Synthesis of Zn, Mn doped Fe3O4 Nanoparticles with Tunable Size

Tian-Sheng CHENG; Jiong PAN; Ying-Ying XU; Qun-Qun BAO; Ping HU; Jian-Lin SHI

doi:10.15541/jim20190013

Journals >Journal of Inorganic Materials >Volume 34 >Issue 8 >Page 899 > Article

Journal of Inorganic Materials
Vol. 34, Issue 8, 899 (2019)

Synthesis of Zn, Mn doped Fe₃O₄ Nanoparticles with Tunable Size

Tian-Sheng CHENG^1、2、3, Jiong PAN⁴, Ying-Ying XU^1、2、3, Qun-Qun BAO^1、2、3, Ping HU^1、*, and Jian-Lin SHI^1、*

Author Affiliations

¹State Key Laboratory of High Performance Ceramics and Superfine Microstructures, Shanghai Institute of Ceramics, Chinese Academy of Sciences, Shanghai 200050, China

²University of Chinese Academy of Sciences, Beijing 100049, China

³Shanghai Tech University, Shanghai 201210, China

⁴Tongji University, Shanghai 200092, China

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DOI: 10.15541/jim20190013 Cite this Article

Tian-Sheng CHENG, Jiong PAN, Ying-Ying XU, Qun-Qun BAO, Ping HU, Jian-Lin SHI. Synthesis of Zn, Mn doped Fe₃O₄ Nanoparticles with Tunable Size[J]. Journal of Inorganic Materials, 2019, 34(8): 899 Copy Citation Text

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TEM images of ZnMn-Fe3O4 nanoparticles and histograms of their size distributions obtained by Fe(acac)3, Mn(acac)2 and Zn(acac)2 with (a, c) and without (b, d) adding 1,2-hexadecanediol

. TEM images of ZnMn-Fe₃O₄nanoparticles and histograms of their size distributions obtained by Fe(acac)₃, Mn(acac)₂and Zn(acac)₂ with (a, c) and without (b, d) adding 1,2-hexadecanediol

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$TEM image (a), histograms of their size distributions (b), high-resolution TEM image (c) and selected area electron diffraction (SAED) pattern (d) of 15 nm-sized ZnMn-Fe3O4 nanoparticles prepared from Fe(acac)3, MnCl2 and ZnCl2$

. TEM image (a), histograms of their size distributions (b), high-resolution TEM image (c) and selected area electron diffraction (SAED) pattern (d) of 15 nm-sized ZnMn-Fe₃O₄ nanoparticles prepared from Fe(acac)₃, MnCl₂ and ZnCl₂

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. TEM images of 20 nm-sized ZnMn-Fe₃O₄nanoparticles synthesized from Fe(acac)₃, MnCl₂ and ZnCl₂ with different reflux time durations of 1.5 h (a) and 2 h (b), and the corresponding histograms of size distributions of 1.5 h (c) and 2 h (d)

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. XRD patterns (a), FT-IR spectra (b) and energy dispersive X-ray spectroscopy (EDS) data (c) of 5 nm, 10 nm, 15 nm, and 20 nm-sized ZnMn-Fe₃O₄ nanoparticles

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. Magnetic hysteresis curve (a) and d^-1-dependent M_s curve (b) of 5-20 nm-sized ZnMn-Fe₃O₄ nanoparticles

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Tian-Sheng CHENG, Jiong PAN, Ying-Ying XU, Qun-Qun BAO, Ping HU, Jian-Lin SHI. Synthesis of Zn, Mn doped Fe₃O₄ Nanoparticles with Tunable Size[J]. Journal of Inorganic Materials, 2019, 34(8): 899

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