Author Affiliations
1College of Mechanical Engineering, University of Shanghai for Science and Technology, Shanghai 200093, China2Shanghai Aerospace Equipments Manufacturer Co., Ltd., Shanghai 200245, Chinashow less
Fig. 1. Transport diagram of heterogeneous alloy powder, as well as morphology and particle size distributions of two kinds of powders. (a) Schematic diagram of synchronous delivery of heterogeneous alloy powder; (b) micro-morphology of Ti6Al4V powder; (c) particle size distribution of Ti6Al4V powder; (d) micro-morphology of Ni55.5Ti44.5 powder; (e) particle size distribution of Ni55.5Ti44.5 powder
Fig. 2. Gradient compositional design of Ti6Al4V/NiTi heterogeneous alloy prepared by in-situ additive manufacturing
Fig. 3. XRD spectra and macroscopic morphology of Ti6Al4V/NiTi composites thin-walled samples with 11 compositional ratios. (a) XRD spectra; (b) macroscopic morphology
Fig. 4. Microstructures of Ti6Al4V/NiTi composites thin-walled samples with different composition ratios
Fig. 5. Elemental mass fraction changing of Ti6Al4V/NiTi thin-walled samples with different composition ratios
Fig. 6. In-situ gradient additive manufacturing of Ti6Al4V/NiTi heterogeneous functional materials. (a) Macroscopic morphology of formed part; (b) planer surface and partial enlargement of gradient transition zone of formed sample
Fig. 7. EDS line scan results near Ti6Al4V/NiTi gradient alloy interfaces. (a) Interfaces 1 and 2; (b) interface 3; (c) interface 4; (d) interface 5
Fig. 8. Schematic diagram of microhardness measurement points and distribution of measurement results for Ti6Al4V/NiTi gradient alloy. (a) Schematic diagram of sampling measurement points; (b) distribution of microhardness measurement results
No. | Ingredient ratio (mass fraction) | P /W | S /(mm/s) | F /(g/min) | FTi6Al4V / (g/min) | FNiTi / (g/min) | Interlayerlift /mm | Number ofprint layers | Substrate |
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1 | 100%Ti6Al4V | 1292 | 8.79 | 5.19 | 5.19 | | 0.56 | 18 | Ti6Al4V | 2 | 90%Ti6Al4V+10%NiTi | 1292 | 8.79 | 5.58 | 5.02 | 0.56 | 0.53 | 18 | Ti6Al4V | 3 | 80%Ti6Al4V+20%NiTi | 1292 | 8.79 | 6.03 | 4.82 | 1.21 | 0.54 | 18 | Ti6Al4V | 4 | 70%Ti6Al4V+30%NiTi | 1292 | 8.79 | 6.55 | 4.59 | 1.97 | 0.56 | 18 | Ti6Al4V | 5 | 60%Ti6Al4V+40%NiTi | 1292 | 8.79 | 7.18 | 4.31 | 2.87 | 0.61 | 16 | Ti6Al4V | 6 | 50%Ti6Al4V+50%NiTi | 1292 | 8.79 | 7.93 | 3.97 | 3.97 | 0.75 | 14 | NiTi | 7 | 40%Ti6Al4V+60%NiTi | 1292 | 8.79 | 8.87 | 3.55 | 5.32 | 0.78 | 12 | NiTi | 8 | 30%Ti6Al4V+70%NiTi | 1292 | 8.79 | 10.05 | 3.02 | 7.04 | 0.79 | 12 | NiTi | 9 | 20%Ti6Al4V+80%NiTi | 1292 | 8.79 | 11.60 | 2.32 | 9.28 | 0.85 | 12 | NiTi | 10 | 10%Ti6Al4V+90%NiTi | 1292 | 8.79 | 13.72 | 1.37 | 12.35 | 0.96 | 10 | NiTi | 11 | 100%NiTi | 1292 | 8.79 | 16.78 | | 16.78 | 1.26 | 8 | NiTi |
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Table 1. Process parameters corresponding to different composition ratios
SEM morphology | Position | Atomic fraction /% | Possible phase |
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Ti | Ni | Al | V |
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| Region A | 46.3 | 52.4 | 1.0 | 0.3 | | Point A1 | 47.4 | 51.8 | 0.5 | 0.3 | NiTi+Ni3Ti | Point A2 | 46.7 | 52.8 | 0.3 | 0.2 | NiTi+Ni3Ti | Region B | 48.3 | 50.8 | 0.7 | 0.2 | | Point B1 | 48.1 | 51.0 | 0.5 | 0.4 | NiTi | | Region C | 49.5 | 49.4 | 0.8 | 0.3 | | Point C1 | 55.5 | 42.0 | 1.3 | 1.2 | NiTi+NiTi2 | Region D | 53.5 | 44.7 | 1.0 | 0.8 | | Point D1 | 53.7 | 43.9 | 1.5 | 0.9 | NiTi+NiTi2 | | Region E | 54.5 | 43.1 | 1.3 | 1.1 | | Point E1 | 53.9 | 43.9 | 1.3 | 0.8 | NiTi+NiTi2 | Region F2 | 62.1 | 34.8 | 1.8 | 1.3 | | Point F2 | 61.5 | 35.3 | 2.0 | 1.2 | NiTi2 | Region F | 61.0 | 35.8 | 2.1 | 1.1 | | Point F1 | 60.6 | 36.2 | 2.0 | 1.2 | NiTi2 | | Region G | 61.2 | 35.6 | 2.2 | 1.1 | | Point G1 | 61.7 | 35.7 | 1.6 | 1.0 | NiTi2 | Region H | 83.8 | 8.8 | 4.7 | 2.7 | | Point H1 | 82.9 | 9.3 | 4.4 | 3.5 | α-Ti+NiTi2 | Region I | 90.7 | 0.1 | 5.2 | 4.0 | | Point I1 | 91.0 | 0 | 5.3 | 3.7 | α-Ti+β-Ti |
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Table 2. SEM observation and EDS analysis of Ti6Al4V/NiTi gradient alloy