• Journal of Inorganic Materials
  • Vol. 35, Issue 6, 729 (2020)
Jianxiang DING1, Peiyan HUANG1, Yuhui ZHA1, Dandan WANG2, Peigen ZHANG2, Wubian TIAN2、*, and Zhengming SUN2、*
Author Affiliations
  • 1Key Laboratory of Green Fabrieation and Surface Technology of Adranced Metal Materials, Ministry of Education, School of Materials Science and Engineering, Anhui University of Technology, Ma’anshan 243002, China
  • 2School of Materials Science and Engineering, Southeast University, Nanjing 211189, China
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    DOI: 10.15541/jim20190243 Cite this Article
    Jianxiang DING, Peiyan HUANG, Yuhui ZHA, Dandan WANG, Peigen ZHANG, Wubian TIAN, Zhengming SUN. High-purity Ti2AlC Powder: Preparation and Application in Ag-based Electrical Contact Materials[J]. Journal of Inorganic Materials, 2020, 35(6): 729 Copy Citation Text show less
    XRD patterns of samples with different Al contents
    . XRD patterns of samples with different Al contents
    XRD patterns of samples with different C contents
    . XRD patterns of samples with different C contents
    SEM images of samples with different C contents
    . SEM images of samples with different C contents
    XRD patterns of 0.95TiC/1.05Ti/1.05Al sintered at different temperatures
    . XRD patterns of 0.95TiC/1.05Ti/1.05Al sintered at different temperatures
    Contact angles and optical images of Ag/Ti2AlC in the process of heating
    . Contact angles and optical images of Ag/Ti2AlC in the process of heating
    XRD pattern of Ag/10TAC composite with insets showing (a) picture of the bulk, (b) microstructure of composite, and (c) the magnified SEM image
    . XRD pattern of Ag/10TAC composite with insets showing (a) picture of the bulk, (b) microstructure of composite, and (c) the magnified SEM image
    (a) Optical image of the Ag/10TAC contact after 5610 arc discharging cycles, with magnified SEM image in the inset; (b) SEM image of the contact surface morphology; (c) Morphology of the Ag molten pool, with magnified SEM image of cauliflower-shaped Ag particles in the inset; (d) Magnified SEM image of the aggregated eroded Ti2AlC (dark area in (b))
    . (a) Optical image of the Ag/10TAC contact after 5610 arc discharging cycles, with magnified SEM image in the inset; (b) SEM image of the contact surface morphology; (c) Morphology of the Ag molten pool, with magnified SEM image of cauliflower-shaped Ag particles in the inset; (d) Magnified SEM image of the aggregated eroded Ti2AlC (dark area in (b))
    SampleComposition, xPurity/%
    S11.0577.5
    S21.1057.9
    S31.1541.4
    S41.2031.5
    Table 1.

    Molar ratio of raw material powder TiC/Ti/xAl

    SampleComposition, xPurity/%
    S11.0077.5
    S51.0599.2
    S61.1092.3
    S71.1591.7
    Table 2.

    Molar ratio of raw material powder (2-x)TiC/xTi/1.05Al

    SampleTemperature/℃Purity/%
    S8120016.3
    S9130035.7
    S10140099.2
    S11150081.8
    Table 3.

    Preparation of Ti2AlC powder from 0.95TiC/1.05Ti/1.05Al at different temperatures

    Density/(g·cm-3)Relative density/%Hardness, HVResistivity/(nΩ·m)
    8.69295.7%9679.5
    Table 4.

    Basic properties of Ag/Ti2AlC composite

    Jianxiang DING, Peiyan HUANG, Yuhui ZHA, Dandan WANG, Peigen ZHANG, Wubian TIAN, Zhengming SUN. High-purity Ti2AlC Powder: Preparation and Application in Ag-based Electrical Contact Materials[J]. Journal of Inorganic Materials, 2020, 35(6): 729
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