• Chinese Journal of Lasers
  • Vol. 51, Issue 10, 1002322 (2024)
Lanyun Qin1, Heda Wang1, Changfu Li2, Yuhang Ren2..., Chao Wang2 and Guang Yang1,*|Show fewer author(s)
Author Affiliations
  • 1School of Mechatronic Engineering, Shenyang Aerospace University, Shenyang 110136, Liaoning, China
  • 2Key Laboratory of Fundamental Science for National Defense of Aeronautical Digital Manufacturing Process of Shenyang Aerospace University, Shenyang 110136, Liaoning, China
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    DOI: 10.3788/CJL231572 Cite this Article Set citation alerts
    Lanyun Qin, Heda Wang, Changfu Li, Yuhang Ren, Chao Wang, Guang Yang. Influence of Base Material Microstructure on Liquation Cracks Sensitivity in Laser Deposition Repaired K4169 Alloy[J]. Chinese Journal of Lasers, 2024, 51(10): 1002322 Copy Citation Text show less
    Microstructure of base material (K4169 alloy in cast state) and micro-morphology of powder. (a) Microstructure of K4169 alloy in cast state; (b) micro-morphology of GH4169 spherical powder
    Fig. 1. Microstructure of base material (K4169 alloy in cast state) and micro-morphology of powder. (a) Microstructure of K4169 alloy in cast state; (b) micro-morphology of GH4169 spherical powder
    Schematics of laser deposition repair experiment. (a) Schematic of laser deposition repair; (b) schematic of laser deposition scanning path
    Fig. 2. Schematics of laser deposition repair experiment. (a) Schematic of laser deposition repair; (b) schematic of laser deposition scanning path
    Schematic of tensile specimens
    Fig. 3. Schematic of tensile specimens
    OM images of K4169 alloy base material in different heat treatment states. (a) Homogenization+solution+aging treated base material; (b) homogenization+hot isostatic pressing+solution+aging treated base material
    Fig. 4. OM images of K4169 alloy base material in different heat treatment states. (a) Homogenization+solution+aging treated base material; (b) homogenization+hot isostatic pressing+solution+aging treated base material
    SEM images of K4169 alloy base material in different heat treatment states. (a) Homogenization+solution+aging treated base material; (b) homogenization+hot isostatic pressing+solution+aging treated base material
    Fig. 5. SEM images of K4169 alloy base material in different heat treatment states. (a) Homogenization+solution+aging treated base material; (b) homogenization+hot isostatic pressing+solution+aging treated base material
    XRD patterns of K4169 alloy base material in different heat treatment states
    Fig. 6. XRD patterns of K4169 alloy base material in different heat treatment states
    Liquefaction cracks in the heat-affected zone of repaired specimens of K4169 alloy in different heat treatment states. (a) Homogenization+solution+aging treated alloy; (b) homogenization+hot isostatic pressing+solution+aging treated alloy
    Fig. 7. Liquefaction cracks in the heat-affected zone of repaired specimens of K4169 alloy in different heat treatment states. (a) Homogenization+solution+aging treated alloy; (b) homogenization+hot isostatic pressing+solution+aging treated alloy
    Microstructures of heat-affected zone of repaired specimen of homogenization+solution+aging treated K4169 alloy
    Fig. 8. Microstructures of heat-affected zone of repaired specimen of homogenization+solution+aging treated K4169 alloy
    Liquation cracks in heat-affected zone of repaired specimen of homogenization+hot isostatic pressing+solution+aging treated K4169 alloy. (a) Overall crack morphology; (b)(c)(d) magnified view of cracks in different zones
    Fig. 9. Liquation cracks in heat-affected zone of repaired specimen of homogenization+hot isostatic pressing+solution+aging treated K4169 alloy. (a) Overall crack morphology; (b)(c)(d) magnified view of cracks in different zones
    Distribution of elements near liquation cracks in repaired specimen of homogenization+hot isostatic pressing+solution+aging treated K4169 alloy
    Fig. 10. Distribution of elements near liquation cracks in repaired specimen of homogenization+hot isostatic pressing+solution+aging treated K4169 alloy
    Liquation crack generation mechanism for repaired specimen of homogenization+hot isostatic pressing+solution+aging treated K4169 alloy, where image Ⅰ shows phase dissolution stage, image Ⅱ shows eutectic liquefaction stage, and image Ⅲ shows eutectic solidification stage
    Fig. 11. Liquation crack generation mechanism for repaired specimen of homogenization+hot isostatic pressing+solution+aging treated K4169 alloy, where image Ⅰ shows phase dissolution stage, image Ⅱ shows eutectic liquefaction stage, and image Ⅲ shows eutectic solidification stage
    Liquid film generation mechanism for repaired specimen of homogenization+solution+aging treated K4169 alloy, where image Ⅰ shows phase dissolution stage, image Ⅱ shows eutectic liquefaction stage, and image Ⅲ shows eutectic solidification stage
    Fig. 12. Liquid film generation mechanism for repaired specimen of homogenization+solution+aging treated K4169 alloy, where image Ⅰ shows phase dissolution stage, image Ⅱ shows eutectic liquefaction stage, and image Ⅲ shows eutectic solidification stage
    Microhardness of K4169 alloy repaired specimens with different heat treatment states
    Fig. 13. Microhardness of K4169 alloy repaired specimens with different heat treatment states
    Tensile results of repaired specimens of K4169 alloy in different heat treatment states
    Fig. 14. Tensile results of repaired specimens of K4169 alloy in different heat treatment states
    No.Heat treatmentDetail process
    1Homogenization+solution+aging1065 ℃/1.5 h,AC+980 ℃/1 h,AC+720 ℃/8 h(50 ℃/h,FC)to 620 ℃/8 h,AC
    2Homogenization+hot isotropic pressing +solution+aging1065 ℃/1.5 h,AC+1260 ℃/140 MPa/4 h,AC+980 ℃/ 1h,AC+720 ℃/8 h(50 ℃/h,FC)to 620 ℃/8 h,AC
    Table 1. Heat treatment of K4169 alloy
    MaterialMass fraction /%
    CrNiMoAlTiNbC
    K416919.249.43.30.50.844.4≤0.1
    GH416917‒2150‒552.8‒3.30.2‒0.60.65‒1.154.4‒5.40.063
    Table 2. Chemical composition of K4169 alloy and GH4169 spherical powder
    ParameterValue
    Power /W1600
    Scanning speed /(mm/s)8
    Feeding rate /(rad/min)1
    Layer thickness /mm0.4
    Overlap rate /%40
    Table 3. Laser deposition repair (LDR) parameters
    Regions in Fig. 5Atomic fraction /%Phase
    CAlSiTiCrFeNiNbMo
    A34.870.260.031.793.783.8443.7410.880.81Laves
    B22.930.980.141.1216.2913.9740.272.721.58δ
    C59.610.030.036.070.400.321.1032.190.24(Nb,Ti)C
    D61.090.040.014.690.710.591.5231.340(Nb,Ti)C
    E18.821.000.120.9417.6115.1042.472.421.52δ
    Table 4. EDS results of precipitates in K4169 alloy in different heat treatment states
    Lanyun Qin, Heda Wang, Changfu Li, Yuhang Ren, Chao Wang, Guang Yang. Influence of Base Material Microstructure on Liquation Cracks Sensitivity in Laser Deposition Repaired K4169 Alloy[J]. Chinese Journal of Lasers, 2024, 51(10): 1002322
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