• Journal of Infrared and Millimeter Waves
  • Vol. 40, Issue 2, 204 (2021)
Xu-Yao SONG, Wei DONG*, Yi-Jie PAN, Zun-Dong YUAN, and Xiao-Feng LU
Author Affiliations
  • Heat Division, National Institute of Metrology, Beijing 100029, China
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    DOI: 10.11972/j.issn.1001-9014.2021.02.011 Cite this Article
    Xu-Yao SONG, Wei DONG, Yi-Jie PAN, Zun-Dong YUAN, Xiao-Feng LU. The infrared spectral emissivity measurement of a graphite material in a high temperature range of 1000~1500℃ using integrated blackbody principle[J]. Journal of Infrared and Millimeter Waves, 2021, 40(2): 204 Copy Citation Text show less
    Schematic of the integrated blackbody principle (a) A integrated blackbody formed by a sample on the cavity bottom coupled with the cavity wall, (b) a sample moved from the bottom to the mouth of the cavity
    Fig. 1. Schematic of the integrated blackbody principle (a) A integrated blackbody formed by a sample on the cavity bottom coupled with the cavity wall, (b) a sample moved from the bottom to the mouth of the cavity
    Distributions of the radiance temperature of the integrated blackbody cavity at a nominal temperature of 1 000 ℃
    Fig. 2. Distributions of the radiance temperature of the integrated blackbody cavity at a nominal temperature of 1 000 ℃
    Simulation and validation results of the effective emissivity of the integrated blackbody
    Fig. 3. Simulation and validation results of the effective emissivity of the integrated blackbody
    Schematic of the emissivity measurement device using the integrated blackbody principle
    Fig. 4. Schematic of the emissivity measurement device using the integrated blackbody principle
    The spectral outputs of the integrated blackbody and the graphite material (a) The spectral outputs during the spectral emissivity measurement of a graphite material at a nominal temperature of 1 000 ℃ of the integrated blackbody, (b) The effective spectral outputs of the integrated blackbody and the graphite material in the measurement state at the nominal temperatures of 1 000 ℃, 1 300℃ and 1 500 ℃
    Fig. 5. The spectral outputs of the integrated blackbody and the graphite material (a) The spectral outputs during the spectral emissivity measurement of a graphite material at a nominal temperature of 1 000 ℃ of the integrated blackbody, (b) The effective spectral outputs of the integrated blackbody and the graphite material in the measurement state at the nominal temperatures of 1 000 ℃, 1 300℃ and 1 500 ℃
    The measurement and comparison results of the infrared spectral emissivity of graphite
    Fig. 6. The measurement and comparison results of the infrared spectral emissivity of graphite
    Heat transfer model of a sample surface
    Fig. 7. Heat transfer model of a sample surface
    The maximum temperature drop evaluations of a graphite material
    Fig. 8. The maximum temperature drop evaluations of a graphite material
    Results of the SSE measurements
    Fig. 9. Results of the SSE measurements
    Results of the linearity of the spectral responsivity
    Fig. 10. Results of the linearity of the spectral responsivity
    Linearity correction coefficients of the spectral responsivity
    Fig. 11. Linearity correction coefficients of the spectral responsivity
    不确定度主项不确定度子项评定方法
    集成黑体发射率uεb
    集成黑体温场A
    集成控温稳定性A
    腔体材料辐射特性B
    观测因子比uK
    辐射源尺寸效应B
    距离效应B
    集成黑体-样品亮度比uRatio
    光谱亮度比测量重复性A
    FTIR响应度非线性B
    FTIR噪声B
    FTIR波数准确性B
    FTIR波数重复性B
    FTIR短期稳定性B
    环境杂散辐射A
    飞行动态温降修正因子uC
    LP4波长准确性B
    LP4滤波片带宽B
    LP4量程系数B
    LP4噪声B
    LP4辐射源尺寸效应B
    LP4短期稳定性B
    LP4非线性B
    示值精度B
    样品在腔底控温精度A
    飞行温降A
    样品定位精度B
    控温重复性A
    Table 1. Uncertainties and evaluation methods of the materials infrared spectral emissivity measurements using integrated blackbody principle
    不确定度主项不确定度子项

    u(1 000 ℃)

    /(%)

    u(1 300 ℃)

    /(%)

    u(1 500 ℃)

    /(%)

    集成黑体发射率uεb
    集成黑体温场2.11.50.6
    集成黑体短期控温稳定性0.010.010.01
    腔体材料辐射特性0.10.10.1
    观测因子比uK
    辐射源尺寸效应0.050.060.08
    距离效应可忽略可忽略可忽略
    集成黑体-样品亮度比uRatio
    光谱亮度比测量重复性0.20.30.6
    FTIR响应度非线性0.50.50.6
    FTIR噪声0.010.010.01
    FTIR波数准确性0.010.010.01
    FTIR波数重复性0.00030.00030.0003
    FTIR短期稳定性可忽略可忽略可忽略
    环境杂散辐射0.0010.0010.001
    飞行动态温降修正因子uC
    LP4波长准确性可忽略可忽略可忽略
    LP4滤波片带宽可忽略可忽略可忽略
    LP4量程系数0.020.030.04
    LP4噪声0.010.020.02
    LP4辐射源尺寸效应0.060.080.12
    LP4短期稳定性0.10.130.17
    LP4非线性可忽略可忽略可忽略
    示值精度可忽略可忽略可忽略
    样品在腔底控温精度0.10.10.2
    飞行温降1.793.324.61
    样品定位精度0.0020.0020.002
    控温重复性0.010.010.01
    合成不确定度方正汇总行uεs/(%),k=12.823.694.75
    Table 2. Summary of measurement uncertainties of the infrared spectral emissivity of the graphite material
    Xu-Yao SONG, Wei DONG, Yi-Jie PAN, Zun-Dong YUAN, Xiao-Feng LU. The infrared spectral emissivity measurement of a graphite material in a high temperature range of 1000~1500℃ using integrated blackbody principle[J]. Journal of Infrared and Millimeter Waves, 2021, 40(2): 204
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