• Acta Physica Sinica
  • Vol. 68, Issue 2, 020701-1 (2019)
Yu-Kun Qin1, Hong-Yu Xiao1、*, Li-Na Liu1, Rui-Rui Sun1, Qiu-Bo Hu1, Zhi-Gang Bao1, Yong-Sheng Zhang1, Shang-Sheng Li2, and Xiao-Peng Jia3
Author Affiliations
  • 1Department of Mathematics and Physics, Luoyang Institute of Science and Technology, Luoyang 471023, China
  • 2School of Materials Science and Engineering, Henan Polytechnic University, Jiaozuo 454000, China
  • 3State Key Laboratory of Superhard Materials, Jilin University, Changchun 130012, China
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    DOI: 10.7498/aps.68.20181855 Cite this Article
    Yu-Kun Qin, Hong-Yu Xiao, Li-Na Liu, Rui-Rui Sun, Qiu-Bo Hu, Zhi-Gang Bao, Yong-Sheng Zhang, Shang-Sheng Li, Xiao-Peng Jia. Effects of seed crystal size on growth of gem-diamond single crystal[J]. Acta Physica Sinica, 2019, 68(2): 020701-1 Copy Citation Text show less
    Sample assembly to treat Gem-diamond single crystals.宝石级金刚石单晶的生长组装示意图
    Fig. 1. Sample assembly to treat Gem-diamond single crystals.宝石级金刚石单晶的生长组装示意图
    Optical photos of the diamonds using different seed-crystals in diameters: (a) 0.8 mm; (b) 1.5 mm; (c), (d) 2.2 mm.不同直径的籽晶生长金刚石大单晶的光学显微照片 (a) 0.8 mm; (b) 1.5 mm; (c), (d) 2.2 mm
    Fig. 2. Optical photos of the diamonds using different seed-crystals in diameters: (a) 0.8 mm; (b) 1.5 mm; (c), (d) 2.2 mm.不同直径的籽晶生长金刚石大单晶的光学显微照片 (a) 0.8 mm; (b) 1.5 mm; (c), (d) 2.2 mm
    Optical photos of the diamonds and the carbon source.金刚石大单晶及剩余碳源的光学显微照片
    Fig. 3. Optical photos of the diamonds and the carbon source.金刚石大单晶及剩余碳源的光学显微照片
    Curves between the limit growth rate and the synthesis time of the high quality diamonds with different diameters of the seed-crystals: (a) 0.8 mm; (b) 1.5 mm; (c) 2.2 mm.不同尺寸籽晶生长优质金刚石单晶的极限生长速度与合成时间关系曲线 (a) 0.8 mm; (b) 1.5 mm; (c) 2.2 mm
    Fig. 4. Curves between the limit growth rate and the synthesis time of the high quality diamonds with different diameters of the seed-crystals: (a) 0.8 mm; (b) 1.5 mm; (c) 2.2 mm.不同尺寸籽晶生长优质金刚石单晶的极限生长速度与合成时间关系曲线 (a) 0.8 mm; (b) 1.5 mm; (c) 2.2 mm
    Scanning electron microscope photographs of diamond single crystals using different seed-crystals in diameters.不同尺寸籽晶生长金刚石单晶的SEM测试结果
    Fig. 5. Scanning electron microscope photographs of diamond single crystals using different seed-crystals in diameters.不同尺寸籽晶生长金刚石单晶的SEM测试结果
    FTIR curves of diamond single crystals: (a) Diamond crystal of Fig. 2 (a); (b) diamond crystal of Fig. 2 (b); (c) diamond crystal of Fig. 2 (c).金刚石单晶的微区FTIR测试 (a) 图2(a)所示晶体; (b) 图2(b)所示晶体; (c) 图2(c)所示晶体
    Fig. 6. FTIR curves of diamond single crystals: (a) Diamond crystal of Fig. 2 (a); (b) diamond crystal of Fig. 2 (b); (c) diamond crystal of Fig. 2 (c). 金刚石单晶的微区FTIR测试 (a) 图2(a)所示晶体; (b) 图2(b)所示晶体; (c) 图2(c)所示晶体
    序号名称序号名称
    1叶蜡石块6导电金属片
    2白云石衬管7石墨发热管
    3反应容器8碳素源
    4触媒合金9金刚石单晶
    5导电石墨片10密封、导电堵头
    Table 1.

    Part names of gem-diamond sample assembly.

    宝石级金刚石单晶生长组装内各部件名称

    样品籽晶尺寸/mm晶体尺寸/mm生长速度/mg·h−1晶体品质
    图2(a)0.84.83.7优质
    图2(b)1.54.44.2优质
    图2(c)2.25.75.3优质、少量包裹体
    图2(d)2.25.46.1劣质、裂晶
    Table 2.

    Parameters and quality of gem-diamond single crystals.

    宝石级金刚石单晶的晶体参数及品质

    Yu-Kun Qin, Hong-Yu Xiao, Li-Na Liu, Rui-Rui Sun, Qiu-Bo Hu, Zhi-Gang Bao, Yong-Sheng Zhang, Shang-Sheng Li, Xiao-Peng Jia. Effects of seed crystal size on growth of gem-diamond single crystal[J]. Acta Physica Sinica, 2019, 68(2): 020701-1
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