• Journal of Inorganic Materials
  • Vol. 35, Issue 11, 1227 (2020)
Xuqin LI1, Zhiyong TAN2, Laifei CHENG3, Lingke ZHOU1, and Jian GAO1
Author Affiliations
  • 1School of Materials and Environmental Engineering, Chengdu Technological University, Chengdu 611730, China
  • 2Beijing Institute of Nearspace Vehicle's Systems Engineering, Beijing 100076, China
  • 3Science and Technology on Thermostructural Composite Materials Laboratory, Northwestern Polytechnical University, Xian 710072, China
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    DOI: 10.15541/jim20200109 Cite this Article
    Xuqin LI, Zhiyong TAN, Laifei CHENG, Lingke ZHOU, Jian GAO. Tensile Behaviors and Matrix Cracking Mechanism of C/SiCN Composite Prepared by Precursor Infiltration Pyrolysis Method[J]. Journal of Inorganic Materials, 2020, 35(11): 1227 Copy Citation Text show less
    XRD patterns of mini C/SiCN composite heat-treated at different temperatures
    1. XRD patterns of mini C/SiCN composite heat-treated at different temperatures
    (a) Typical tensile stress versus displacement curve for mini C/SiCN composite fabricated by different PIP cycles; (b) tensile strength as a function of PIP cycle
    2. (a) Typical tensile stress versus displacement curve for mini C/SiCN composite fabricated by different PIP cycles; (b) tensile strength as a function of PIP cycle
    SEM micrographs of mini C/SiCN composite fabricated by different PIP cycles (a) One cycle; (b) Two cycles; (c) Three cycles; (d) Four cycles
    3. SEM micrographs of mini C/SiCN composite fabricated by different PIP cycles (a) One cycle; (b) Two cycles; (c) Three cycles; (d) Four cycles
    Contour map and 3D surface view of surface roughness
    4. Contour map and 3D surface view of surface roughness
    Matrix crack spacing and crack opening distance as a function of PIP cycle
    5. Matrix crack spacing and crack opening distance as a function of PIP cycle
    Fiber pull-out for mini C/SiCN composite fabricated by different PIP cycles (a) One cycle; (b) Two cycles; (c) Three cycles; (d) Four cycles
    6. Fiber pull-out for mini C/SiCN composite fabricated by different PIP cycles (a) One cycle; (b) Two cycles; (c) Three cycles; (d) Four cycles
    Schematic of crack deflection
    7. Schematic of crack deflection
    Bonding between fiber and matrix of mini C/SiCN composite prepared by (a) one PIP cycle and (b) four PIP cycles
    8. Bonding between fiber and matrix of mini C/SiCN composite prepared by (a) one PIP cycle and (b) four PIP cycles
    (a) Typical tensile stress versus displacement curve for mini C/SiCN composite after heat-treatment at different temperatures; (b) the tensile strength as a function of heat treatment temperature
    9. (a) Typical tensile stress versus displacement curve for mini C/SiCN composite after heat-treatment at different temperatures; (b) the tensile strength as a function of heat treatment temperature
    SEM images of mini C/SiCN composite heat-treated at different temperatures (a) 1000 ℃; (b) 1200 ℃; (c) 1400 ℃; (d) 1600 ℃
    10. SEM images of mini C/SiCN composite heat-treated at different temperatures (a) 1000 ℃; (b) 1200 ℃; (c) 1400 ℃; (d) 1600 ℃
    Crystalline morphologies of the SiCN matrix after heat-treatment at 1600 ℃
    11. Crystalline morphologies of the SiCN matrix after heat-treatment at 1600 ℃
    Fiber pull-out for mini C/SiCN composite after heat-treatment at different temperatures (a) 1000 ℃; (b) 1200 ℃; (c) 1400 ℃; (d) 1600 ℃
    12. Fiber pull-out for mini C/SiCN composite after heat-treatment at different temperatures (a) 1000 ℃; (b) 1200 ℃; (c) 1400 ℃; (d) 1600 ℃
    Heat-treatment temperature/℃Stoichiometric ratioEquivalent content ratio
    1000Si1C2.96N0.26O0.300.15SiO2•0.07Si3N4•0.66SiC•0.75C
    1200Si1C2.98N0.27O0.320.16SiO2•0.07Si3N4•0.64SiC•0.76C
    1400Si1C2.49N0.24O0.300.15SiO2•0.06Si3N4•0.68SiC•0.70C
    1600Si1C2.36N0.11O0.120.06SiO2•0.03Si3N4•0.86SiC•0.60C
    Table 1. Chemical compositions of mini C/SiCN composite heat-treated at different temperatures
    Xuqin LI, Zhiyong TAN, Laifei CHENG, Lingke ZHOU, Jian GAO. Tensile Behaviors and Matrix Cracking Mechanism of C/SiCN Composite Prepared by Precursor Infiltration Pyrolysis Method[J]. Journal of Inorganic Materials, 2020, 35(11): 1227
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