Author Affiliations
1 Key Laboratory of High Power Laser Materials, Shanghai Institute of Optics and Fine Mechanics, Chinese Academy of Sciences, Shanghai 201800, China2 University of Chinese Academy of Sciences, Beijing 100049, Chinashow less
Fig. 1. Requirements for mandrels in high brightness Yb-doped LMA-PCF
Fig. 2. MCVD process flowchart[26]
Fig. 3. Preparation of preform by DND process[35]
Fig. 4. Powder sintering process[37]
Fig. 5. Process of phase separation to prepare porous[43]
Fig. 6. Fabrication of rare earth doped optical fibers by phase separation method[45]
Fig. 7. Fabrication of large mode ytterbium doped fiber process by sol-gel process
Fig. 8. (a) Glass forming region of Yb/Al/P doped silica glass; (b) magnified view of glass forming region in area with high content of SiO224
Fig. 9. Performances of Yb3+ in YAP series samples[29]. (a) Absorption spectrum; (b) emission spectrum
Fig. 10. Raman spectra of Yb3+/Al3+/P5+ doped silica glass[26]
Fig. 11. Structure of Yb3+/Al3+/P5+ co-doped quartz glass[26]
Fig. 12. Effects of Yb2O3, Al2O3, P/Al ratio, and AlPO4 on refractive index of silica glass[26,29,31]
Fig. 13. Photographs of Yb-doped quartz glass mandrels
Fig. 14. Photographs of photonic crystal fibers and composition distribution of fiber cores. (a) PCF cross-sectional photographs; (b) EPMA line scan maps of Yb, Al, P, and F elements in fiber core
Fig. 15. Laser amplification system and output laser characteristics. (a) Main oscillator power amplifier system; (b) average pulse amplification power versus pump power. Insets are beam qualities at 120 W and 272 W, respectively
Fig. 16. Photo of photonic crystal fiber end face and laser amplification performance. (a) SEM photograph of large mode area PCF with 75 μm core diameter; (b) average pulse amplification power versus pump power
Fig. 17. Development of LMA-PCF fabricated by sol-gel method
Time | Composition | Mole fractionof Yb2O3 /% | Fibertype | Corediameter /μm | Lasersystem | Averagepower /W | Peakpower /MW | M2 | Reference |
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2013 | Yb/Al | 0.3 | PCF | 30 | CW | 6.8 | - | - | [22] | 2013 | Yb/Al | 0.1 | PCF | 90 | CW | 81 | - | - | [23] | 2013 | Yb/Al/P | 0.05 | PCF | 35 | CW | 35 | - | - | [53] | 2015 | Yb/Al/P | 0.035 | DCFPCF | 3550 | CW | 3.246 | -- | 1.3- | [57] | 2016 | Yb/Al | 0.1 | PCF | 105 | MOPA | 255 | 1.2 | >10 | [54] | 2016 | Yb/Al/F | 0.05 | DCF | 50 | CW | 8 | - | 1.1 | [20] | 2017 | Yb/Al | 0.1 | PCF | 100 | MOPA | 310 | 1.5 | 5 | [59] | 2017 | Yb/Al/P/F | 0.075 | PCF | 50 | MOPA | 97 | 0.093 | 1.4 | [55] | 2019 | Yb/Al/P/F | 0.09 | PCF | 50 | MOPA | 272 | 0.266 | 2.2 | [51] | 2019 | Yb/Al/P/F | 0.15 | PCF | 75 | MOPA | 102 | 1 | 2.1 | [60] |
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Table 1. Development of ytterbium doped silica fibers using sol-gel method
Core glass | Glass forming ability | Homogeneity | Refractive difference | Spectra properties | Reference |
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Yb/Al | Easy | 1×10-4 | Far larger than pure silica glass | Good | [22,52] | Yb/Al/P | Easy (with largerAl content than P) | 2×10-4 | (3-6)×10-4 | Great changes (withmuch larger P than Al) | [28-29,31] | Yb/Al/F | Easy | 2×10-4 | Almost equal to pure silica glass | Good | [20,30] | Yb/Al/P/F | Possible phaseseparation | 1×10-4 | Almost equal to pure silica glass | Good (with less Pcontent than Al) | [51,55-56] |
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Table 2. Characteristics of Yb-doped silica glass rods with different compositions
Specification | SIOM | Heraeus |
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Powder sintering | Sol-gel | SiCl4+H2O | Active glass rod diameter | >5 mm | >5 mm | Homogeneity | About1×10-4 | <2×10-4 | Codoping F | Yes | No | Codoping P | Yes | No | Core glass attenuation | >50 dB/km@1200 nm | <50 dB/km@1200 nm | Main application | Low NA ultra large mode fieldphotonic crystal fibers forpulse amplification | Ultra large core diameter claddingfiber for high average powerCW/pulsed fiber laser amplifier |
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Table 3. Performance comparison between Yb-doped quartz glass mandrel prepared by our research group and Heraeus products