• Infrared and Laser Engineering
  • Vol. 54, Issue 2, 20240414 (2025)
Yaqian ZHANG, Yugang JIANG*, Jingsong RONG, Rongshi ZHANG..., Tong ZHANG and |Show fewer author(s)
Author Affiliations
  • Tianjin Key Laboratory of Optical Thin Film, Tianjin Jinhang Institute of Technical Physics, Tianjin 300308, China
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    DOI: 10.3788/IRLA20240414 Cite this Article
    Yaqian ZHANG, Yugang JIANG, Jingsong RONG, Rongshi ZHANG, Tong ZHANG, [in Chinese]. Effect of annealing treatment on the optical properties and residual stress of MgAl2O4[J]. Infrared and Laser Engineering, 2025, 54(2): 20240414 Copy Citation Text show less
    Annealing process curve of MgAl2O4 transparent ceramic sample
    Fig. 1. Annealing process curve of MgAl2O4 transparent ceramic sample
    Optical transmittance curve of annealed MgAl2O4 transparent ceramic sample
    Fig. 2. Optical transmittance curve of annealed MgAl2O4 transparent ceramic sample
    Cross-sectional morphology of MgAl2O4 transparent ceramic samples before and after annealing. (a) Unannealed; (b) Annealed at 1 300 ℃; (c) Annealed at 1 400 ℃; (d) Annealed at 1 500 ℃
    Fig. 3. Cross-sectional morphology of MgAl2O4 transparent ceramic samples before and after annealing. (a) Unannealed; (b) Annealed at 1 300 ℃; (c) Annealed at 1 400 ℃; (d) Annealed at 1 500
    Influence curve of porosity on material transmittance
    Fig. 4. Influence curve of porosity on material transmittance
    Influence curve of pore size on the optical transmittance of the material
    Fig. 5. Influence curve of pore size on the optical transmittance of the material
    Stress result of the annealed MgAl2O4 transparent ceramic samples
    Fig. 6. Stress result of the annealed MgAl2O4 transparent ceramic samples
    Raman spectra of MgAl2O4 powder and annealed transparent ceramic samples (excited by 785 nm laser)
    Fig. 7. Raman spectra of MgAl2O4 powder and annealed transparent ceramic samples (excited by 785 nm laser)
    Eg mode Raman peaks and their fitting curves of MgAl2O4 powder and annealed transparent ceramic samples
    Fig. 8. Eg mode Raman peaks and their fitting curves of MgAl2O4 powder and annealed transparent ceramic samples
    Effect of annealing temperature on the drift of Eg mode Raman peak of magnesium-aluminum spinel
    Fig. 9. Effect of annealing temperature on the drift of Eg mode Raman peak of magnesium-aluminum spinel
    X-ray diffraction spectra of MgAl2O4 powder and annealed transparent ceramic samples
    Fig. 10. X-ray diffraction spectra of MgAl2O4 powder and annealed transparent ceramic samples
    Samplesa
    MgAl2O4 powder8.08664
    No annealed8.07720
    800 ℃-5 h8.07724
    1150 ℃-5 h8.07746
    1200 ℃-5 h8.07822
    1250 ℃-5 h8.07849
    1300 ℃-5 h8.07912
    1350 ℃-5 h8.08002
    1400 ℃-5 h8.08133
    Table 1. Lattice constants of MgAl2O4 powder and annealed transparent ceramic samples
    Yaqian ZHANG, Yugang JIANG, Jingsong RONG, Rongshi ZHANG, Tong ZHANG, [in Chinese]. Effect of annealing treatment on the optical properties and residual stress of MgAl2O4[J]. Infrared and Laser Engineering, 2025, 54(2): 20240414
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