• Acta Optica Sinica
  • Vol. 37, Issue 10, 1029001 (2017)
Linchao Pan1、2, Baozhen Ge1、2, and Fugen Zhang1、3、*
Author Affiliations
  • 1 School of Precision Instrument and Opto-Electronics Engineering, Tianjin University, Tianjin 300072, China
  • 2 Key Laboratory of Opto-Electronics Information Technology, Ministry of Education, Tianjin 300072, China
  • 3 Zhuhai Linkoptik Instruments Co., Ltd., Zhuhai, Guangdong 519085, China
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    DOI: 10.3788/AOS201737.1029001 Cite this Article Set citation alerts
    Linchao Pan, Baozhen Ge, Fugen Zhang. Laser Particle Size Measurement Based on Annular Sample Cell[J]. Acta Optica Sinica, 2017, 37(10): 1029001 Copy Citation Text show less
    (a) Typical optical structure of laser particle size analyzer; (b) structural schematic of traditional sample cell
    Fig. 1. (a) Typical optical structure of laser particle size analyzer; (b) structural schematic of traditional sample cell
    (a) Schematic of multiple beams; (b) schematic of trapezoidal sample cell; (c) schematic of prism sample cell; (d) schematic of cylindrical-lens sample cell
    Fig. 2. (a) Schematic of multiple beams; (b) schematic of trapezoidal sample cell; (c) schematic of prism sample cell; (d) schematic of cylindrical-lens sample cell
    (a) Propagation schematic of beams parallel to paper in laser particle size analyzer based on annular sample cell; (b) propagation schematic of incident rays and refractive rays parallel to paper within annular sample cell
    Fig. 3. (a) Propagation schematic of beams parallel to paper in laser particle size analyzer based on annular sample cell; (b) propagation schematic of incident rays and refractive rays parallel to paper within annular sample cell
    Propagation schematic of scattering light from particles at off-center position within sample cell
    Fig. 4. Propagation schematic of scattering light from particles at off-center position within sample cell
    (a) Light energy distributions corresponding to typical particle sizes, gray region is range of scattering angle unreceived by traditional sample cell; (b) ERMS versus α
    Fig. 5. (a) Light energy distributions corresponding to typical particle sizes, gray region is range of scattering angle unreceived by traditional sample cell; (b) ERMS versus α
    Schematic of reflection inside annular sample cell with blackened ektexine
    Fig. 6. Schematic of reflection inside annular sample cell with blackened ektexine
    Experimental setup with annular sample cell
    Fig. 7. Experimental setup with annular sample cell
    Measurement results of Duke standard particles. (a) 50 nm; (b) 100 nm; (c) 200 nm; (d) 400 nm; (e) mixed 100 nm and 200 nm particles; (f) mixed 200 nm and 400 nm particles
    Fig. 8. Measurement results of Duke standard particles. (a) 50 nm; (b) 100 nm; (c) 200 nm; (d) 400 nm; (e) mixed 100 nm and 200 nm particles; (f) mixed 200 nm and 400 nm particles
    Sample size /nm50100200400
    Measured D50 /nm49.1101206392
    48.7104202407
    49.1102204396
    Mean D50 /nm49.0102204398
    Cv /%0.51.51.02.0
    Referenced D50 /nm51±3100±3200±5400±9
    Table 1. Measurement results of Duke standard particles
    Linchao Pan, Baozhen Ge, Fugen Zhang. Laser Particle Size Measurement Based on Annular Sample Cell[J]. Acta Optica Sinica, 2017, 37(10): 1029001
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