Jian LIU, Lingkun WANG, Baoliang XU, Qian ZHAO, Yaoxuan WANG, Yi DING, Shengtai ZHANG, Tao DUAN. Nd-doped ZrSiO4 Ceramics: Synthesis in Molten Salt at Low Temperature, Phase Evolution and Chemical Stability [J]. Journal of Inorganic Materials, 2023, 38(8): 910
- Journal of Inorganic Materials
- Vol. 38, Issue 8, 910 (2023)
1. Synthetic schematic of Nd-doped ZrSiO4 by MSS
2. XRD patterns of ZrSiO4 synthesized by MSS at different temperatures (1100, 1200, 1300, 1400, and 1500 ℃)
3. XRD patterns of ZrSiO4 synthesized by MSS at 1200 ℃ for different time (3, 6, 9, 12, and 15 h)
4. XRD patterns of ZrSiO4 synthesized by MSS with different molar ratios of molten salt to oxide (1200 ℃/6 h)
5. Mechanism of ZrSiO4 ceramics synthesis by MSS
6. XRD patterns of Zr1-x Ndx SiO4-x /2 (0≤x ≤0.1) synthesized by MSS at 1200 ℃ for 6 h
7. Variation of lattice volume of Zr1-x Ndx SiO4-x /2 (0≤x ≤0.1) in contrast to Nd content
8. Micromorphologies and correponding particle size distributions of Zr1-x Ndx SiO4-x /2
9. Normalized leaching rate of Zr1-x Ndx SiO4-x /2 (0.02≤x ≤0.10)
10. Logarithmic relationship of ${{B}_{\text{Nd}}}$ on the time of contact with leaching solution
11. XRD patterns of Zr1-x Ndx SiO4-x /2 (0.02≤x ≤0.10) after leaching for 42 d
12. SEM images of Zr1-x Ndx SiO4-x /2 (x =0.02, 0.08) after leaching for 42 d
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