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Journal of Inorganic Materials
Contents
2020
Volume: 35 Issue 7
14 Article(s)
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RESEARCH LETTERS
Flux Growth of Tungsten Oxychloride Li
23
CuW
10
O
40
Cl
5
Shufang LI, Shuang ZHAO, and Manrong LI
Mixed anion compounds can generate the emergence of novel properties that differ from those with mono-type anion due to the difference of electronegativities, ionic radii, polarizabilities, and oxidation states between unlike anions. Abundant research has been conducted on metallic mixed-anion materials with potential
Mixed anion compounds can generate the emergence of novel properties that differ from those with mono-type anion due to the difference of electronegativities, ionic radii, polarizabilities, and oxidation states between unlike anions. Abundant research has been conducted on metallic mixed-anion materials with potential application in electronics, detectors of moisture, gas sensors, electrodes for solar batteries,
etc.
The flux method has been widely applied for mixed-anion crystal growth, which based on metathetical reaction with appropriate metal-salts ?ux under mild conditions. It is meaningful to synthesize the mixed anion compounds by the flux method. Single crystals of tungsten oxychloride Li
23
CuW
10
O
40
Cl
5
were prepared
via
CuCl
2
flux-growth method by two steps, which using high quality and phase-pure polycrystalline Li
4
WO
5
as precursor. The crystal structure was determined by single-crystal X-ray diffraction analysis, which indicates that Li
23
CuW
10
O
40
Cl
5
crystallizes in P6
3
/mcm space group (
a
= 1.02846(3) nm,
c
=1.98768(9) nm,
V
=1.82076(11) nm
3
, and
Z
=2). There are crystallographically independent five Li, two W, one Cu, two Cl, and five O atoms in the unit cell, where W(1) atoms are coordinated with one Cl and five O atoms in a distorted octahedra geometry, while W(2) atoms are connected with four O atoms in a tetrahedral coordination. The Cu atoms are connected with six O atoms forming [CuO
6
] octahedra. Thus, the crystal structure of the titled compound consists of [CuO
6
] and [W(1)O
5
Cl] octahedra, and [W(2)O
4
] tetrahedra. The successful synthesis of tungsten oxychloride Li
23
CuW
10
O
40
Cl
5
through flux-growth method is meaningful for explore new mixed anion compounds in future..
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Journal of Inorganic Materials
Publication Date: Jul. 20, 2020
Vol. 35, Issue 7, 834 (2020)
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Fabrication of Z-scheme BiVO
4
/GO/g-C
3
N
4
Photocatalyst with Efficient Visble-light Photocatalytic Performance
Shichao XU, Tianzhe ZHU, Yang QIAO, Xuejian BAI, Nan TANG, and Chunming ZHENG
Fabricating Z-scheme photocatalysts is a promising method for improving photocatalytic activity by effectively enhancing charge separation. A new Z-scheme BiVO4/GO/g-C3N4 photocatalyst was prepared by two steps of impregnation-calcination and hydrothermal method, and then characterized by different methods. In the phot
Fabricating Z-scheme photocatalysts is a promising method for improving photocatalytic activity by effectively enhancing charge separation. A new Z-scheme BiVO
4
/GO/g-C
3
N
4
photocatalyst was prepared by two steps of impregnation-calcination and hydrothermal method, and then characterized by different methods. In the photocatalytic process of BiVO
4
/GO/g-C
3
N
4
, GO nanosheet act as fast transmission channels between BiVO
4
and g-C
3
N
4
and can suppress electron-hole recombination, which significantly promotes the charge separation and improves the redox ability of the ternary heterojunction. The ternary photocatalyst has good photocatalytic degradation of Rhodamine B (RhB) as compared to the single-component or binary composite. It is capable of degrading 85% of RhB in 120 min under visible light irradiation and the hole (h
+
) plays a major role in the reaction. This work provides a simple preparation method for a ternary photocatalyst system in which g-C
3
N
4
coupled with BiVO
4
by GO to significantly improve photocatalytic activity..
