Feng SUN, Qing-qing YAN, Lu WANG, Zhen-fei SUN. Study on the Conditions of Hydrothermal Synthesis of Chinese Purple BaCuSi2O6 and the Analysis of Its Products[J]. Spectroscopy and Spectral Analysis, 2021, 41(7): 2284
- Spectroscopy and Spectral Analysis
- Vol. 41, Issue 7, 2284 (2021)
Fig. 1. XRD patterns of samples at pH 7, 8, 9
a : pH 7; b : pH 8; c : pH 9
Fig. 1. XRD patterns of samples at pH 10, 11, 12
d : pH 10; e : pH 11; f : pH 12
Fig. 2. Samples of Chinese purple
(a): 160 ℃; (b): 180 ℃
(a): 160 ℃; (b): 180 ℃
Fig. 2. XRD patterns of samples at hydrothermal temperature of 120 and 140 ℃
a : 120 ℃; b : 140 ℃
Fig. 2. XRD patterns of samples at hydrothermal temperature of 160 and 180 ℃
c : 160 ℃; d : 180 ℃
Fig. 3. XRD patterns of samples with hydrothermal time of 12 and 24 hours
a : 12 h; b : 24 h; c : 48 h; d : 72 h
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