• Journal of Inorganic Materials
  • Vol. 37, Issue 12, 1267 (2022)
Pingping LIU*, Xin ZHONG, Le ZHANG, Hong LI, Yaran NIU, Xiangyu ZHANG, Qilian LI, and Xuebin ZHENG
DOI: 10.15541/jim20220265 Cite this Article
Pingping LIU, Xin ZHONG, Le ZHANG, Hong LI, Yaran NIU, Xiangyu ZHANG, Qilian LI, Xuebin ZHENG. Molten Salt Corrosion Behaviors and Mechanisms of Ytterbium Silicate Environmental Barrier Coating[J]. Journal of Inorganic Materials, 2022, 37(12): 1267 Copy Citation Text show less
XRD patterns and SEM morphologies of as-sprayed Yb2SiO5/Yb2Si2O7/Si coating
. XRD patterns and SEM morphologies of as-sprayed Yb2SiO5/Yb2Si2O7/Si coating
Macro-photographs of Yb2SiO5/Yb2Si2O7/Si coating after molten salt corrosion for different time
. Macro-photographs of Yb2SiO5/Yb2Si2O7/Si coating after molten salt corrosion for different time
XRD patterns of Yb2SiO5/Yb2Si2O7/Si coating after molten salt corrosion for different time
. XRD patterns of Yb2SiO5/Yb2Si2O7/Si coating after molten salt corrosion for different time
Surface morphologies of Yb2SiO5/Yb2Si2O7/Si coating after molten salt corrosion for different time and correponding EDS analyses of different areas
. Surface morphologies of Yb2SiO5/Yb2Si2O7/Si coating after molten salt corrosion for different time and correponding EDS analyses of different areas
Cross-sectional morphologies and corresponding element analyses of Yb2SiO5 top layer after molten salt corrosion for different time
. Cross-sectional morphologies and corresponding element analyses of Yb2SiO5 top layer after molten salt corrosion for different time
Cross-sectional morphologies and corresponding EDS element mappings of Yb2SiO5/Yb2Si2O7/Si EBCs after molten salt corrosion for different time
. Cross-sectional morphologies and corresponding EDS element mappings of Yb2SiO5/Yb2Si2O7/Si EBCs after molten salt corrosion for different time
High-magnification cross-sectional morphologies and corresponding EDS mappings of infiltration zone in Yb2Si2O7 interlayer after molten salt corrosion for different time
. High-magnification cross-sectional morphologies and corresponding EDS mappings of infiltration zone in Yb2Si2O7 interlayer after molten salt corrosion for different time
Schematic diagrams of Yb2SiO5/Yb2Si2O7/Si coating under Na2SO4+25% NaCl molten salt corrosion at 900 ℃
. Schematic diagrams of Yb2SiO5/Yb2Si2O7/Si coating under Na2SO4+25% NaCl molten salt corrosion at 900 ℃
EPR spectra of Yb2SiO5 and Yb2Si2O7 coating
. EPR spectra of Yb2SiO5 and Yb2Si2O7 coating
Yb2SiO5Yb2Si2O7Si
Primary Ar/(L·min-1)465352
Secondary H2/(L·min-1)141013
Carrier Ar/(L·min-1)2.32.32.0
Spray distance/mm220220290
Table 1. Operating parameters used for vacuum plasma spraying
PositionYbSiNaO
121.6914.271.9862.06
224.9112.57-62.52
318.2918.09-63.62
410.1518.672.4158.77
522.5013.751.6762.08
624.9212.57-62.51
718.0318.31-63.66
88.9519.2513.2558.55
922.9313.202.0461.82
1024.4512.96-62.59
1117.8218.04-63.25
128.9119.2113.3958.49
Table 2. EDS elemental compositions of the marked regions in Fig. 7/%(in atom)
Pingping LIU, Xin ZHONG, Le ZHANG, Hong LI, Yaran NIU, Xiangyu ZHANG, Qilian LI, Xuebin ZHENG. Molten Salt Corrosion Behaviors and Mechanisms of Ytterbium Silicate Environmental Barrier Coating[J]. Journal of Inorganic Materials, 2022, 37(12): 1267
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