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Journal of Inorganic Materials
Publication Date: Jul. 20, 2020
Vol. 35, Issue 7, 839 (2020)
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RESEARCH PAPER
Synergistic Effect of Ag and Ag
2
O on Photocatalytic H
2
-evolution Performance of TiO
2
Ping WANG, Xinyu LI, Zhanling SHI, and Haitao LI
Highly efficient TiO2 photocatalysts (TiO2/Ag-Ag2O) co-modified by Ag as electron cocatalysts and Ag2O as interfacial catalytic active sites were synthesized via a two-step process including the initial photoinduced deposition of metallic Ag nanoparticles on the TiO2 surface (TiO2/Ag) and the following in situ oxidatio
Highly efficient TiO
2
photocatalysts (TiO
2
/Ag-Ag
2
O) co-modified by Ag as electron cocatalysts and Ag
2
O as interfacial catalytic active sites were synthesized
via
a two-step process including the initial photoinduced deposition of metallic Ag nanoparticles on the TiO
2
surface (TiO
2
/Ag) and the following
in situ
oxidation of partial Ag into Ag
2
O by low-temperature calcination. Ag nanoparticles function as effective electron cocatalysts for the steady capture and rapid transportation of photogenerated electrons from TiO
2
surface to Ag
2
O, while the adsorbed H
+
ions from solution to Ag
2
O as the interfacial catalytic active sites are reduced into H
2
. The synergistic effect of Ag and Ag
2
O can accelerate the electrons transfer and promote the rapid H
2
-evolution reaction for enhanced photocatalytic H
2
-evolution performance of TiO
2
/Ag-Ag
2
O. The highest H
2
-evolution rate of the resultant TiO
2
/Ag-Ag
2
O calcinated at 300 ℃ reached 75.20 μmol/h, which was higher than those of the TiO
2
(3.59 μmol/h) and TiO
2
/Ag (41.13 μmol/h) by 21.0 and 1.8 times, respectively. This study provides a new strategy for the design and synthesis of highly efficient photocatalytic H
2
-evolution materials..
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Journal of Inorganic Materials
Publication Date: Jul. 20, 2020
Vol. 35, Issue 7, 781 (2020)
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Morphology and Photocatalytic Performance Regulation of Nd
3+
-doped BiVO
4
with Staggered Band Structure
Jingwei XU, Zheng LI, Zepu WANG, Han YU, Qi HE, Nian FU, Bangfu DING, Shukai ZHENG, and Xiaobing YAN
To investigate the modification mechanism of mixed heterogeneous on photocatalysis, a series of Nd3+-doped BiVO4 photo-catalysts with different Nd3+ contents were synthesized through a facile hydrothermal reaction. The samples exhibit Nd3+ content-dependent phase transition from monoclinic to tetragonal phase, as demon
To investigate the modification mechanism of mixed heterogeneous on photocatalysis, a series of Nd
3+
-doped BiVO
4
photo-catalysts with different Nd
3+
contents were synthesized through a facile hydrothermal reaction. The samples exhibit Nd
3+
content-dependent phase transition from monoclinic to tetragonal phase, as demonstrated by XRD and Raman analyses. SEM images show that the phase transition is accompanied by obvious morphology variation. Less than 1at% Nd
3+
-doped monocline BiVO
4
is composed of irregular particles, while more than 7at% Nd
3+
doping results in tetragonal phase BiVO
4
of sphere-like or kernel with groove surface. When Nd
3+
content is in the range of 1at%-7at%, the micron cuboid bars appear in the samples. More importantly, monoclinic and tetragonal phase is concomitant in the product and a heterogeneous junction with staggered band structure is formed. The Rhodamine B degradation efficiencies of all Nd
3+
-doped samples are higher than those of undoped samples due to the regular morphology after doping. The formed heterogeneous junction inhibits photo-generated electrons and holes recombination of Nd
3+
-doped BiVO
4
, inducing 99.4% catalytic efficiency in 4at% Nd
3+
-doped sample. The novel morphology and the intrinsic mechanism of photocatalysis enhancement upon Nd
3+
-doped BiVO
4
are obtained from the synthesis strategy and the energy band structure..
