• Acta Physica Sinica
  • Vol. 69, Issue 10, 104101-1 (2020)
Jun-Liang Yang1、3, Zhong-Liang Li2、*, Tang Li1、3, Ye Zhu1、3, Li Song2, Lian Xue2, and Xiao-Wei Zhang1、*
Author Affiliations
  • 1Beijing Synchrotron Radiation Facility, Institute of High Energy Physics, Chinese Academy of Sciences, Beijing 100049, China
  • 2Shanghai Synchrotron Radiation Facility, Shanghai Advanced Research Institute, Chinese Academy of Sciences, Shanghai 200120, China
  • 3University of Chinese Academy of Sciences, Chinese Academy of Sciences, Beijing 100049, China
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    DOI: 10.7498/aps.69.20200165 Cite this Article
    Jun-Liang Yang, Zhong-Liang Li, Tang Li, Ye Zhu, Li Song, Lian Xue, Xiao-Wei Zhang. Characteristics of multi-crystals monfiguration X-ray diffraction and application in characterizing synchrotron beamline bandwidth[J]. Acta Physica Sinica, 2020, 69(10): 104101-1 Copy Citation Text show less
    DuMond diagram for the symmetric Bragg geometry. The differential equation (2) of diffraction formula corresponds to the line band with a slope of . and represent the kinematic diffraction angle and the Darwin width of the dynamic diffraction, respectively. In this article, we ignore the change of X-ray diffraction angle position which is influenced by crystal refraction. When the incident white beam is completely parallel, both the receiving and emitting angle of the symmetric crystal are the same, which can be represented by . The limited angle broadband introduces the corresponding wavelength distribution . When the incident beam with a divergence angle, the distribution of the incident angle on the crystal becomes larger which affects the angular divergence of bandwidth changing from to (the divergence angle of the beam) and the wavelength distribution changing to
    Fig. 1. DuMond diagram for the symmetric Bragg geometry. The differential equation (2) of diffraction formula corresponds to the line band with a slope of . and represent the kinematic diffraction angle and the Darwin width of the dynamic diffraction, respectively. In this article, we ignore the change of X-ray diffraction angle position which is influenced by crystal refraction. When the incident white beam is completely parallel, both the receiving and emitting angle of the symmetric crystal are the same, which can be represented by . The limited angle broadband introduces the corresponding wavelength distribution . When the incident beam with a divergence angle, the distribution of the incident angle on the crystal becomes larger which affects the angular divergence of bandwidth changing from to (the divergence angle of the beam) and the wavelength distribution changing to
    The experimental configuration of (+1, –1) type non-dispersive consists of the second crystal of Si111-DCM and Si111 analyzer. The[111] is the crystal direction of the normal of the diffraction plane.
    Fig. 2. The experimental configuration of (+1, –1) type non-dispersive consists of the second crystal of Si111-DCM and Si111 analyzer. The[111] is the crystal direction of the normal of the diffraction plane.
    The experimental configuration of (+1, +1) type dispersive consists of the second crystal of Si111-DCM and Si111 analyzer.
    Fig. 3. The experimental configuration of (+1, +1) type dispersive consists of the second crystal of Si111-DCM and Si111 analyzer.
    DuMond diagrams during scanning the output beam of DCM by analyzer. Panel (a) represents the non-dispersive (+1, –1) configuration and panel (b) represents the dispersive (+1, +1) configuration. The oblique line region is the DuMond window of the DCM. The point region is the DuMond window of the analyzer.
    Fig. 4. DuMond diagrams during scanning the output beam of DCM by analyzer. Panel (a) represents the non-dispersive (+1, –1) configuration and panel (b) represents the dispersive (+1, +1) configuration. The oblique line region is the DuMond window of the DCM. The point region is the DuMond window of the analyzer.
    The experimental configuration of (+1, –3) type dispersive consists of the second crystal of Si111-DCM and Si333 analyzer.
