• Journal of Inorganic Materials
  • Vol. 37, Issue 12, 1275 (2022)
Xishi WU*, Yunzhou ZHU, Qing HUANG, and Zhengren HUANG
DOI: 10.15541/jim20220294 Cite this Article
Xishi WU, Yunzhou ZHU, Qing HUANG, Zhengren HUANG. Effect of Pore Structure of Organic Resin-based Porous Carbon on Joining Properties of Cf/SiC Composites[J]. Journal of Inorganic Materials, 2022, 37(12): 1275 Copy Citation Text show less
Microstructures of joints with different volumn densities ((a) 0.51, (b) 0.70, (b) 0.90) and (d) flexural strengths of the joined specimens
. Microstructures of joints with different volumn densities ((a) 0.51, (b) 0.70, (b) 0.90) and (d) flexural strengths of the joined specimens
Morphologies of the polished surfaces before and after HF-HNO3 corrosion of RBSC fabricated from preforms with different pore sizes
. Morphologies of the polished surfaces before and after HF-HNO3 corrosion of RBSC fabricated from preforms with different pore sizes
XRD patterns of the RBSC fabricated from preforms with different pore sizes
. XRD patterns of the RBSC fabricated from preforms with different pore sizes
Surface microstructures after HF-HNO3 corrosion of joining samples with different pore sizes
. Surface microstructures after HF-HNO3 corrosion of joining samples with different pore sizes
(a) Schematic of the action of inert filler and (b) volume shrinkage and porosity change curves of porous carbon blanks
. (a) Schematic of the action of inert filler and (b) volume shrinkage and porosity change curves of porous carbon blanks
Microstructures of the joint with different contents of inert filler ((a) 30%; (b) 40%; (c) 50%; (d) 55%, in mass) and (e) partial enlargement of (d)
. Microstructures of the joint with different contents of inert filler ((a) 30%; (b) 40%; (c) 50%; (d) 55%, in mass) and (e) partial enlargement of (d)
Flexural strength of the joined samples with different contents of inert filler
. Flexural strength of the joined samples with different contents of inert filler
SamplePF/%EG/%Pore former*Residual carbon**/% Average pore size/nmBulk density/(g·cm-3)
15050FeCl2 (1%)23+1.1190±150.73±0.01
25050H3BO3 (1.5%)24.3±0.9642±150.74±0.01
35050FeCl2 (1%) + H3BO3 (1.5%)24.1±1.71226±480.74±0.03
45050H3BO3 (2.5%)25.8±2.11552±380.79±0.03
55050H3BO3 (3.5%)26.7±1.52363±540.79±0.03
Table 1. Composition of resin solution and properties of porous carbons after pyrolysis
Pore size/nmOpen porosity/%Density/ (g·cm-3) Flexural strength/MPaResidual Si/(%, in volume)
1900.972.93296±2816
6421.262.91268±4614
12261.872.88248±2216
15523.512.81238±4412
236318.762.10115±3213
Table 2. Properties of the RBSC fabricated from preforms with different pore sizes
Pore size/nmFlexural strength/MPaStrength retention/%
1490±2861
190125±1285
31677±1052
642107±1573
122665±2244
Table 3. Properties of joining samples with different pore sizes
SamplePF/% EG/% Dispersant*/% Pore former**(FeCl2)/% α-SiCpowder/%
140404120
235354130
330304140
425254150
522.522.54155
Table 4. Composition of resin-based slurry
Xishi WU, Yunzhou ZHU, Qing HUANG, Zhengren HUANG. Effect of Pore Structure of Organic Resin-based Porous Carbon on Joining Properties of Cf/SiC Composites[J]. Journal of Inorganic Materials, 2022, 37(12): 1275
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