• Spectroscopy and Spectral Analysis
  • Vol. 41, Issue 10, 3083 (2021)
Jing-xuan WU*, Jie LI*;, Jia-wei LIN, Shi-wen YI, Min LI, and Wen-rou SU
Author Affiliations
  • Key Laboratory of Integrated Exploitation of Bayan Obo Multi-Metal Resources, Inner Mongolia University of Science and Technology, Baotou 014010, China
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    DOI: 10.3964/j.issn.1000-0593(2021)10-3083-09 Cite this Article
    Jing-xuan WU, Jie LI, Jia-wei LIN, Shi-wen YI, Min LI, Wen-rou SU. Influence Mechanism of Microwave on Barite Flotation Based on Infrared Fitting Spectrum Analysis[J]. Spectroscopy and Spectral Analysis, 2021, 41(10): 3083 Copy Citation Text show less
    Effect of microwave pretreatment on flotation recovery of barite(a): Recovery rate under different dosages of sodium oleate; (b): Recovery rate under different pH values
    Fig. 1. Effect of microwave pretreatment on flotation recovery of barite
    (a): Recovery rate under different dosages of sodium oleate; (b): Recovery rate under different pH values
    Infrared spectra of barite before and after interaction with sodium oleat
    Fig. 2. Infrared spectra of barite before and after interaction with sodium oleat
    Infrared spectra of the interactions between barite and sodium oleate under different microwave heating timea: 0 s; b: 10 s; c: 30 s; d: 60 s
    Fig. 3. Infrared spectra of the interactions between barite and sodium oleate under different microwave heating time
    a: 0 s; b: 10 s; c: 30 s; d: 60 s
    High resolution spectra of barite flotation before and after microwave pretreatment(a): 3 000~2 800 cm-1; (b): 1 200~1 050 cm-1; (c): 1 000~970 cm-1; (d): 650~600 cm-1
    Fig. 4. High resolution spectra of barite flotation before and after microwave pretreatment
    (a): 3 000~2 800 cm-1; (b): 1 200~1 050 cm-1; (c): 1 000~970 cm-1; (d): 650~600 cm-1
    Fitted smoothed and second derivative spectra of barite treated by microwave heating for 0 second(a): 3 000~2 800 cm-1; (b): 1 200~1 050 cm-1; (c): 1 000~970 cm-1; (d): 650~600 cm-1
    Fig. 5. Fitted smoothed and second derivative spectra of barite treated by microwave heating for 0 second
    (a): 3 000~2 800 cm-1; (b): 1 200~1 050 cm-1; (c): 1 000~970 cm-1; (d): 650~600 cm-1
    Fitted smoothed and second derivative spectra of barite treated by microwave heating for 10 seconds(a): 3 000~2 800 cm-1; (b): 1 200~1 050 cm-1; (c): 1 000~970 cm-1; (d): 650~600 cm-1
    Fig. 6. Fitted smoothed and second derivative spectra of barite treated by microwave heating for 10 seconds
    (a): 3 000~2 800 cm-1; (b): 1 200~1 050 cm-1; (c): 1 000~970 cm-1; (d): 650~600 cm-1
    Fitted smoothed and second derivative spectra of barite treated by microwave heating for 30 seconds(a): 3 000~2 800 cm-1; (b): 1 200~1 050 cm-1; (c): 1 000~970 cm-1; (d): 650~600 cm-1
    Fig. 7. Fitted smoothed and second derivative spectra of barite treated by microwave heating for 30 seconds
    (a): 3 000~2 800 cm-1; (b): 1 200~1 050 cm-1; (c): 1 000~970 cm-1; (d): 650~600 cm-1
    Fitted smoothed and second derivative spectra of barite treated by microwave heating for 60 seconds(a): 3 000~2 800 cm-1; (b): 1 200~1 050 cm-1; (c): 1 000~970 cm-1; (d): 650~600 cm-1
    Fig. 8. Fitted smoothed and second derivative spectra of barite treated by microwave heating for 60 seconds
    (a): 3 000~2 800 cm-1; (b): 1 200~1 050 cm-1; (c): 1 000~970 cm-1; (d): 650~600 cm-1
    元素BaOSO3SiO2Na2OCaOAl2O3Fe2O3
    含量63.1932.992.450.340.730.230.07
    Table 1. XRF analysis results of barite pure minerals, %
    序号峰位/cm-1峰高半高宽/cm-1峰面积
    12 9580.007 836.449 20.304 1
    22 9230.015 536.996 50.609 9
    32 8530.004 524.814 80.118 4
    41 0860.050 832.813 11.752 6
    51 1220.039 537.829 91.589 2
    61 1810.024 727.459 70.701 1
    79820.011 310.493 30.125 6
    86100.041 812.449 00.542 8
    96350.026 514.760 70.413 6
    Table 2. Fitting results of barite treated by microwave heating for 0 second
    序号峰位/cm-1峰高半高宽/cm-1峰面积
    12 9580.011 533.392 50.407 8
    22 9230.022 537.083 10.888 2
    32 8530.006 120.510 70.131 5
    41 0860.065 832.877 62.261 9
    51 1220.060 446.205 42.971 5
    61 1810.035 329.661 71.077 3
    79820.040 59.177 70.389 1
    86100.097 213.858 91.391 0
    96350.074 116.186 41.260 9
    Table 3. Fitting results of barite treated by microwave heating for 10 seconds
    序号峰位/cm-1峰高半高宽/cm-1峰面积
    12 9580.016 434.281 90.598 2
    22 9230.031 837.362 11.264 6
    32 8530.008 720.130 90.186 3
    41 0860.095 734.205 83.421 8
    51 1220.076 937.800 83.097 3
    61 1810.052 128.010 41.500 1
    79820.045 59.387 70.448 3
    86100.132 513.865 21.904 1
    96350.107 015.611 11.757 2
    Table 4. Fitting results of barite treated by microwave heating for 30 seconds
    序号峰位/cm-1峰高半高宽/cm-1峰面积
    12 9580.014 120.693 60.309 7
    22 9230.051 539.970 22.190 3
    32 8530.028 333.825 51.019 6
    41 0860.151 737.364 25.883 9
    51 1220.111 332.943 53.903 2
    61 1810.081 424.938 42.092 8
    79820.104 28.499 80.930 9
    86100.249 113.654 13.526 4
    96350.220 715.076 33.494 8
    Table 5. Fitting results of barite treated by microwave heating for 60 seconds
    Jing-xuan WU, Jie LI, Jia-wei LIN, Shi-wen YI, Min LI, Wen-rou SU. Influence Mechanism of Microwave on Barite Flotation Based on Infrared Fitting Spectrum Analysis[J]. Spectroscopy and Spectral Analysis, 2021, 41(10): 3083
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