    Fig. 5. The experimental configuration of (+1, –3) type dispersive consists of the second crystal of Si111-DCM and Si333 analyzer.
    The experimental configuration of (+1, +3) type dispersive consists of the second crystal of Si111-DCM and Si333 analyzer.
    Fig. 6. The experimental configuration of (+1, +3) type dispersive consists of the second crystal of Si111-DCM and Si333 analyzer.
    DuMond diagrams during scanning the output beam of DCM by Si(333) analyzer. Panel (a) and (b) represent the (+1, –3) typeand (+1, +3) type dispersive configuration, respectively. The green dotted arrow indicates the scanning process. The two point-regions give the starting and ending position of the DuMond window of the analyzer.
    Fig. 7. DuMond diagrams during scanning the output beam of DCM by Si(333) analyzer. Panel (a) and (b) represent the (+1, –3) typeand (+1, +3) type dispersive configuration, respectively. The green dotted arrow indicates the scanning process. The two point-regions give the starting and ending position of the DuMond window of the analyzer.
    (a) and (b) give the rocking curves of the Si (111) analyzer with different slit vertical widths under the conditions of non-dispersion configuration and “fixed dispersion” configuration, respectively. (c) gives the FWHM curve of the rocking curve when the slit vertical width is adjusted under the condition of non-dispersion configuration and “fixed dispersion” configuration.
    Fig. 8. (a) and (b) give the rocking curves of the Si (111) analyzer with different slit vertical widths under the conditions of non-dispersion configuration and “fixed dispersion” configuration, respectively. (c) gives the FWHM curve of the rocking curve when the slit vertical width is adjusted under the condition of non-dispersion configuration and “fixed dispersion” configuration.
    (a) and (b) show the results of slit width difference of rocking curve with (+1, –1) and (+1, +1) experimental configurations with Si111 analyzer, respectively. The coordinate origin of the transverse axis corresponds to the diffraction angle of the analytic crystal at 10 keV. Also, (b) is the DuMond diagram without slit (angle) - wavelength conversion obtained using Si111 analyzer under the condition of dispersion configuration. The measured values of rocking curve FWHM with different slit widths can be read directly from the figure.
    Fig. 9. (a) and (b) show the results of slit width difference of rocking curve with (+1, –1) and (+1, +1) experimental configurations with Si111 analyzer, respectively. The coordinate origin of the transverse axis corresponds to the diffraction angle of the analytic crystal at 10 keV. Also, (b) is the DuMond diagram without slit (angle) - wavelength conversion obtained using Si111 analyzer under the condition of dispersion configuration. The measured values of rocking curve FWHM with different slit widths can be read directly from the figure.
    (a) and (b) give the pseudo DuMond diagram using Si333 analyzer under the condition of (+1, –3) type and (+1, +3) type dispersion configuration, respectively.
    Fig. 10. (a) and (b) give the pseudo DuMond diagram using Si333 analyzer under the condition of (+1, –3) type and (+1, +3) type dispersion configuration, respectively.
    分析器衍射面实验配置色散类别测量值退卷积和色散展宽值理论值备注
    (111)(+n, –n) 无色散7.64(4)5.40(4)5.38双晶单色器带宽
    (+n, +n) “固定”色散52(1)26(1)
    (333)(+n, –m) “弱”色散67(1)26(1)25.8光束的带宽
    (+n, +m) “强”色散117(1)26(1)
    Table 1. The experimental values obtained from different experimental configurations and the values after deconvolution of the analyzer and removal of dispersion broadening. Unit: arcsec.
    Jun-Liang Yang, Zhong-Liang Li, Tang Li, Ye Zhu, Li Song, Lian Xue, Xiao-Wei Zhang. Characteristics of multi-crystals monfiguration X-ray diffraction and application in characterizing synchrotron beamline bandwidth[J]. Acta Physica Sinica, 2020, 69(10): 104101-1
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