• Spectroscopy and Spectral Analysis
  • Vol. 42, Issue 11, 3428 (2022)
Ai-guo OUYANG*, Bin YU, Jun HU, Tong-zheng LIN, and Yan-de LIU
Author Affiliations
  • Intelligent Electromechanical Equipment Innovation Research Institute, East China Jiaotong University, Nanchang 330013, China
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    DOI: 10.3964/j.issn.1000-0593(2022)11-3428-07 Cite this Article
    Ai-guo OUYANG, Bin YU, Jun HU, Tong-zheng LIN, Yan-de LIU. Grade Evaluation of Grain Size in High-Speed Railway Wheel Steel Based on Laser-Induced Breakdown Spectroscopy[J]. Spectroscopy and Spectral Analysis, 2022, 42(11): 3428 Copy Citation Text show less
    Metallographic organization images with 100 times magnification of samples with different grain sizes(a): at level 9.5; (b): at level 10.0; (c): at level 10.5;(d): at level 11.0; (e): at level 11.5
    Fig. 1. Metallographic organization images with 100 times magnification of samples with different grain sizes
    (a): at level 9.5; (b): at level 10.0; (c): at level 10.5;(d): at level 11.0; (e): at level 11.5
    A schematic diagram of LIBS system
    Fig. 2. A schematic diagram of LIBS system
    LIBS spectra of Fe, Cr, Mo and Co of 5 samples(a): the wavelength range of 402~406 nm; (b): the wavelength range of 423~427 nm;(c): the wavelength range of 384~388 nm; (d): the wavelength range of 239~243 nm
    Fig. 3. LIBS spectra of Fe, Cr, Mo and Co of 5 samples
    (a): the wavelength range of 402~406 nm; (b): the wavelength range of 423~427 nm;(c): the wavelength range of 384~388 nm; (d): the wavelength range of 239~243 nm
    Modelling results of PLS-DA based on full band spectral intensities pretreated by SNN(a): Training set; (b): Prediction set
    Fig. 4. Modelling results of PLS-DA based on full band spectral intensities pretreated by SNN
    (a): Training set; (b): Prediction set
    CARS wavelength screening process
    Fig. 5. CARS wavelength screening process
    Wavelength screening process of SPA
    Fig. 6. Wavelength screening process of SPA
    CARS-SPA wavelength screening process
    Fig. 7. CARS-SPA wavelength screening process
    ElementMass fraction/%ElementMass fraction/%
    C0.35V0.98
    Si0.32Mo2.02
    Mn1.27B0.003
    P0.012Co0.93
    Cr2.43
    Table 1. Main chemical composition of ER8 steel(Wt%)
    Numberthermal treatmentGrain size
    grades
    1875 ℃ normalizing+900 ℃ quenching9.5
    2raw material10.0
    3950 ℃ tempering10.5
    4875 ℃ normalizing+810 ℃ quenching11.0
    5800 ℃ normalizing11.5
    Table 2. Grain size grades of sample under different heat treatment conditions
    VariablePretreatment
    method
    MethodModeling setPrediction set
    Misjudgment
    times/piece
    Discrimination
    accuracy/%
    Misjudgment
    times/piece
    Discrimination
    accuracy/%
    Spectral
    line
    intensity
    NonePLS-DA0100486.7
    SNV495.7390
    MSC495.8583.3
    SG smoothing1089.4680
    Table 3. Results for model evaluation indeces
    MethodCharacteristic
    wavelength
    screening method
    Number of
    screening
    wavelengths
    Modeling setPrediction set
    Misjudgment
    times/piece
    Discrimination
    accuracy/%
    Misjudgment
    times/piece
    Discrimination
    accuracy/%
    CARS31297.9196.7
    PLS-DASPA105641.11646.7
    CARS-SPA141683.2390.0
    Table 4. PLS-DA discriminant analysis results based on different characteristic wavelength screening methods
    Ai-guo OUYANG, Bin YU, Jun HU, Tong-zheng LIN, Yan-de LIU. Grade Evaluation of Grain Size in High-Speed Railway Wheel Steel Based on Laser-Induced Breakdown Spectroscopy[J]. Spectroscopy and Spectral Analysis, 2022, 42(11): 3428
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