• Laser & Optoelectronics Progress
  • Vol. 61, Issue 21, 2114005 (2024)
Zhao Zhang, Maomao Cui, Xiao Wang*, Wenkai Shen..., Tao Wang and Huixia Liu|Show fewer author(s)
Author Affiliations
  • School of Mechanical Engineering, Jiangsu University, Jiangsu 212013, Zhenjiang , China
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    DOI: 10.3788/LOP240599 Cite this Article Set citation alerts
    Zhao Zhang, Maomao Cui, Xiao Wang, Wenkai Shen, Tao Wang, Huixia Liu. Parameter Modeling and Optimization of Laser Stereolithography Process for Alumina Ceramics[J]. Laser & Optoelectronics Progress, 2024, 61(21): 2114005 Copy Citation Text show less
    Morphology of alumina powder, rheological properties curve of ceramic slurry and particle size distribution of Al2O3 powder with different particle sizes. (a) SEM image of Al2O3 particle; (b) rheological properties curve of ceramic slurry; (c) particle size distribution of 5 μm Al2O3 powder; (d) particle size distribution of 2 μm Al2O3 powder
    Fig. 1. Morphology of alumina powder, rheological properties curve of ceramic slurry and particle size distribution of Al2O3 powder with different particle sizes. (a) SEM image of Al2O3 particle; (b) rheological properties curve of ceramic slurry; (c) particle size distribution of 5 μm Al2O3 powder; (d) particle size distribution of 2 μm Al2O3 powder
    SLA ceramic forming equipment and laser scanning stereolithography process. (a) Schematic diagram of SLA ceramic forming equipment; (b) schematic diagram of laser scanning stereolithography ceramic slurry curing principle; (c) schematic diagram of stereolithography ceramic green body forming principle
    Fig. 2. SLA ceramic forming equipment and laser scanning stereolithography process. (a) Schematic diagram of SLA ceramic forming equipment; (b) schematic diagram of laser scanning stereolithography ceramic slurry curing principle; (c) schematic diagram of stereolithography ceramic green body forming principle
    Cross-sectional morphology of bending specimens of stereolithography alumina ceramics in green, degreased and sintered bodies. (a) Cross-sectional morphology of green bodies; (b) cross-sectional morphology of sintered bodies; (c) cross-sectional morphology of degreased body; (d) localized enlargement diagram of cross-section morphology of degreased body
    Fig. 3. Cross-sectional morphology of bending specimens of stereolithography alumina ceramics in green, degreased and sintered bodies. (a) Cross-sectional morphology of green bodies; (b) cross-sectional morphology of sintered bodies; (c) cross-sectional morphology of degreased body; (d) localized enlargement diagram of cross-section morphology of degreased body
    Residual analysis results. (a) Comparation of actual value with predicted value of flexural strength; (b) normal distribution of standardized residuals; (c) comparation of standardized residual with predicted value
    Fig. 4. Residual analysis results. (a) Comparation of actual value with predicted value of flexural strength; (b) normal distribution of standardized residuals; (c) comparation of standardized residual with predicted value
    Influence curve of each process parameter on flexural strength of bending specimens
    Fig. 5. Influence curve of each process parameter on flexural strength of bending specimens
    Response surface plot of the interaction between process parameters. (a) Interaction of scanning speed and scanning spacing (AB); (b) interaction of scanning speed and slice thickness (AC); (c) interaction of scanning speed and laser power (AD); (d) interaction of scanning spacing and slice thickness (BC); (e) interaction of scanning spacing and laser power (BD); (f) interaction of slice thickness and laser power (CD)
    Fig. 6. Response surface plot of the interaction between process parameters. (a) Interaction of scanning speed and scanning spacing (AB); (b) interaction of scanning speed and slice thickness (AC); (c) interaction of scanning speed and laser power (AD); (d) interaction of scanning spacing and slice thickness (BC); (e) interaction of scanning spacing and laser power (BD); (f) interaction of slice thickness and laser power (CD)
    Contour plot of the interaction between process parameters. (a) Interaction of scanning speed and scanning spacing (AB); (b) interaction of scanning speed and slice thickness (AC); (c) interaction of scanning speed and laser power (AD); (d) interaction of scanning spacing and slice thickness (BC); (e) interaction of scanning spacing and laser power (BD); (f) interaction of slice thickness and laser power (CD)
