• Journal of Inorganic Materials
  • Vol. 36, Issue 12, 1237 (2021)
Qian LIU*, Jiacheng WANG, Zhenzhen ZHOU, and Xiaoke XU
DOI: 10.15541/jim20210247 Cite this Article
Qian LIU, Jiacheng WANG, Zhenzhen ZHOU, Xiaoke XU. Research Progress on High Throughput Parallel Synthesis of Micro-nano Powders Libraries[J]. Journal of Inorganic Materials, 2021, 36(12): 1237 Copy Citation Text show less
Front view of the experimental setup for visible-light irradiation of the photocatalysts libraries[9]
. Front view of the experimental setup for visible-light irradiation of the photocatalysts libraries[9]
(a) Schematic diagram of drop-on-demand inkjet delivery system (mainly with micro-piezoelectric inkjet head, solution reservoir, x-y moving stage, microreactor and substrate)[12]; (b) schematic diagram of Sol-Gel device (1-box with temperature controlling insides; 4-shaking motor; 5-support rod; 7-reaction chamber; 8-microreactor array)[16]
. (a) Schematic diagram of drop-on-demand inkjet delivery system (mainly with micro-piezoelectric inkjet head, solution reservoir, x-y moving stage, microreactor and substrate)[12]; (b) schematic diagram of Sol-Gel device (1-box with temperature controlling insides; 4-shaking motor; 5-support rod; 7-reaction chamber; 8-microreactor array)[16]
(a) Schematic diagram of a typical triple-laser-beam parallel heating system(mainly including laser sources, reflectors, sample library holder and moving platform, computer and controllers)[21]; (b) Schematic diagram of a representative triple channel optical spectrometer(mainly including fiber optical spectrometer, spectral calibration device, modular LE and LED excitation source, sample library holder and moving platform)[22]
. (a) Schematic diagram of a typical triple-laser-beam parallel heating system(mainly including laser sources, reflectors, sample library holder and moving platform, computer and controllers)[21]; (b) Schematic diagram of a representative triple channel optical spectrometer(mainly including fiber optical spectrometer, spectral calibration device, modular LE and LED excitation source, sample library holder and moving platform)[22]
View of the multi-autoclave showing the mode of stacking of the Teflon blocks and one of the alternative designs using Teflon inserts which can be stacked vertically[23]
. View of the multi-autoclave showing the mode of stacking of the Teflon blocks and one of the alternative designs using Teflon inserts which can be stacked vertically[23]
(a) Schematic layout of the high-throughput hydrothermal (HiTCH) flow synthesis system, and (b) shematic of freeze-dried powders fired at 1000 ℃ and filled into a PTFE triangular holder[29]
. (a) Schematic layout of the high-throughput hydrothermal (HiTCH) flow synthesis system, and (b) shematic of freeze-dried powders fired at 1000 ℃ and filled into a PTFE triangular holder[29]
Schematic diagram (a) and photograph (b) of the ceramic substrate-copper net-metal mask microreactor array, (c) a plastic substrate with the same predrilled shallow wells (2 mm in depth) as the library, then flipped over the synthesized powders into the shallow wells, and (d) a metal plate used to compact powders[39]
. Schematic diagram (a) and photograph (b) of the ceramic substrate-copper net-metal mask microreactor array, (c) a plastic substrate with the same predrilled shallow wells (2 mm in depth) as the library, then flipped over the synthesized powders into the shallow wells, and (d) a metal plate used to compact powders[39]
Schematic diagram of microfluidic chip for synthesis of three-elements compounds[42]
. Schematic diagram of microfluidic chip for synthesis of three-elements compounds[42]
Setup of the microchip-based photocatalyst screening system (a), schematic diagram of the multi-channel array ship with a wedge structure in each channel (b), schematic diagram of the catalyst loading (c), and illustration of the catalyst screening procedure (d)[43]
. Setup of the microchip-based photocatalyst screening system (a), schematic diagram of the multi-channel array ship with a wedge structure in each channel (b), schematic diagram of the catalyst loading (c), and illustration of the catalyst screening procedure (d)[43]
Photos of the microfluidic-based composition and temperature controlling platform with two inlets and 20 outlets (a), details of the micro-reactor arrays (120-230 ℃, 100 holes) and microfluidic chip having Christmas-tree-type structure (b)[48]
. Photos of the microfluidic-based composition and temperature controlling platform with two inlets and 20 outlets (a), details of the micro-reactor arrays (120-230 ℃, 100 holes) and microfluidic chip having Christmas-tree-type structure (b)[48]
Ternary combi-chem libraries for (a) (Ca,Sr,Mg)2Si5N8: Eu2+, (b) (Ca,Sr,Mg)2Si5N8:Eu2+, (c) (Ca,Sr,Ba)2Si5N8:Eu2+, and (d) (Sr,Ba,Mg)2Si5N8:Eu2+ in terms of photoluminescent intensity and color chromaticity[49]
. Ternary combi-chem libraries for (a) (Ca,Sr,Mg)2Si5N8: Eu2+, (b) (Ca,Sr,Mg)2Si5N8:Eu2+, (c) (Ca,Sr,Ba)2Si5N8:Eu2+, and (d) (Sr,Ba,Mg)2Si5N8:Eu2+ in terms of photoluminescent intensity and color chromaticity[49]
Internal structure(a), schematic diagram (b) and operation flow chart (c) of the high throughput equipment[53]
. Internal structure(a), schematic diagram (b) and operation flow chart (c) of the high throughput equipment[53]
Schematic diagram of high-throughput electric field-assisted combustion synthesis system[55]
. Schematic diagram of high-throughput electric field-assisted combustion synthesis system[55]
Qian LIU, Jiacheng WANG, Zhenzhen ZHOU, Xiaoke XU. Research Progress on High Throughput Parallel Synthesis of Micro-nano Powders Libraries[J]. Journal of Inorganic Materials, 2021, 36(12): 1237
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