• Chinese Journal of Lasers
  • Vol. 50, Issue 4, 0402009 (2023)
Tianchun Zou, Siyuan Mei*, and Minying Chen
Author Affiliations
  • College of Safety Science and Engineering, Civil Aviation University of China, Tianjin 300300, China
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    DOI: 10.3788/CJL220736 Cite this Article Set citation alerts
    Tianchun Zou, Siyuan Mei, Minying Chen. Microstructure and Electrochemical Corrosion Properties of AlMgScZr Alloys Fabricated Using Selective Laser Melting[J]. Chinese Journal of Lasers, 2023, 50(4): 0402009 Copy Citation Text show less
    AlMgScZr alloy powder. (a) Morphology of powder; (b) size distribution
    Fig. 1. AlMgScZr alloy powder. (a) Morphology of powder; (b) size distribution
    Relative densities of specimens fabricated under different scanning speeds
    Fig. 2. Relative densities of specimens fabricated under different scanning speeds
    Microstructures of longitudinal section of AlMgScZr alloy formed at 1200 mm/s scanning speed. (a) OM image; (b) SEM image
    Fig. 3. Microstructures of longitudinal section of AlMgScZr alloy formed at 1200 mm/s scanning speed. (a) OM image; (b) SEM image
    TEM images of longitudinal section of AlMgScZr alloy formed at 1200 mm/s scanning speed. (a) Bright-field image; (b) local enlargement of Fig. 4(a); (c) precipitated phase in fine grain region and its corresponding HRTRM image and FFT image; (d) precipitated phase in coarse grain region and its corresponding HRTEM image and FFT image
    Fig. 4. TEM images of longitudinal section of AlMgScZr alloy formed at 1200 mm/s scanning speed. (a) Bright-field image; (b) local enlargement of Fig. 4(a); (c) precipitated phase in fine grain region and its corresponding HRTRM image and FFT image; (d) precipitated phase in coarse grain region and its corresponding HRTEM image and FFT image
    IPFs and grain size distributions of different specimens. (a)(c) IPFs; (d)(f) grain size distributions
    Fig. 5.

    IPFs and grain size distributions of different specimens. (a) (c) IPFs; (d) (f) grain size distributions

    Grain boundary mappings and grain boundary misorientation angle distributions of different specimens. (a)(c) Grain boundary mappings; (d)(f) grain boundary misorientation angle distributions
    Fig. 6.

    Grain boundary mappings and grain boundary misorientation angle distributions of different specimens. (a) (c) Grain boundary mappings; (d) (f) grain boundary misorientation angle distributions

    Potentiodynamic polarization curves for specimens #1, #2, #3 in NaCl solution with mass fraction of 3.5%
    Fig. 7. Potentiodynamic polarization curves for specimens #1, #2, #3 in NaCl solution with mass fraction of 3.5%
    EIS measurement results. (a) Nyquist plot; (b)(c) Bode plots; (d) equivalent circuit model
    Fig. 8. EIS measurement results. (a) Nyquist plot; (b)(c) Bode plots; (d) equivalent circuit model
    Corrosion morphologies of specimens. (a) OM image of corrosion morphology; (b) SEM image of corrosion morphology of specimen #1; (c) SEM image of corrosion morphology of specimen #2; (d) SEM image of corrosion morphology of specimen #3
    Fig. 9. Corrosion morphologies of specimens. (a) OM image of corrosion morphology; (b) SEM image of corrosion morphology of specimen #1; (c) SEM image of corrosion morphology of specimen #2; (d) SEM image of corrosion morphology of specimen #3
    ElementMgScZrMnFeAl
    Mass fraction /%4.840.820.280.570.06Bal.
    Table 1. Chemical compositions of AlMgScZr alloy
    Process parameterValue
    Laser power /W375
    Scanning speed /(mm/s)800,1000,1200,1400,1600
    Hatch spacing /μm120
    Layer thickness /μm30
    Table 2. Process parameters for SLM forming
    Specimenicorr /(μA·cm-2βa-βcEpit /VRp /(Ω·cm2
    Specimen #131.29393.06148.40-0.6711528.25
    Specimen #214.48890.39151.00-0.6454165.80
    Specimen #323.91482.71123.11-0.6611795.75
    Table 3. Fitting results corresponding to Fig. 7
    SpecimenRs /(Ω·cm2Rf /(kΩ·cm2

    CPE1 /

    (10-6 F·cm-2

    n1

    Rct /

    (kΩ·cm2

    CPE2 /

    (10-4 F·cm-2

    n2χ2 /10-3
    Specimen #111.3328.329.580.8843.784.270.842.61
    Specimen #210.3482.206.800.89237.248.780.751.46
    Specimen #39.5543.927.700.9259.612.530.841.22
    Table 4. Fitting results corresponding to Fig. 8
    Tianchun Zou, Siyuan Mei, Minying Chen. Microstructure and Electrochemical Corrosion Properties of AlMgScZr Alloys Fabricated Using Selective Laser Melting[J]. Chinese Journal of Lasers, 2023, 50(4): 0402009
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