Researching

Journals
  • Advanced Photonics
  • Photonics Insights
  • Advanced Photonics Nexus
  • Photonics Research
  • Advanced Imaging
  • View All Journals
  • Chinese Optics Letters
  • High Power Laser Science and Engineering
    • Articles
  • Optics
  • Physics
  • Geography
  • View All Subjects
    • Conferences
  • CIOP
  • HPLSE
  • AP
  • View All Events
    • News
    About CLP
    Search by keywords or author
    Journals >Journal of Inorganic Materials >Volume 37 >Issue 10 >Page 1102 > Article
    • Journal of Inorganic Materials
    • Vol. 37, Issue 10, 1102 (2022)
    Synthesis of Orthorhombic Black Phosphorus by Chemical Vapor Transport Method
    Mingfu FU, Wen YANG, Jiabao LI, Shukang DENG, Qihang ZHOU, Xiaobo FENG, and Peizhi YANG*
    Author Affiliations
  • Key Laboratory of Renewable Energy Advanced Materials and Manufacturing Technology (Ministry of Education), Yunnan Normal University, Kunming 650500, China
    • show less
    DOI: 10.15541/jim20210805 Cite this Article
    Mingfu FU, Wen YANG, Jiabao LI, Shukang DENG, Qihang ZHOU, Xiaobo FENG, Peizhi YANG. Synthesis of Orthorhombic Black Phosphorus by Chemical Vapor Transport Method[J]. Journal of Inorganic Materials, 2022, 37(10): 1102 Copy Citation Text show less
    Photos of orthorhombic BP synthesized with different mineralizer components
    1. Photos of orthorhombic BP synthesized with different mineralizer components
    Download full size | View in the Article
    Pictures of orthorhombic BP synthesized under different w(Sn/I2) ratios and relationship between the yields of BP and w(Sn/I2)
    2. Pictures of orthorhombic BP synthesized under different w(Sn/I2) ratios and relationship between the yields of BP and w(Sn/I2)
    Download full size | View in the Article
    XRD patterns (a) of BP with different w(Sn/I2) and schematic diagram (b) of cell atoms and crystal planes of BP
    3. XRD patterns (a) of BP with different w(Sn/I2) and schematic diagram (b) of cell atoms and crystal planes of BP
    Download full size | View in the Article
    Raman characterizations of BP with different w(Sn/I2), and optical microscope image of Raman using the surface scan and its vibration mode
    4. Raman characterizations of BP with different w(Sn/I2), and optical microscope image of Raman using the surface scan and its vibration mode
    Download full size | View in the Article
    Component analysis of BP with different w(Sn/I2)
    5. Component analysis of BP with different w(Sn/I2)
    Download full size | View in the Article
    Surface morphologies and microstructures of BP with different ratios
    6. Surface morphologies and microstructures of BP with different ratios
    Download full size | View in the Article
    Experiment number Experimental materials Mass ratio of mineralizer
    1RP@Sn@I2w(Sn/I2)=2.51
    2RP@Pb@I2w(Pb/I2)=3.96
    3RP@Sn@SnI4w(Sn/I)=2.61
    4RP@I2-
    5RP@Sn@SnCl2w(Sn/Cl)=9.29
    6RP@SnI4w(Sn/I)=0.23
    Table 1. Preparation of BP by different mineralizers
    View in the Article
    Experiment numberRed phosphorus/mgw(Sn/I2)
    740056.77
    840031.39
    940020.84
    104009.20
    114003.18
    124001.17
    134000.47
    144000.41
    Table 2. Synthesis of BP via diverse mass ratios of w(Sn/I2)
    View in the Article
    Abstract
    Get PDF(in Chinese)
    Figures&Tables (8)
    Equations (0)
    References (18)
    Get Citation
    Copy Citation Text
    Mingfu FU, Wen YANG, Jiabao LI, Shukang DENG, Qihang ZHOU, Xiaobo FENG, Peizhi YANG. Synthesis of Orthorhombic Black Phosphorus by Chemical Vapor Transport Method[J]. Journal of Inorganic Materials, 2022, 37(10): 1102
    Download Citation
    Tools
    Share
    Save the article for my favorites
    Paper Information
    Recommended Topics
    laser devices and laser physics
    Lasers and Laser Optics
    Laser physics
    laser manufacturing
    Instrumentation, Measurement and Metrology