Multispectral Analysis on Lacquer Films of Boxes Excavated From Haiqu Cemetery During the Han Dynasties

Shuang-cheng WU; Pu CHENG; Ting-ting LI; Yang YANG; Fu-de TIE; Pu-jun JIN

doi:10.3964/j.issn.1000-0593(2022)04-1150-06

Journals >Spectroscopy and Spectral Analysis >Volume 42 >Issue 4 >Page 1150 > Article

Spectroscopy and Spectral Analysis
Vol. 42, Issue 4, 1150 (2022)

Multispectral Analysis on Lacquer Films of Boxes Excavated From Haiqu Cemetery During the Han Dynasties

Shuang-cheng WU^1、*, Pu CHENG^2、2;, Ting-ting LI^2、2;, Yang YANG^2、2;, Fu-de TIE^{1、1; *;}, and Pu-jun JIN^{2、2; *;}

Author Affiliations

¹1. School of Cultural Heritage, Northwest University, Xi’an 710069, China

²2. School of Materials Science and Engineering, Shaanxi Normal University, Xi’an 710119, China

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DOI: 10.3964/j.issn.1000-0593(2022)04-1150-06 Cite this Article

Shuang-cheng WU, Pu CHENG, Ting-ting LI, Yang YANG, Fu-de TIE, Pu-jun JIN. Multispectral Analysis on Lacquer Films of Boxes Excavated From Haiqu Cemetery During the Han Dynasties[J]. Spectroscopy and Spectral Analysis, 2022, 42(4): 1150 Copy Citation Text

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Fig. 1. Lacquer cosmetic box containing five small boxes excavated from M106 at the Haiqu Cemetery, Rizhao city, Shandong province

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Fig. 2. Microtomic lacquer slides from samples No.1-No.8

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$Measurement and analysis of Sample No.8(a): Raman spectrograms of red pigment; (b): XRD (X-ray powder diffraction) pattern of red pigment; (c), (d): Raman spectrogram of white flecks inlacquer plaster$

Fig. 3. Measurement and analysis of Sample No.8
(a): Raman spectrograms of red pigment; (b): XRD (X-ray powder diffraction) pattern of red pigment; (c), (d): Raman spectrogram of white flecks inlacquer plaster

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Fig. 4. The elemental distribution of lacquer boxes No.5 and No.8

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Fig. 5. The FTIR diagrams of lacquer film samples No.1-No.9

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Fig. 6. UV-Vis absorption spectra of for lacquer film samples No.1-No. 9

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编号	名称	墓葬	编号	名称	墓葬
No.1	奁盒残片	M106	No.5	奁盒残片	M128
No.2	圆盒残片	M106	No.6	奁盒残片	M217
No.3	圆奁盒残片	M118	No.7	梳盒残片	M224
No.4	长方形盒残片	M125	No.8	圆奁盒残片	M224

Table 1. List of lacquer box samples from Haiqu Cemetery, Rizhao city, Shandong Province

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样品编号	样品厚度	结果
No.1	4.0 mm	内为红褐色漆膜上绘暗色纹饰, 外髹黑色漆层。分为彩绘层、面漆层、底漆层与漆灰层。其中, 红色面漆层厚约15 μm, 底漆层厚约11 μm, 漆灰层厚13~25 μm。
No.2	1.9 mm	内壁, 分为面漆层、红色漆膜、底漆层与漆灰层。黑色面漆层厚约12 μm, 红色漆膜厚约63 μm, 底漆层厚约71 μm, 漆灰层厚约867 μm。
No.3	1.1 mm	外壁漆膜分为面漆层、底漆层及漆灰层。面漆层厚约31 μm, 底漆层厚34~48 μm, 漆灰层厚约296 μm。
No.4	2.8 mm	内壁, 分为红色漆膜层、底漆层和漆灰层。红色漆膜层厚约12 μm, 底漆层厚约22 μm, 漆灰层厚约316 μm。
No.5	4.0 mm	内壁, 分为面漆层、底漆层和漆灰层。面漆层厚约69 μm, 底漆层厚约111 μm, 漆灰层厚650~829 μm。
No.6	2.6 cm	内壁分为纹饰层、面漆层、底漆层和漆灰层。面漆层厚约37 μm, 底漆层厚约21 μm, 最下面漆灰层厚约881 μm。
No.7	2.9 mm	外壁髹黑褐色漆膜, 内壁为红色漆膜。内壁漆膜分为红色漆膜底漆层和漆灰层。其中, 红色漆膜厚约13μm, 底漆层厚约47 μm, 漆灰层厚约496 μm。
No.8	2.0 mm	内壁, 分为面漆层、底漆层和漆灰层。面漆层厚约65 μm, 底漆层厚约14 μm, 漆灰层厚约209 μm。

Table 2. Layer thickness of lacquer samples No.1-No.8

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编号	C	O	Na	Mg	Al	Si	S	K	Fe	P	Ca
No.5	69.19	23.56	0.08	0.07	0.58	0.51	0.23	0.01	5.01	0.28	0.48
No.8	51.52	32.20	0.26	0.32	3.13	6.92	0.44	0.60	4.42	0.01	0.16

Table 3. The element content of lacquer plaster analyzed by SEM/EDAX for No.5 and No.8

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