• Journal of Inorganic Materials
  • Vol. 35, Issue 2, 231 (2020)
Xing-Bang LI1,2, He ZHONG1, Jing-Xian ZHANG1,3,*, Yu-Sen DUAN1,2, and Dong-Liang JIANG1
Author Affiliations
  • 1State Key Laboratory of High Performance Ceramics and Superfine Microstructure, Shanghai Institute of Ceramics, Chinese Academy of Sciences, Shanghai 200050, China
  • 2University of Chinese Academy of Sciences, Beijing 100049, China
  • 3Suzhou Institute of SICCAS (Shanghai Institute of Ceramics, Chinese Academy of Sciences), Taicang 215499, China
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    DOI: 10.15541/jim20190091 Cite this Article
    Xing-Bang LI, He ZHONG, Jing-Xian ZHANG, Yu-Sen DUAN, Dong-Liang JIANG. Powder Characteristics on the Rheological Performance of Resin-based Zirconia Suspension for Stereolithography[J]. Journal of Inorganic Materials, 2020, 35(2): 231 Copy Citation Text show less
    Viscosity as a function of shear rate for 35vol% dispersions with different powders
    . Viscosity as a function of shear rate for 35vol% dispersions with different powders
    Rheological curves of slurries using powders with (a) similar particle size distribution and (b) similar specific surface area
    . Rheological curves of slurries using powders with (a) similar particle size distribution and (b) similar specific surface area
    SEM images of (a) No. 7 powder, (b) No. 5 powder and (c) No. 9 powder
    . SEM images of (a) No. 7 powder, (b) No. 5 powder and (c) No. 9 powder
    Rheological behavior of slurries with different solid loadings
    . Rheological behavior of slurries with different solid loadings
    Relative viscosity of slurries as a function of solid loading at the shear rate of 30 s-1
    . Relative viscosity of slurries as a function of solid loading at the shear rate of 30 s-1
    Optical pictures of green (a) and sintered (b) zirconia parts fabricated by stereolithography
    . Optical pictures of green (a) and sintered (b) zirconia parts fabricated by stereolithography
    SEM image of the fracture surface of the sintered part
    . SEM image of the fracture surface of the sintered part
    No.Product nameSupplier
    1SZ-DT-SE2Jiangxi Size Materials Co., Ltd.
    2YH-3YSZYixingshi Yihui Naimo Cailiao Co., Ltd.
    3SG-3YB-S2Z0-EDongguan CSG Ceramics Technology Co., Ltd.
    4OZ-3Y-6Guangdong Orient Zirconic Ind Sci & Tech Co., Ltd.
    5TYSZ-3-SHubei Jing Gui Zirconium Co., Ltd.
    6HWYA-N-3SGuangDong Huawang Zirconium Materials Co., Ltd.
    7G3Y-020OOShandong Sinocera Functional Material Co., Ltd.
    8SZ-DM-3.0-F3Jiangxi Size Materials Co., Ltd.
    9TZ-3YSETosoh Corp., Tokyo, Japan
    Table 1.

    Basic information of the raw powders used in this work

    Powderd10/nmd50/nmd90/nm
    Before roll milling196.7316.9510.3
    After roll milling207.0318.0488.4
    Table 2.

    Particle size and distribution of No. 9 powder before and after ball milling

    No.d10/nmd50/nmd90/nmSBET/(m2·g-1)Slurry viscosity/(Pa·s)
    1172.7283.3464.615.59667.2
    2323.2577.61032.38.64343.8
    3146.0252.4436.515.71222.6
    4180.3309.1529.917.52118
    5229.0390.3665.38.19414.5
    6140.1206.6304.59.23614
    7236.5386.4631.49.1811.7
    8169.2300.0531.710.18811
    9196.7316.9510.37.1339
    Table 3.

    Particle size distribution and BET specific surface area of raw powders

    Xing-Bang LI, He ZHONG, Jing-Xian ZHANG, Yu-Sen DUAN, Dong-Liang JIANG. Powder Characteristics on the Rheological Performance of Resin-based Zirconia Suspension for Stereolithography[J]. Journal of Inorganic Materials, 2020, 35(2): 231
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