• Spectroscopy and Spectral Analysis
  • Vol. 42, Issue 11, 3387 (2022)
Xiang-cheng KAN*, Guang-qiang XIE, Yao-xiang LI*;, Li-hai WANG, Yi-na LI, Jun-ming XIE, and Xu TANG
Author Affiliations
  • College of Engineering and Technology, Northeast Forestry University, Harbin 150040, China
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    DOI: 10.3964/j.issn.1000-0593(2022)11-3387-08 Cite this Article
    Xiang-cheng KAN, Guang-qiang XIE, Yao-xiang LI, Li-hai WANG, Yi-na LI, Jun-ming XIE, Xu TANG. Influence of Temperature Change on the Prediction of Wood Moisture Content by NIR[J]. Spectroscopy and Spectral Analysis, 2022, 42(11): 3387 Copy Citation Text show less
    Wood samples
    Fig. 1. Wood samples
    Average NIR spectra of wood at different temperatures(a): Pinus sylvestris; (b): Fraxinus mandshurica; (c): Populus sylvestris; (d): Korean pine
    Fig. 2. Average NIR spectra of wood at different temperatures
    (a): Pinus sylvestris; (b): Fraxinus mandshurica; (c): Populus sylvestris; (d): Korean pine
    The first-order derivative graphs of NIR spectral peaks of wood samples at 1 450 nm(a): Pinus sylvestris; (b): Fraxinus mandshurica; (c): Populus sylvestris; (d): Korean pine
    Fig. 3. The first-order derivative graphs of NIR spectral peaks of wood samples at 1 450 nm
    (a): Pinus sylvestris; (b): Fraxinus mandshurica; (c): Populus sylvestris; (d): Korean pine
    NIR spectral peak shifts of wood samples at different temperatures(a): Pinus sylvestris; (b): Fraxinus mandshurica; (c): Populus sylvestris; (d): Korean pine
    Fig. 4. NIR spectral peak shifts of wood samples at different temperatures
    (a): Pinus sylvestris; (b): Fraxinus mandshurica; (c): Populus sylvestris; (d): Korean pine
    Scores of the first two PCs of Pinus sylvestris samples at different temperatures
    Fig. 5. Scores of the first two PCs of Pinus sylvestris samples at different temperatures
    Principal component analysis cumulative variance plot
    Fig. 6. Principal component analysis cumulative variance plot
    Result of partial least squares discriminant analysis of different temperatures
    Fig. 7. Result of partial least squares discriminant analysis of different temperatures
    NIR spectra of Pinus sylvestris at different temperature (-20~30℃) (a): Raw spectra; (b): S-G smoothing+MSC;(c): S-G smoothing+MSC+1st derivative
    Fig. 8. NIR spectra of Pinus sylvestris at different temperature (-20~30℃)
    (a): Raw spectra; (b): S-G smoothing+MSC;(c): S-G smoothing+MSC+1st derivative
    树种胸径
    /cm
    距髓心
    距离/cm
    最高含水
    率/%
    最低含水
    率/%
    平均含水
    率/%
    樟子松24635.3565.9256.62
    水曲柳20630.9554.3643.16
    大青杨22639.3675.2368.6
    红松17634.2663.8451.23
    Table 1. Nature of the samples
    设备名称型号参数生产厂家
    LabSpec便携式快速扫描光谱仪FR /A114260波长范围为: 350~2 500 nm美国ASD公司
    红外线测温仪TA601测量精度: ±1 ℃; 发射率ε: 0.1~1.0中国特安斯公司
    烘箱401-3BC温度范围: 50~300 ℃; 均匀度: ±1%杭州蓝天化验仪器厂
    恒温恒湿箱CLC-B2V-M温度范围0~99 ℃; 温度波动±0.1 ℃;
    湿度范围10~95%rH
    德国MMM group公司
    冰柜BD/C-100A最低温度-30 ℃中国容声公司
    Table 2. Experimental equipments
    Table 3. The RMSEP of the validation sets predicted by the calibration models developed by the NIR spectra collected under different temperatures
    校正集验测集
    RcRMSECRpRMSEP
    无预处理樟子松0.8370.1300.8260.156
    水曲柳0.8500.1250.8320.151
    大青杨0.7860.1860.7760.192
    红松0.8450.1330.8120.169
    MA樟子松0.8670.1110.8610.132
    水曲柳0.8690.1090.8660.121
    大青杨0.8210.1450.8010.152
    红松0.8650.1230.8600.135
    SG樟子松0.8970.1210.8900.129
    水曲柳0.8890.1030.8810.115
    大青杨0.8860.1230.8790.123
    红松0.9110.1130.9050.123
    MSC樟子松0.9070.1010.9000.114
    水曲柳0.8820.1010.8810.114
    大青杨0.8860.1120.8810.106
    红松0.9110.1030.9110.120
    一次微分樟子松0.9480.0960.9420.099
    水曲柳0.9500.0950.9480.095
    大青杨0.9490.0990.9450.102
    红松0.9590.0920.9400.113
    SG+MSC樟子松0.9430.0990.9390.102
    水曲柳0.9560.0880.9480.094
    大青杨0.9400.1020.9350.109
    红松0.9510.0820.9470.088
    SG+MSC+
    一次微分
    樟子松0.9780.0860.9720.085
    水曲柳0.9810.0750.9780.074
    大青杨0.9790.0760.9750.080
    红松0.9790.0820.9770.088
    Table 4. Prediction results of PLS models using different sectral preprocessing methods
    Xiang-cheng KAN, Guang-qiang XIE, Yao-xiang LI, Li-hai WANG, Yi-na LI, Jun-ming XIE, Xu TANG. Influence of Temperature Change on the Prediction of Wood Moisture Content by NIR[J]. Spectroscopy and Spectral Analysis, 2022, 42(11): 3387
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