• Spectroscopy and Spectral Analysis
  • Vol. 42, Issue 4, 1122 (2022)
Liang SHENG1、1;, Liang-jing YUAN2、2; *;, Dong-ling LI2、2;, Xiao-fen ZHANG3、3;, Qiao-chu ZHANG2、2;, Lei YU2、2;, and Yun-hai JIA1、1; *;
Author Affiliations
  • 11. Central Iron & Steel Research Institute, Beijing 100081, China
  • 22. NCS Testing Technology Co., Ltd., Beijing 100081, China
  • 33. University of Science and Technology Beijing, Beijing 100083, China
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    DOI: 10.3964/j.issn.1000-0593(2022)04-1122-07 Cite this Article
    Liang SHENG, Liang-jing YUAN, Dong-ling LI, Xiao-fen ZHANG, Qiao-chu ZHANG, Lei YU, Yun-hai JIA. Determination on Complex Inclusions of High-Speed Railway Wheel Using Spark Source Original Position Analysis[J]. Spectroscopy and Spectral Analysis, 2022, 42(4): 1122 Copy Citation Text show less
    Cross section of high railway wheel and its analysis area(a): SEM-EDS analysis area; (b): OPA analysis area
    Fig. 1. Cross section of high railway wheel and its analysis area
    (a): SEM-EDS analysis area; (b): OPA analysis area
    Microstructure morphologies and composition of typical inclusions(a): Al2O3; (b): MnS; (c): Al2O3/MnS;(d): Energy dispersive spectrum of Al2O3/MnS
    Fig. 2. Microstructure morphologies and composition of typical inclusions
    (a): Al2O3; (b): MnS; (c): Al2O3/MnS;(d): Energy dispersive spectrum of Al2O3/MnS
    Spectral threshold of Al2O3 inclusion
    Fig. 3. Spectral threshold of Al2O3 inclusion
    Fitting curve between the average area of Al2O3 inclusion and the spectral intensity
    Fig. 4. Fitting curve between the average area of Al2O3 inclusion and the spectral intensity
    Fitting curve between the average area of MnS inclusion and the spectral intensity
    Fig. 5. Fitting curve between the average area of MnS inclusion and the spectral intensity
    Sequential diagram of Al single sparks
    Fig. 6. Sequential diagram of Al single sparks
    Sequential diagram of MnS inclusion
    Fig. 7. Sequential diagram of MnS inclusion
    Sequential diagram of Al2O3/MnS complex inclusions
    Fig. 8. Sequential diagram of Al2O3/MnS complex inclusions
    The relation curve of the areas of Al2O3/MnS complex inclusions measured by SEM and OPA
    Fig. 9. The relation curve of the areas of Al2O3/MnS complex inclusions measured by SEM and OPA
    夹杂物尺寸
    范围/μm
    夹杂物面积
    范围/μm2
    轮毂部分A1轮辐部分A2轮辋部分A3
    Al2O3
    杂物/颗
    MnS夹
    杂物/颗
    Al2O3/MnS复
    合夹杂物/颗
    Al2O3
    杂物/颗
    MnS夹
    杂物/颗
    Al2O3/MnS复
    合夹杂物/颗
    Al2O3
    杂物/颗
    MnS夹
    杂物/颗
    Al2O3/MnS复
    合夹杂物/颗
    0~30~7.15592 9421533011 2773219115 007635
    3~57.1~19.62862 4653773046443087322 312721
    5~719.6~38.51361 329183139228137237655257
    7~938.5~63.654530914568696516967
    9~1163.6~95272585081611254532
    11~1395~132.71075181151110104
    13~15132.7~176.64284511261
    >15>176.63145711210
    Table 1. Inclusion size distribution measured by SEM
    夹杂物尺寸
    范围/μm
    夹杂物面积
    范围/μm2
    Al2O3/MnS复合
    夹杂物/颗
    0~30~7.1761
    3~57.1~19.61 111
    5~719.6~38.51 398
    7~938.5~63.61 304
    9~1163.6~951 202
    11~1395~132.71 042
    13~15132.7~176.6523
    >15>176.6498
    Table 2. Inclusion size distribution of complex inclusions of B1 region of the bub by using OPA analysis
    夹杂物尺寸
    范围/μm
    夹杂物面积
    范围/μm2
    OPA分析Al2O3/MnS
    复合夹杂物/颗
    OPA分析归一化后Al2O3/MnS
    复合夹杂物/颗
    SEM分析Al2O3/MnS
    复合夹杂物/颗
    0~30~7.1403101321
    3~57.1~19.6723362308
    5~719.6~38.5888127137
    7~938.5~63.69927169
    9~1163.6~957673211
    11~1395~132.78271511
    13~15132.7~176.640031
    >15 μm>176.635241
    Table 3. Inclusion size distribution of Al2O3/MnS complex inclusions of B2 region of the spoke
    夹杂物尺寸
    范围/μm
    夹杂物面积
    范围/μm2
    OPA分析Al2O3/MnS
    复合夹杂物/颗
    OPA分析归一化后Al2O3/MnS
    复合夹杂物/颗
    SEM分析Al2O3/MnS
    复合夹杂物/颗
    0~30~7.11 119280635
    3~57.1~19.61 671836721
    5~719.6~38.51 793256257
    7~938.5~63.61 79212867
    9~1163.6~951 4576132
    11~1395~132.71 070194
    13~15132.7~176.654241
    >15 μm>176.638740
    Table 4. Size distribution of Al2O3/MnS complex inclusions of B3 region of the rim
    分析方式SEMOPA
    面积/
    μm2
    等效直径/
    μm
    面积/
    μm2
    等效直径/
    μm
    轮毂部分2681941423
    轮辐部分1821541423
    轮辋部分1451440123
    Table 5. The maximum size of Al2O3/MnS complex inclusions over each cross section of high speed railway wheel
    Liang SHENG, Liang-jing YUAN, Dong-ling LI, Xiao-fen ZHANG, Qiao-chu ZHANG, Lei YU, Yun-hai JIA. Determination on Complex Inclusions of High-Speed Railway Wheel Using Spark Source Original Position Analysis[J]. Spectroscopy and Spectral Analysis, 2022, 42(4): 1122
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