The demand for developing atmospheric chemistry experiment courses is urgent, but the textbooks are relatively lacking. This paper introduces the concepts, characteristics and practice of the new textbook “Atmospheric Chemistry Experiment” edited by the School of Atmospheric Sciences, Sun Yat-sen University. This textbook highlights the characteristics of atmospheric science discipline, including basic standard experiments of meteorological departments with reference to national standard methods, and cutting-edge experimental technology methodologies by advantage of large instruments. The content basically covers the theoretical knowledge in atmospheric chemistry, and encourages independent design of experiments, aiming to help cultivate practical and innovative undergraduate talents in atmospheric sciences. This textbook can serve as teaching materials of atmospheric chemistry experiment, and is expected to provide perspectives into the construction of other related courses.