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Journal of Inorganic Materials
Publication Date: Jul. 20, 2020
Vol. 35, Issue 7, 789 (2020)
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Trace SiO
2
Addition on Optical and Scintillation Property of Pr:Lu
3
Al
5
O
12
Ceramics
Zewang HU, Xiaopu CHEN, Xin LIU, Xiaoying LI, Yun SHI, Huamin KOU, Tengfei XIE, and Jiang LI
Sintering aids are widely used to improve the optical quality of ceramics in the preparation of transparent ceramics. However, sintering aids may deteriorate the luminescent properties of the ceramics. In this work, 0.25at%Pr:LuAG scintillation ceramics were prepared by vacuum pre-sintering combined with hot isostatic
Sintering aids are widely used to improve the optical quality of ceramics in the preparation of transparent ceramics. However, sintering aids may deteriorate the luminescent properties of the ceramics. In this work, 0.25at%Pr:LuAG scintillation ceramics were prepared by vacuum pre-sintering combined with hot isostatic pressing. The influences of trace SiO
2
sintering aid on the optical and scintillation properties of the ceramics were studied. The results show that a small amount of SiO
2
below 200 ppm (1 ppm means that addition content is 1×10
-6
g/g) can effectively promote the remove of pore during hot isostatic pressing and improve the optical quality of the Pr:LuAG ceramics. Their in-line transmittance with 150 ppm SiO
2
is about 77% at 400 nm. The effects of pre-sintering temperature and holding time on the optical properties of Pr:LuAG ceramics were also investigated. When completely closed pore structure is formed, further increasing the pre-sintering temperature or prolonging the holding time reduce the densification rate in the hot isostatic pressing process, which is not conducive to the remove of pores and lower the optical quality of the Pr:LuAG ceramics. In addition, trace SiO
2
addition has less effect on scintillation properties of the Pr:LuAG ceramics. Adding trace SiO
2
sintering aid combined with hot isostatic pressing is an effective way to prepare Pr doped garnet scintillation ceramics..
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Journal of Inorganic Materials
Publication Date: Jul. 20, 2020
Vol. 35, Issue 7, 796 (2020)
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Adsorption-enrichment and Localized-photodegradation of Bentonite-supported Red Phosphorus Composites
Enquan ZHU, Yuhua MA, Munire AINIWA·, and Zhi SU
The hydrothermally treated red phosphorus (HRP) was dispersed on exfoliated bentonite (EB) supporter to prepare the EB/HRP photocatalyst for improving photocatalytic performance. The as-synthesized samples were characterized by different methods. Rhodamine B was selected as the model pollutant to evaluate the photodegr
The hydrothermally treated red phosphorus (HRP) was dispersed on exfoliated bentonite (EB) supporter to prepare the EB/HRP photocatalyst for improving photocatalytic performance. The as-synthesized samples were characterized by different methods. Rhodamine B was selected as the model pollutant to evaluate the photodegradation property of EB/HRP. Results showed that the photodegradation efficiency of the EB/HRP photocatalyst composite increased with increased EB mass fraction, and decreased after reaching the highest value. When the mass fraction of EB was 9%, the EB
9
/HRP photocatalyst composite exhibited the maximum adsorption performance and photodegradation activity. Its degradation rate constant
k
was 0.0641 min
-1
, which was two times that of HRP. In addition, after five cycles of photodegradation experiments, EB
9
/HRP still had high photocatalytic activity (96.8%). Therefore, the EB
9
/HRP catalyst composite had good photocatalytic activity and stability, which can be an efficient and stable photocatalyst for the degradation of pollutants..
