• Chinese Optics Letters
  • Vol. 20, Issue 6, 061601 (2022)
Oksana Semenova1、*, Aleksei Sosunov1, Nikolai Prokhorov1, and Roman Ponomarev1、2
Author Affiliations
  • 1Department of Nanotechnology and Microsystems Engineering, Perm State University, Perm 614990, Russia
  • 2Perm Federal Research Center of the Ural Branch of the Russian Academy of Sciences, Perm 614990, Russia
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    DOI: 10.3788/COL202220.061601 Cite this Article Set citation alerts
    Oksana Semenova, Aleksei Sosunov, Nikolai Prokhorov, Roman Ponomarev. Temperature dependence of LiNbO3 dislocation density in the near-surface layer[J]. Chinese Optics Letters, 2022, 20(6): 061601 Copy Citation Text show less
    Etching pits of LiNbO3 (a) after thermal annealing at 500°C and (b) in pristine state.
    Fig. 1. Etching pits of LiNbO3 (a) after thermal annealing at 500°C and (b) in pristine state.
    Dependence of the dislocation density N determined by wet selective etching on the annealing temperature T.
    Fig. 2. Dependence of the dislocation density N determined by wet selective etching on the annealing temperature T.
    AFM image of etch pits and the profile of etching pits (line 146).
    Fig. 3. AFM image of etch pits and the profile of etching pits (line 146).
    Dependence of ρ110/ρ220 for a single crystal of X-cut LN on the density of chaotically distributed dislocations N, X-ray Co-λβ-radiation.
    Fig. 4. Dependence of ρ110/ρ220 for a single crystal of X-cut LN on the density of chaotically distributed dislocations N, X-ray Co-λβ-radiation.
    Dependence of the dislocation density N (determined by the results of XRD) on the thermal annealing temperature T.
    Fig. 5. Dependence of the dislocation density N (determined by the results of XRD) on the thermal annealing temperature T.
    Thermal AnnealingSample ρ110/ρ220
    Pristine3.17
    400°C – 4 h3.26
    500°C – 4 h3.57
    600°C – 4 h3.55
    Table 1. The Experimental Ratio of the Integral Reflection Coefficients ρ110/ρ220
    Oksana Semenova, Aleksei Sosunov, Nikolai Prokhorov, Roman Ponomarev. Temperature dependence of LiNbO3 dislocation density in the near-surface layer[J]. Chinese Optics Letters, 2022, 20(6): 061601
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