Author Affiliations
1College of Engineering, Nanjing Agricultural University, Nanjing , Jiangsu 210031, China2College of Transportation Engineering, Nanjing Vocational University of Industry Technology, Nanjing , Jiangsu 210023, China3Key Laboratory of Intelligence Agricultural Equipment of Jiangsu Province (Nanjing Agricultural University), Nanjing , Jiangsu 210031, Chinashow less
Fig. 1. Characterization of the coating surface microstructures. (a) Spherical-cap shaped bump; (b) W-shaped pit; (c) crater pit; (d) pit with double concentric holes
Fig. 2. Surface morphology and cross-section of the coating. (a) 2D morphology image; (b) cross-section
Fig. 3. XRD spectrum of coating
Fig. 4. Top views, 3D images, and contour lines of cross-sections of four typical microstructures
Fig. 5. Characteristic parametric diagrams of the coating surface microstructures at varying pulse energy densities. (a) Diameter; (b) altitude
Fig. 6. Cross-section contour lines of the coating surface microstructures in phase 1
Fig. 7. Cross-section contour lines of the coating surface microstructures in phase 2
Fig. 8. Cross-section contour lines of the coating surface microstructures in phase 3
Fig. 9. Cross-section contour lines of the coating surface microstructures in phase 4
Fig. 10. Characteristic parametric diagrams of coating surface microstructures with varying pulse widths. (a) Diameter; (b) altitude
Fig. 11. Cross-section contour lines of the coating surface microstructures with varying pulse widths. (a) 10-35 μs; (b) 35-50 μs
Fig. 12. Characteristic parametric diagrams of the coating surface microstructures at different numbers of pulses. (a) Diameter; (b) altitude
Fig. 13. Cross-section contour lines of the coating surface microstructures at varying numbers of pulses
Bath component | Molecular formula | Mass concentration / (g·L-1) | Specification |
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Nickel sulphate | NiSO4·6H2O | 200.000 | A.R. | Nickel chloride | NiCl2·6H2O | 50.000 | A.R. | Cobalt sulfate | CoSO4·7H2O | 10.000 | A.R. | Boric acid | H3BO3 | 30.000 | A.R. | Sodium dodecyl sulfate | C12H25SO4Na | 0.050 | A.R. | Thiourea | CH4N2S | 0.002 | A.R. | Silicon nitride | Si3N4 | 6.000 | 20 nm |
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Table 1. Plating solution composition
Number of pulses | Laser pulse width /µs | Laser energy density / (J·cm-2) |
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1 | 10 | 198.73-287.75 | 1 | 10-50 | 248.47 | 1-9 | 10 | 211.23 |
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Table 2. Laser processing parameters used for experiments
Element | Ni | Co | Si | N | C | O | S |
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Mass fraction /% | Balance | 14.23 | 0.31 | 0.35 | 3.63 | 0.72 | 0.41 |
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Table 3. EDS analysis results of coating