• Spectroscopy and Spectral Analysis
  • Vol. 41, Issue 12, 3759 (2021)
Si-qian SHI*, Fang-wei YANG, Wei-rong YAO, Hang YU, and Yun-fei XIE*;
Author Affiliations
  • College of Food, Jiangnan University, Wuxi 214000, China
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    DOI: 10.3964/j.issn.1000-0593(2021)12-3759-06 Cite this Article
    Si-qian SHI, Fang-wei YANG, Wei-rong YAO, Hang YU, Yun-fei XIE. Rapid Detection of Levamisole Residue in Pork by Surface Enhanced Raman Spectroscopy[J]. Spectroscopy and Spectral Analysis, 2021, 41(12): 3759 Copy Citation Text show less
    Chemical structural formula of levamisole
    Fig. 1. Chemical structural formula of levamisole
    Theoretical calculation results of levamisole hydrochloride(a): Optimize molecular structural formula of levamisole hydrochloride; (b): Comparison between theoretical Raman spectra and solid Raman spectra
    Fig. 2. Theoretical calculation results of levamisole hydrochloride
    (a): Optimize molecular structural formula of levamisole hydrochloride; (b): Comparison between theoretical Raman spectra and solid Raman spectra
    SERS peak intensity at 469 cm-1 under different detection conditions
    Fig. 3. SERS peak intensity at 469 cm-1 under different detection conditions
    SERS spectra of levamisole hydrochloride in methanol solution with different concentrationsa—j, solid, methanol, 0.01, 0.1, 1, 10, 75, 100, 250, 500 mg·L-1 solution respectively
    Fig. 4. SERS spectra of levamisole hydrochloride in methanol solution with different concentrations
    aj, solid, methanol, 0.01, 0.1, 1, 10, 75, 100, 250, 500 mg·L-1 solution respectively
    Linear relationship between peak intensity and concentration
    Fig. 5. Linear relationship between peak intensity and concentration
    Comparison of extraction effects of different extraction methodsa: Solid; b: Once liquid-liquid extraction blank; c: Once liquid-liquid extraction standard addition; d: Twice liquid-liquid extraction blank; e: Twice liquid-liquid extraction standard addition
    Fig. 6. Comparison of extraction effects of different extraction methods
    a: Solid; b: Once liquid-liquid extraction blank; c: Once liquid-liquid extraction standard addition; d: Twice liquid-liquid extraction blank; e: Twice liquid-liquid extraction standard addition
    Comparison of extraction effects of different extraction solventsa: Solid; b: Ethyl acetate blank; c: n-hexane blank; d: Chloroform blank; e: Ethyl acetate extraction; f: n-hexane extraction; g: Chloroform extraction
    Fig. 7. Comparison of extraction effects of different extraction solvents
    a: Solid; b: Ethyl acetate blank; c: n-hexane blank; d: Chloroform blank; e: Ethyl acetate extraction; f: n-hexane extraction; g: Chloroform extraction
    Si-qian SHI, Fang-wei YANG, Wei-rong YAO, Hang YU, Yun-fei XIE. Rapid Detection of Levamisole Residue in Pork by Surface Enhanced Raman Spectroscopy[J]. Spectroscopy and Spectral Analysis, 2021, 41(12): 3759
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