In-situ monitoring of saccharides removal of alcohol precipitation using near-infrared spectroscopy

Hongxia Huang; Haibin Qu

doi:10.1142/s179354581850027x

[1] X. C. Gong, S. S. Wang, H. B. Qu, "Comparison of two separation technologies applied in the manufacture of botanical injections: Second ethanol precipitation and solvent extraction," Ind. Eng. Chem. Res. 50, 7542–7548 (2011).

[2] G. Eggleston, J. R. Vercellotti, "Degradation of sucrose, glucose and fructose in concentrated aqueous solutions under constant PH conditions at elevated temperature," J. Carbohydr. Chem. 19, 1305–1318 (2000).

[3] M. Coca, M. T. Garcia, G. Gonzalez, M. Pena, J. A. Garcia, "Study of colored components formed in sugar beet processing," Food Chem. 86, 421–433 (2004).

[4] B. Y. Yang, R. Montgomery, "Alkaline degradation of fructofuranosides," Carbohydr. Res. 280, 47–57 (1996).

[5] F. S. Asghari, H. Yoshida, "Acid-catalyzed production of 5-hydroxymethyl furfural from D-fructose in subcritical water," Ind. Eng. Chem. Res. 45, 2163–2173 (2006).

[6] I. Severin, C. Dumont, A. Jondeau-Cabaton, V. Graillot, M. C. Chagnon, "Genotoxic activities of the food contaminant 5-hydroxymethylfurfural using different in vitro bioassays," Toxicol. Lett. 192, 189– 194 (2010).

[7] G. Schmourlo, R. R. Mendonca-Filho, C. S. Alviano, S. Cost, "Screening of antifungal agents using ethanol precipitation and bioautography of medicinal and food plant," J. Ethnopharmacol. 96, 563–568 (2005).

[8] J. Huang, G. Kaul, C. S. Cai, R. Chatlapalli, P. Hernandez-Abad, K. Ghosh, A. Nagi, "Quality by design case study: An integrated multivariate approach to drug product and process development," Int. J. Pharm. 382, 23–32 (2009).

[9] H. X. Huang, H. B. Qu, "In-line monitoring of alcohol precipitation by near-infrared spectroscopy in conjunction with multivariate batch modeling," Anal. Chim. Acta. 707, 47–56 (2011).

[10] J. Xu, R. Q. Yue, J. Liu, H. M. Ho, T. Yi, H. B. Chen, Q. B. Han, "Structural diversity requires individual optimization of ethanol concentration in polysaccharide precipitation," Int. J. Biol. Macromol. 67, 205–209 (2014).

[11] J. Zídkova, J. Cabalkova, "Determination of saccharides in fruit juices by capillary electrophoresis and matrix-assisted laser desorption/ionization time-of-flight mass spectrometry," J. Mass Spectrom. 36, 417–421 (2001).

[12] B. Lai, M. R. Plan, M. P. Hodson, J. O. Kr€omer, "Simultaneous determination of sugars, carboxylates, alcohols and aldehydes from fermentations by high performance liquid chromatography," Fermentation 2, 6-1–6-7 (2016).

[13] L. Zhao, A. M. Chanon, N. Chattopadhyay, I. E. Dami, J. J. Blakeslee, "Quantification of carbohydrates in grape tissues using capillary zone electrophoresis," Front. Plant Sci. 7(818), 1–14 (2016).

[14] J. P. Higgins, S. M. Arrivo, G. Thurau, R. L. Green, W. Bowen, A. Lange, A. C. Templeton, D. L. Thomas, R. A. Reed, "Spectroscopic approach for on-line monitoring of particle size during the processing of pharmaceutical nanoparticles," Anal. Chem. 75, 1777–1785 (2003).

[15] U.S. Department of Health and Human Services et al., "Guidance for industry PAT: A framework for innovative pharmaceutical development, manufacturing, and quality assurance," http://www.fda. gov/downloads/Drugs/Guidances/ucm070305.pdf (2004).

[16] M. Blanco, J. Coello, H. Iturriaga, S. Maspoch, C. Pezuela, "Critical review near-infrared spectroscopy in the pharmaceutical industry," Analyst 123, 135R–150R (1998).

[17] E. W. Ciurczak, J. K. Drennen, Pharmaceutical and Medical Applications of Near-Infrared Spectroscopy, Marcel Dekker, New York (2002).

[18] X. Xiao, J. F. Ma, F. H. Ge, X. D. Zhang, H. H. Yang, Q. L. Liang, Y. M. Wang, G. A. Luo, "Application of near-infrared spectroscopy for the rapid analysis of Lonicerae Japonicae Flos solution extracted by water," J. Innov. Opt. Health Sci. 7(4), 1350069-1–1350069-9 (2014).