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Journal of Inorganic Materials
Publication Date: Jul. 20, 2020
Vol. 35, Issue 7, 803 (2020)
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RuFe Nanoparticles Modified Sheet-like BiVO
4
: High-efficient Synergistic Catalyst for Ammonia Borane Hydrolytic Dehydrogenation
Yiqing ZHANG, Shujuan ZHANG, Zhengrui WAN, Han MO, Niangui WANG, and Liqun ZHOU
Developing highly efficient and low-cost catalysts is crucial in the field of clean energy economy, in which ammonia borane (AB) has attracted great attention due to its high hydrogen production through the catalytic hydrolysis. In this work, BiVO4 nanosheet was firstly synthesized by a facile reflux method. And then b
Developing highly efficient and low-cost catalysts is crucial in the field of clean energy economy, in which ammonia borane (AB) has attracted great attention due to its high hydrogen production through the catalytic hydrolysis. In this work, BiVO
4
nanosheet was firstly synthesized by a facile reflux method. And then bimetallic RuFe@BiVO
4
catalysts with different molar ratios of Ru/Fe were prepared
via in situ
impregnation-reduction techniques and their catalytic activities were also tested in the hydrogen generation from aqueous solution of AB at room temperature. Compared with the releasing hydrogen rates of catalysts of BiVO
4
, Ru@BiVO
4
, Fe@BiVO
4
, RuFe NPs and RuFe@BiVO
4
, respectively, Ru
1
Fe
0.1
@BiVO
4
exhibits the highest catalytic activity for the dehydrogenation of AB among all catalysts, the activation energy (
E
a
) and turnover frequency (TOF) are 43.7 kJ·mol
-1
and 205.4 mol
H2
·mol
Ru
·min
-1
, respectively. The addition of non-noble Fe can significantly enhance the catalytic activity of Ru counterparts, which is closely related to the strong electronic effect between Ru and Fe NPs, bi-functional effect generated between the RuFe NPs and the support BiVO
4
..
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Journal of Inorganic Materials
Publication Date: Jul. 20, 2020
Vol. 35, Issue 7, 809 (2020)
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Creep Properties and Damage Mechanisms of 2D-SiC
f
/SiC Composites Prepared by CVI
Xi WANG, Kejie WANG, Hui BAI, Zhuolin SONG, Bo WANG, and Chengyu ZHANG
The creep properties of 2D-SiCf/SiC composites prepared by chemical vapor infiltration were studied. The creep temperatures were 1200, 1300 and 1400 ℃, and the stress levels ranged from 100 MPa to 140 MPa. Scanning electron microscope was used to observe the fracture morphology, and their microstructure was analyzed by
The creep properties of 2D-SiC
f
/SiC composites prepared by chemical vapor infiltration were studied. The creep temperatures were 1200, 1300 and 1400 ℃, and the stress levels ranged from 100 MPa to 140 MPa. Scanning electron microscope was used to observe the fracture morphology, and their microstructure was analyzed by high resolution transmission electron microscope. The results show that the creep damage modes of 2D-SiC
f
/SiC composites mainly include the generation of matrix crack, interfacial debonding and fiber creep. The creep of bridging fibers leads to increase of the opening distance of the matrix cracks and further creep rupture of the composite. The microstructural stability of the SiC fiber plays a critical role in the creep properties of 2D-SiC
f
/SiC composites. SiC grains in the fibers of 2D-SiC
f
/SiC composites do not grow when it is crept at 1200 ℃/100 MPa. However, the grains grow significantly when the creep temperature increases to 1400 ℃. The creep rupture time decreases to 8.6 h from above 200 h, and the steady-state creep rate increases by three orders of magnitude..
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Journal of Inorganic Materials
Publication Date: Jul. 20, 2020
Vol. 35, Issue 7, 817 (2020)
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Reaction Synthesizes of ZrN and Phase Diagram in the Si
3
N
4
-ZrO
2
-La
2
O
3
System
Yanrui LI, Youjun LU, Yang LIU, Zhenxia YUAN, and Zhenkun HUANG
Si3N4-ZrO2-La2O3 ternary system were prepared via solid-state reaction at 1500 ℃ for 1 h with N2 protection, yielding coexistence phase of ZrN and lanthanum-based compounds, such as La4.67Si3O13, La5Si3NO12, La4Si2N2O7, LaSiNO2, and La2Zr2O7. Since the generated ZrN and lanthanum-based compounds are not located on the
Si
3
N
4
-ZrO
2
-La
2
O
3
ternary system were prepared
via
solid-state reaction at 1500 ℃ for 1 h with N
2
protection, yielding coexistence phase of ZrN and lanthanum-based compounds, such as La
4.67
Si
3
O
13
, La
5
Si
3
NO
12
, La
4
Si
2
N
2
O
7
, LaSiNO
2
, and La
2
Zr
2
O
7
. Since the generated ZrN and lanthanum-based compounds are not located on the triangle plane of Si
3
N
4
-ZrO
2
-La
2
O
3
system, it is necessary to add SiO
2
to extend the ternary into quinary system of Si
3
N
4
-SiO
2
-La
2
O
3
-ZrO
2
-ZrN. After the phase diagram of this quinary system is confirmed and presented, the phase diagram of La
2
O
3
-SiO
2
-ZrO
2
ternary subsystem at 1570 ℃ is further proposed for the first time. In addition, La
2
O
3
in the Si
3
N
4
-ZrO
2
-La
2
O
3
ternary system can help to simulate the substitution reaction between Si
3
N
4
and ZrO
2
to produce ZrN..
