• Journal of Inorganic Materials
  • Vol. 37, Issue 3, 310 (2021)
Meng LI1、2, Hailu HUANG1、2, Jiamin WU1、2、*, Chunlei LIU1、2, Yaru WU1、2, Jingxian ZHANG3, and Yusheng SHI1、2
Author Affiliations
  • 11. State Key Laboratory of Materials Processing and Die & Mould Technology, School of Materials Science and Engineering, Huazhong University of Science and Technology, Wuhan 430074, China
  • 22. Engineering Research Center of Ceramic Materials for Additive Manufacturing, Ministry of Education, Wuhan 430074, China
  • 33. State Key Laboratory of High Performance Ceramics and Superfine Microstructure, Shanghai Institute of Ceramics, Chinese Academy of Sciences, Shanghai 200050, China
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    DOI: 10.15541/jim20210609 Cite this Article
    Meng LI, Hailu HUANG, Jiamin WU, Chunlei LIU, Yaru WU, Jingxian ZHANG, Yusheng SHI. Effect of Solid Loading of Slurry on Properties of Si3N4 Ceramics Formed by Digital Light Processing [J]. Journal of Inorganic Materials, 2021, 37(3): 310 Copy Citation Text show less

    Abstract

    With the continuous development of science and technology, Si3N4 ceramics are playing an increasingly important role in high-tech fields such as aviation machinery, biology and medical treatment. In this work, Si3N4 ceramics were successfully prepared by digital light processing (DLP) technology using Si3N4 powder coated with Al2O3-Y2O3 as raw material. Effects of solid loading of slurry on the performance of Si3N4 ceramic slurry, Si3N4 ceramic green parts and Si3N4 ceramics were systematically studied. The results showed that when the solid loading of slurry was less than 40.0% (in volume), its viscosity was less than 2 Pa·s at shear rate of 30 s-1, which can be used for DLP forming. In that case, the single curing depth of the slurry decreased with the increase of solid loading of the slurry, while the relative density and flexural strength of Si3N4 ceramics formed by DLP increased firstly and then decreased. The relative density and flexural strength reached the maximum of 89.8% and 162.5 MPa at solid loading of 37.5% (in volume), which were 10% and 16% higher than those with solid loading of 32.5% (in volume), respectively. In this work, the properties of Si3N4 ceramics formed by DLP were optimized by determining the best solid loading, which laid the experimental foundation for the photocuring of non-oxide ceramics such as Si3N4.
    Meng LI, Hailu HUANG, Jiamin WU, Chunlei LIU, Yaru WU, Jingxian ZHANG, Yusheng SHI. Effect of Solid Loading of Slurry on Properties of Si3N4 Ceramics Formed by Digital Light Processing [J]. Journal of Inorganic Materials, 2021, 37(3): 310
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