Fig. 1. Schematic of the integrated blackbody principle (a) A integrated blackbody formed by a sample on the cavity bottom coupled with the cavity wall, (b) a sample moved from the bottom to the mouth of the cavity
Fig. 2. Distributions of the radiance temperature of the integrated blackbody cavity at a nominal temperature of 1 000 ℃
Fig. 3. Simulation and validation results of the effective emissivity of the integrated blackbody
Fig. 4. Schematic of the emissivity measurement device using the integrated blackbody principle
Fig. 5. The spectral outputs of the integrated blackbody and the graphite material (a) The spectral outputs during the spectral emissivity measurement of a graphite material at a nominal temperature of 1 000 ℃ of the integrated blackbody, (b) The effective spectral outputs of the integrated blackbody and the graphite material in the measurement state at the nominal temperatures of 1 000 ℃, 1 300℃ and 1 500 ℃
Fig. 6. The measurement and comparison results of the infrared spectral emissivity of graphite
Fig. 7. Heat transfer model of a sample surface
Fig. 8. The maximum temperature drop evaluations of a graphite material
Fig. 9. Results of the SSE measurements
Fig. 10. Results of the linearity of the spectral responsivity
Fig. 11. Linearity correction coefficients of the spectral responsivity
不确定度主项 | 不确定度子项 | 评定方法 |
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集成黑体发射率 | | | | 集成黑体温场 | A | | 集成控温稳定性 | A | | 腔体材料辐射特性 | B | 观测因子比uK | | | | 辐射源尺寸效应 | B | | 距离效应 | B | 集成黑体-样品亮度比uRatio | | | | 光谱亮度比测量重复性 | A | | FTIR响应度非线性 | B | | FTIR噪声 | B | | FTIR波数准确性 | B | | FTIR波数重复性 | B | | FTIR短期稳定性 | B | | 环境杂散辐射 | A | 飞行动态温降修正因子uC | | | | LP4波长准确性 | B | | LP4滤波片带宽 | B | | LP4量程系数 | B | | LP4噪声 | B | | LP4辐射源尺寸效应 | B | | LP4短期稳定性 | B | | LP4非线性 | B | | 示值精度 | B | | 样品在腔底控温精度 | A | | 飞行温降 | A | | 样品定位精度 | B | | 控温重复性 | A |
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Table 1. Uncertainties and evaluation methods of the materials infrared spectral emissivity measurements using integrated blackbody principle
不确定度主项 | 不确定度子项 | u(1 000 ℃) /(%) | u(1 300 ℃) /(%) | u(1 500 ℃) /(%) |
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集成黑体发射率 | | | | | | 集成黑体温场 | 2.1 | 1.5 | 0.6 | | 集成黑体短期控温稳定性 | 0.01 | 0.01 | 0.01 | | 腔体材料辐射特性 | 0.1 | 0.1 | 0.1 | 观测因子比uK | | | | | | 辐射源尺寸效应 | 0.05 | 0.06 | 0.08 | | 距离效应 | 可忽略 | 可忽略 | 可忽略 | 集成黑体-样品亮度比uRatio | | | | | | 光谱亮度比测量重复性 | 0.2 | 0.3 | 0.6 | | FTIR响应度非线性 | 0.5 | 0.5 | 0.6 | | FTIR噪声 | 0.01 | 0.01 | 0.01 | | FTIR波数准确性 | 0.01 | 0.01 | 0.01 | | FTIR波数重复性 | 0.0003 | 0.0003 | 0.0003 | | FTIR短期稳定性 | 可忽略 | 可忽略 | 可忽略 | | 环境杂散辐射 | 0.001 | 0.001 | 0.001 | 飞行动态温降修正因子uC | | | | | | LP4波长准确性 | 可忽略 | 可忽略 | 可忽略 | | LP4滤波片带宽 | 可忽略 | 可忽略 | 可忽略 | | LP4量程系数 | 0.02 | 0.03 | 0.04 | | LP4噪声 | 0.01 | 0.02 | 0.02 | | LP4辐射源尺寸效应 | 0.06 | 0.08 | 0.12 | | LP4短期稳定性 | 0.1 | 0.13 | 0.17 | | LP4非线性 | 可忽略 | 可忽略 | 可忽略 | | 示值精度 | 可忽略 | 可忽略 | 可忽略 | | 样品在腔底控温精度 | 0.1 | 0.1 | 0.2 | | 飞行温降 | 1.79 | 3.32 | 4.61 | | 样品定位精度 | 0.002 | 0.002 | 0.002 | | 控温重复性 | 0.01 | 0.01 | 0.01 | 合成不确定度方正汇总行/(%),k=1 | 2.82 | 3.69 | 4.75 |
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Table 2. Summary of measurement uncertainties of the infrared spectral emissivity of the graphite material