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Journal of Inorganic Materials
Publication Date: Jul. 20, 2020
Vol. 35, Issue 7, 822 (2020)
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Bi
2
Mn
4
O
10
: Preparation by Polyacrylamide Gel Method and Electrochemical Performance
Jing ZHAN, Changfan XU, Yiyu LONG, and Qihou LI
Due to competitive theoretical capacity, Bi2Mn4O10 has been deemed as an efficient Li-ion battery anode material. Bi2Mn4O10 powder was prepared by polyacrylamide gel method using bismuth nitrate and manganese acetate as raw materials. The effects of preparation conditions on the phase, morphology and electrochemical cy
Due to competitive theoretical capacity, Bi
2
Mn
4
O
10
has been deemed as an efficient Li-ion battery anode material. Bi
2
Mn
4
O
10
powder was prepared by polyacrylamide gel method using bismuth nitrate and manganese acetate as raw materials. The effects of preparation conditions on the phase, morphology and electrochemical cycling performance of powder were investigated. Results showed that the spheroid Bi
2
Mn
4
O
10
powder with narrow size distribution was successfully prepared under the conditions of molar ratio of acrylamide to total metal ions of 8 : 1, the glucose concentrations of 1.11 mol/L and heat treatment temperature of 873 K. Lithium ion batteries with as-prepared Bi
2
Mn
4
O
10
as anode material, acquired excellent cycle and rate performances. Its discharge specific capacity is 496.8 mAh/g at 0.2
C
(1
C
=800 mA/g) rate after 50 cycles, corresponding to a high capacity of 76.9%. Even at 3
C
rate, a superior rate capacity of 232 mAh/g is retained..
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Journal of Inorganic Materials
Publication Date: Jul. 20, 2020
Vol. 35, Issue 7, 827 (2020)
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REVIEW
Research Progress of Novel Two-dimensional Materials in Photocatalysis and Electrocatalysis
Neng LI, Zhouzhou KONG, Xingzhu CHEN, and Yufei YANG
Two-dimensional materials have attracted broad interest because of their wide variety of properties. They can be used as photocatalysts and electrocatalysts due to their extremely high specific surface area, and have great potential application in the field of environment and renewable energy. This review focuses on th
Two-dimensional materials have attracted broad interest because of their wide variety of properties. They can be used as photocatalysts and electrocatalysts due to their extremely high specific surface area, and have great potential application in the field of environment and renewable energy. This review focuses on the structure and properties of common two-dimensional materials such as 2D carbides and nitrides (MXenes), g-C
3
N
4
and black phosphorus (BP). Furthermore, the latest research on the modification of two-dimensional materials in the area of photocatalysis and electrocatalysis are discussed and commented. Finally, research prospects for two-dimensional materials in the future are predicted..
