• Spectroscopy and Spectral Analysis
  • Vol. 32, Issue 9, 2572 (2012)
LONG Ling1、*, HUANG An-min1, MENG Di1, and LU Zhi-gang2
Author Affiliations
  • 1[in Chinese]
  • 2[in Chinese]
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    DOI: 10.3964/j.issn.1000-0593(2012)09-2572-04 Cite this Article
    LONG Ling, HUANG An-min, MENG Di, LU Zhi-gang. Determination of Pb, Cd and Cr in Surface Decorating Materials of Wood-Based Panels by Microwave Digestion-AAS[J]. Spectroscopy and Spectral Analysis, 2012, 32(9): 2572 Copy Citation Text show less

    Abstract

    With microwave-digestion as a sample decomposition technique and HNO3 and H2O2 as digestion reagent, the contents of Pb, Cd and Cr in surface decorating materials of wood-based panels were determined by atomic absorption spectrometry. The detection limit of Pb, Cd and Cr of FAAS is 0.12 μg·mL-1, 0.029 μg·L-1 and 0.146 μg·L-1; respectively, the cadmium detection limit of GFAAS is 0.157 μg·L-1. The precision of lead was between 0.8% and 3.0% and the recoveries ranged from 94% to 109.2%. The precision of cadmium was between 0.8% and 2.1%, and the recoveries ranged from 94.6% to 106.4%. The precision of chromium was between 1.8% and 4.9%, and the recoveries ranged from 98.8% to 107.7%. The method is accurate and reliable, and suitable and applicable to determining heavy metal of surface decorating materials of wood-based panels. The result is expected to provide scientific basis for establishing a corresponding Chinese national standard.
    LONG Ling, HUANG An-min, MENG Di, LU Zhi-gang. Determination of Pb, Cd and Cr in Surface Decorating Materials of Wood-Based Panels by Microwave Digestion-AAS[J]. Spectroscopy and Spectral Analysis, 2012, 32(9): 2572
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