Jian-Huang KE, Kai XIE, Yu HAN, Wei-Wei SUN, Shi-Qiang LUO, Jin-Feng LIU. Morphology Controlling of the High-voltage Cathode Materials with Different Co-solvents [J]. Journal of Inorganic Materials, 2019, 34(6): 618

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- Journal of Inorganic Materials
- Vol. 34, Issue 6, 618 (2019)

1. XRD patterns of the LCP obtained from solvents (a) LCP-Theor. (ICSD#87422), (b) LCP-ET, (c) LCP-EG and (d) LCP-DEG

2. SEM images of the LCP obtained from various solvents

3. Relationship curves for the viscosity and solubility with the average particle size of LCP powders obtained from different solvents

4. Schematic illustration for nucleation and crystal growth of LiCoPO4 under solvothermal conditions

5. (a) Capacity retentions and (b) specific capacities vs. C rate obtained in each cycle for LiCoPO4 samples synthesized by solvothermal process using various co-solvents

6. (a) Charge and discharge profiles of the samples obtained from various solvents; (b) Cyclic voltammetry characteristics of LCP-EG at a scanning rate of 0.05 mV/s
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Table 1. Variation of crystal parameters for LCP obtained from various solvents
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Table 2. BET analysis of the three samples
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Table 3. Physical parameters of four solvents

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