• Journal of Inorganic Materials
  • Vol. 34, Issue 8, 803 (2019)
Sheng ZHANG, Yi JIANG, Yuan-Yuan JI, Ying DU, Zhen-Huan SHENG, Jing-Zhou YIN, Qiao-Qi LI, and Li-Li ZHANG*
Author Affiliations
  • Jiangsu Environmental Engineering Laboratory, Jiangsu Key Laboratory for Low-dimension Materials, School of Chemistry and Chemical Enginering, Huaiyin Normal University, Huaian 223300, China
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    DOI: 10.15541/jim20180373 Cite this Article
    Sheng ZHANG, Yi JIANG, Yuan-Yuan JI, Ying DU, Zhen-Huan SHENG, Jing-Zhou YIN, Qiao-Qi LI, Li-Li ZHANG. Attapulgite/g-C3N4 Composites: Synthesis and Electrocatalytic Oxygen Evolution Property[J]. Journal of Inorganic Materials, 2019, 34(8): 803 Copy Citation Text show less
    XRD patterns of different catalysts (a) and ATP/g-C3N4 with different proportions (b)
    1. XRD patterns of different catalysts (a) and ATP/g-C3N4 with different proportions (b)
    Infrared spectra of (a) different catalysts (a) and ATP/g-C3N4 with different proportions (b)
    2. Infrared spectra of (a) different catalysts (a) and ATP/g-C3N4 with different proportions (b)
    XPS spectra of ATP/g-C3N4-0.5 samples
    3. XPS spectra of ATP/g-C3N4-0.5 samples
    SEM images of g-C3N4(a) and ATP(b), SEM image (c) and (d) EDAX pattern of ATP/ g-C3N4-0.50
    4. SEM images of g-C3N4(a) and ATP(b), SEM image (c) and (d) EDAX pattern of ATP/ g-C3N4-0.50
    TG (a) and DSC (b) curves of different samples
    5. TG (a) and DSC (b) curves of different samples
    Cyclic voltammograms of catalytic materials
    6. Cyclic voltammograms of catalytic materials
    (a) LSV of ATP/g-C3N4-w and mechanical mixture, (b) LSV of g-C3N4 and ATP/g-C3N4, (c) LSV and the over potential (d) of ATP/g-C3N4-w
    7. (a) LSV of ATP/g-C3N4-w and mechanical mixture, (b) LSV of g-C3N4 and ATP/g-C3N4, (c) LSV and the over potential (d) of ATP/g-C3N4-w
    Tafel curves of g-C3N4 and ATP/g-C3N4-w
    8. Tafel curves of g-C3N4 and ATP/g-C3N4-w
    EIS curves of the oxygen evolution anode material
    9. EIS curves of the oxygen evolution anode material
    I-t curve of constant potential electrolysis of ATP/g-C3N4-0.50
    10. I-t curve of constant potential electrolysis of ATP/g-C3N4-0.50
    SampleSBET/(m2•g-1)
    ATP190.800
    g-C3N48.821
    ATP/g-C3N4-0.3326.980
    ATP/g-C3N4-0.4038.280
    ATP/g-C3N4-0.5053.180
    ATP/g-C3N4-0.6782.440
    Table 1. Specific surface area of each sample
    SampleE/V(vs RHE)η/mVTafel slope/(mV•dec-1)
    g-C3N41.73500155
    ATP/g-C3N4-0.671.68450175
    ATP/g-C3N4-0.501.64410118
    ATP/g-C3N4-0.401.65420128
    ATP/g-C3N4-0.331.69460143
    Table 2. Oxygen evolution overpotential E(V vs RHE) and overpotential of the catalyst at 10 mA/cm2 and the slope of the Tafel curve
    Sheng ZHANG, Yi JIANG, Yuan-Yuan JI, Ying DU, Zhen-Huan SHENG, Jing-Zhou YIN, Qiao-Qi LI, Li-Li ZHANG. Attapulgite/g-C3N4 Composites: Synthesis and Electrocatalytic Oxygen Evolution Property[J]. Journal of Inorganic Materials, 2019, 34(8): 803
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