Author Affiliations
1School of Precision Instrument and Opto-Electronics Engineering, Tianjin University, Tianjin 300072, China2Key Laboratory of Opto-Electronics Information Technology of Ministry of Education, Tianjin 300072, China3Zhuhai Linkoptik Instruments Co., Ltd., Zhuhai 519085, Guangdong , Chinashow less
Fig. 1. Position of the photoelectric detection unit in the scattering light field
Fig. 2. Signal distribution and power spectrum of scattering light. (a) Particles with a particle size of 1 μm; (b) particles with a particle size of 100 μm
Fig. 3. Fγ(D)curve of scattered light distribution of particles. (a) Single particle size; (b) average particle size segment
Fig. 4. Lower limit of measurement for the ideal model. (a) Effect of noise on the lower limit of measurement; (b) effect of the refractive index of particles on the lower limit of measurement
Fig. 5. Resolving power of ideal model under different noise. (a) mi =0; (b) mi =0.1
Fig. 6. Effect of the real part of refractive index on resolving power (mi=0.1)
Fig. 7. Experimental device approximate to ideal laser particle size analyzer
Fig. 8. Particle size measurement results of single-dispersed standard samples. (a) 50 nm; (b) 100 nm; (c) 200 nm; (d) 300 nm
Fig. 9. Particle size measurement results for samples with bimodal distribution. (a) 50 nm and 200 nm; (b) 100 nm and 200 nm; (c) 200 nm and 300 nm; (d) 300 nm and 400 nm
Sample size /nm | 50 | 100 | 200 | 300 |
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Density coefficient | 1.0905 | 1.1892 | 1.0905 | 1.1892 | 1.0905 | 1.1892 | 1.0905 | 1.1892 | Median /nm | 51.87 | 50.55 | 99.25 | 98.29 | 199.67 | 198.05 | 301.22 | 303.24 | 51.21 | 53.42 | 98.57 | 97.83 | 198.93 | 197.39 | 299.49 | 302.61 | 53.25 | 53.38 | 99.30 | 99.80 | 199.24 | 198.85 | 301.30 | 302.84 | Mean D50 /nm | 52.11 | 52.45 | 99.04 | 98.64 | 199.28 | 198.10 | 300.67 | 302.90 | S /nm | 1.04 | 1.65 | 0.41 | 1.03 | 0.45 | 0.73 | 1.02 | 0.32 | Cv /% | 1.99 | 3.14 | 0.41 | 1.04 | 0.23 | 0.37 | 0.34 | 0.11 | Reference /nm | 51±3 | 100±6 | 203±5 | 303±6 |
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Table 1. Particle size measurement results of single-dispersed standard samples
Sample size /nm | 50 | 100 | 200 | 300 |
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d1 /μm | 0.051 | 0.100 | 0.203 | 0.303 | R /% | 22.4 | 50.5 | 67.3 | 75.0 | d2 /μm | 0.203 | 0.203 | 0.303 | 0.401 | D2 /μm | 0.223 | 0.198 | 0.297 | 0.400 |
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Table 2. Combination of the distinguishing test experiment mix