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Journal of Inorganic Materials
Publication Date: Jul. 20, 2020
Vol. 35, Issue 7, 735 (2020)
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Research Progress of Transition Metal Non-oxide High-entropy Ceramics
Lei CHEN, Kai WANG, Wentao SU, Wen ZHANG, Chenguang XU, Yujin WANG, and Yu ZHOU
High-entropy ceramics, a novel class of single-phase ceramic solid solutions consisting of near-equimolar multielement species, are recently attracting tremendous attentions. Especially, the transition metal non-oxide high-entropy ceramics, such as transition metal carbide and boride high-entropy ceramics, have been pr
High-entropy ceramics, a novel class of single-phase ceramic solid solutions consisting of near-equimolar multielement species, are recently attracting tremendous attentions. Especially, the transition metal non-oxide high-entropy ceramics, such as transition metal carbide and boride high-entropy ceramics, have been proposed for potential applications in aerospace, nuclear energy, high-speed machining and many other extreme environments, owing to their excellent physical and chemical properties including super-high hardness, low thermal conductivity, good oxidation resistance and corrosion/erosion resistance. Recently, the research of high-entropy ceramics is only focused on composition design, fabrication methods, single-phase stability and mechanical properties, but the design criterion and theoretical analysis are rarely reported. Based on the researches of high-entropy alloy, the fabrication, characterization and theoretical study of several transition metal non-oxide high-entropy ceramics are summarized, along with some related results of high-entropy film. The prospects for the future developments of high-entropy ceramics are also discussed..
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Journal of Inorganic Materials
Publication Date: Jul. 20, 2020
Vol. 35, Issue 7, 748 (2020)
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Progress on Hydrothermal Stability of Dental Zirconia Ceramics
Xiaoxu ZHANG, Dongbin ZHU, and Jinsheng LIANG
In recent years, zirconia ceramic, as a preferential choice for teeth restorations, is used as fixed partial dentures and implants due to its excellent mechanical properties, favorable biocompatibility and aesthetic properties, thus significantly shortening the performance life and seriously damaging the reliabilities.
In recent years, zirconia ceramic, as a preferential choice for teeth restorations, is used as fixed partial dentures and implants due to its excellent mechanical properties, favorable biocompatibility and aesthetic properties, thus significantly shortening the performance life and seriously damaging the reliabilities. However, zirconia ceramic easily occurs low temperature degradation (LTD) of
t-m
transformation in humid environments. This paper illustrated the characteristics, mechanism and kinetics of LTD, as well as the conventional characterization methods of LTD phenomena and new methods such as optical coherence tomography and focused ion beam. It is also shown the main factors affecting the aging phenomenon, and emphasized the inhibition methods of LTD. By developing materials system and improving processing technology to enhance the strength, fracture toughness of zirconia and to solve the LTD of zirconia, and to meet the needs of people for their health functionalization, zirconia ceramic will be widely applied in the dental restoration field..
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Journal of Inorganic Materials
Publication Date: Jul. 20, 2020
Vol. 35, Issue 7, 759 (2020)
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Application of Conductive Metal Organic Frameworks in Supercapacitors
Zehui LI, Meijuan TAN, Yuanhao ZHENG, Yuyang LUO, Qiushi JING, Jingkun JIANG, and Mingjie LI
With continuous development of electronics, the requirements for power supply systems are increasing. Supercapacitors (SCs), which have high energy density and excellent power output performance, are ideal power supplies for new generation of miniaturized, intelligent and wearable electronic devices. Thus, developing S
With continuous development of electronics, the requirements for power supply systems are increasing. Supercapacitors (SCs), which have high energy density and excellent power output performance, are ideal power supplies for new generation of miniaturized, intelligent and wearable electronic devices. Thus, developing SCs with fast charge-discharge speed and high stability is a key research topic in the field of energy storage. As the most important part of SCs, electrode materials are critical to its performance. Due to the excellent performances of high-ordered pore structure, large specific surface area, diverse morphologies and dimensions, and adjustable conductivity, conductive metal-organic frameworks (MOFs) materials have shown great potential as promising SCs electrode materials, and have attracted wide attention. This review introduces the structure, conductive mechanism and preparation methods of conductive MOFs following a short introduction of SCs, describes its design strategy as SCs electrode materials, reviews the research progress of conductive MOFs in the field of SCs, and prospects its future application..
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Journal of Inorganic Materials
Publication Date: Jul. 20, 2020
Vol. 35, Issue 7, 769 (2020)
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