    Fig. 7. Contour plot of the interaction between process parameters. (a) Interaction of scanning speed and scanning spacing (AB); (b) interaction of scanning speed and slice thickness (AC); (c) interaction of scanning speed and laser power (AD); (d) interaction of scanning spacing and slice thickness (BC); (e) interaction of scanning spacing and laser power (BD); (f) interaction of slice thickness and laser power (CD)
    Schematic diagram of overcuring of cured layer inside specimen by subsequent irradiation and changes in layer spacing between adjacent layers. (a) Overcuring induced by high exposure energy; (b) overcuring induced by low exposure energy; (c) variation of layer spacing between adjacent layers within specimen
    Fig. 8. Schematic diagram of overcuring of cured layer inside specimen by subsequent irradiation and changes in layer spacing between adjacent layers. (a) Overcuring induced by high exposure energy; (b) overcuring induced by low exposure energy; (c) variation of layer spacing between adjacent layers within specimen
    Cross-section of bending specimen at different stages of ceramic stereolithography process. (a) Delamination in bending specimens made at a scanning speed of 3000 mm/s; (b) delamination in bending specimens made at a hatching spacing of 0.14 mm; (c) bending specimens made at a scanning speed of 3000 mm/s produce laminar gaps at debinding stage; (d) bending specimens made at a hatching spacing of 0.14 mm produce laminar gaps at debinding stage; (e) (f) crack defects within sintered body of a bending specimens
    Fig. 9. Cross-section of bending specimen at different stages of ceramic stereolithography process. (a) Delamination in bending specimens made at a scanning speed of 3000 mm/s; (b) delamination in bending specimens made at a hatching spacing of 0.14 mm; (c) bending specimens made at a scanning speed of 3000 mm/s produce laminar gaps at debinding stage; (d) bending specimens made at a hatching spacing of 0.14 mm produce laminar gaps at debinding stage; (e) (f) crack defects within sintered body of a bending specimens
    FactorVariable symbolLevel
    -101
    Scanning speed A /(mm/s)v200025003000
    Scanning spacing B /mmhs0.100.120.14
    Slice thickness C /mmTs0.100.120.14
    Laser power D /mWW150200250
    Table 1. Experimental factors and levels
    Experimental groupScanning speed /(mm/s)Scanning spacing /mmSlice thickness /mmLaser power /mWFlexural strength /MPa
    1-1-100246
    21-100202
    3-1100275
    41100227
    500-1-1236
    6001-1260
    700-11225
    80011268
    9-100-1238
    10100-1206
    11-1001259
    121001211
    130-1-10237
    1401-10252
    150-110254
    160110277
    17-10-10256
    1810-10215
    19-1010257
    201010250
    210-10-1248
    22010-1257
    230-101235
    240101270
    250000295
    260000298
    270000290
    280000285
    290000288
    Table 2. Box-Behnken experimental design scheme and results
    SourceSum of squaresDegree of freedomMean square errorFPSignificant
    Proposed18863.16141347.3721.27<0.0001Significant
    A4033.3314033.3363.66<0.0001Significant
    B1541.3311541.3324.330.0002Significant
    C1752.0811752.0827.650.0001Significant
    D44.08144.080.69580.4182
    AB4140.06310.8053
    AC28912894.560.0509
    AD641641.010.3319
    BC161160.25250.6231
    BD16911692.670.1247
    CD90.25190.251.420.2525
    A²7746.6717746.67122.26<0.0001Significant
    B²1943.2111943.2130.67<0.0001Significant
    C²1751.711751.727.650.0001Significant
    Residual887.051463.36
    Lack of fit776.251077.632.80.1663Not significant
    Pure error110.8427.7
    Table 3. Analysis of variance
    ParameterCriteriaWeight
    GoalLow limitUpper limit
    Scanning speed /(mm/s)In range200030001
    Hatching spacing /mmIn range0.10.141
    Slice thickness /mmIn range0.10.141
    Laser power /mWIn range1502501
    Flexural strength /MPaMaximize2022981
    Table 4. Optimization criteria and weights
    No.ABCDFlexural strength /MPa
    Predictive valueActual value
    123820.1280.127206299.077295
    223820.1280.127206299.077302
    323820.1280.127206299.077298
    Table 5. Validation of optimization results
    Zhao Zhang, Maomao Cui, Xiao Wang, Wenkai Shen, Tao Wang, Huixia Liu. Parameter Modeling and Optimization of Laser Stereolithography Process for Alumina Ceramics[J]. Laser & Optoelectronics Progress, 2024, 61(21): 2114005
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