[19] C. Y. Wu, J. S. Chen, M. R. Li, Y. Wu, X. S. Liu, "Improvement of NIR models for quality parameters of leech and earthworm medicines using outlier multiple diagnoses," J. Innov. Opt. Health Sci. 11(1), 1750009-1–1750009-15 (2018).

[20] P. J. Brimmer, F. A. DeThomas, J. W. Hall, Method development and implementation of near-infrared spectroscopy in industrial manufacturing process, in Near-Infrared Technology in the Agriculture and Food Industries, pp. 199–214, American Association of Cereal Chemists, Inc., St. Paul, MN (2001).

[21] D. A. Burns, E. W. Ciurczak, Handbook of Near- Infrared Analysis, 2nd Edition, Practical Spectroscopy Series, Vol. 35, Marcel Dekker, New York (2001).

[22] J. Luypaert, D. L. Massart, Y. V. Heyden, "Nearinfrared spectroscopy applications in pharmaceutical analysis," Talanta 72, 865–883 (2007).

[23] ASTM, "ASTM Standard E2537-08: Standard guide for the application of continuous quality veri fication to pharmaceutical and biopharmaceutical manufacturing," ASTM International, West Conshohocken (2008).

[24] J. Huang, S. R. Torres, M. Moshgbar, "Practical considerations in data pre-treatment for NIR and Raman spectroscopy," Pharm. Rev. 6, 116–127 (2010).

[25] T. Hu, T. T. Li, L. Nie, L. X. Zang, H. C. Zang, Y. Z. Zeng, "Rapid monitoring the water extraction process of Radix Paeoniae Alba using near infrared spectroscopy," J. Innov. Opt. Health Sci. 10(3), 1750002-1–1750002-8 (2017).

[26] H. J. Chae, S. W. Chae, D. H. Yun, K. S. Keum, S. K. Yoo, H. R. Kim, "Prevention of bone loss in ovariectomized rats: The effect of Salvia miltiorrhiza extracts," Immunopharmacol. Immunotoxicol. 26(1), 135–144 (2004).

[27] A. H. Liu, L. Li, M. Xu, Y. H. Lin, H. Z. Guo, D. A. Guo, "Simultaneous quantification of six major phenolic acids in the roots of Salvia miltiorrhiza and four related traditional Chinese medicinal preparations by HPLC-DAD method," J. Pharma. Biomed. Anal. 41(1), 48–56 (2006).

[28] J. Z. Xu, J. Shen, Y. Y. Cheng, H. B. Qu, "Simultaneous detection of seven phenolic acids in Danshen injection using HPLC with ultraviolet detector," J. Zhejiang Univ., Sci. B 9(9), 728–733 (2008).

[29] R. Rosipal, N. Kr?mer, Overview and recent advances in partial least squares, Subspace, Latent Structure and Feature Selection, Lecture Notes in Computer Science, Vol. 3940, pp. 34–51, Springer, Berlin (2006).

[30] R. N. M. Pascoa, J. A. Lopes, J. L. F. C. Lima, "In situ near infrared monitoring of activated dairy sludge wastewater treatment processes," J. Near Infrared Spectrosc. 16(4), 409–419 (2008).

[31] P. Geladi, B. Kowalski, "Partial least squares regression: A tutorial," Anal. Chim. Acta. 185, 1–17 (1986).

[32] J. Mantanusa, E. Ziemonsa, P. Lebruna, E. Rozeta, R. Klinkenbergb, B. Streel, B. Evrard, Ph. Hubert, "Active content determination of non-coated pharmaceutical pellets by near infrared spectroscopy: Method development, validation and reliability evaluation," Talanta 80, 1750–1757 (2010).

[33] W. L. Li, H. B. Qu, "Characterization of herbal powder blends homogeneity using near-infrared spectroscopy," J. Innov. Opt. Health Sci. 7(6), 1450004-1–1450004-7 (2014).

[34] A. Nordon, A. Mills, R. T. Burn, F. M. Cusick, D. Littlejohn, "Comparison of non-invasive NIR and Raman spectrometries for determination of alcohol content of spirits," Anal. Chim. Acta. 548, 148–158 (2005).

[35] L. J. Xie, X. Q. Ye, D. H. Liu, Y. B. Ying, "Quantification of glucose, fructose and sucrose in bayberry juice by NIR and PLS," Food Chem. 114, 1135–1140 (2009).