 24.34 | 6.76 | 0.84 | B2 | Mass fraction /% | 81.16 | 12.67 | 4.76 | 1.17 | | Atomic fraction /% | 60.47 | 32.27 | 6.29 | 0.82 | B3 | Mass fraction /% | 83.03 | 11.92 | 3.87 | 0.86 | | Atomic fraction /% | 63.02 | 30.94 | 5.22 | 0.61 | B4 | Mass fraction /% | 81.20 | 13.35 | 4.44 | 0.88 | | Atomic fraction /% | 59.85 | 33.65 | 5.81 | 0.61 | B5 | Mass fraction /% | 73.53 | 22.73 | 2.79 | 0.57 | | Atomic fraction /% | 46.82 | 49.47 | 3.15 | 0.34 |
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Table 2. EDS analysis results of particle interfacial reaction layer in SLD-Ti6Al4V coatings