Author Affiliations
1School of Mechanical Engineering, Zhejiang University of Technology, Hangzhou 310023, Zhejiang , China2Laser Advanced Manufacturing Research Institute, Zhejiang University of Technology, Hangzhou 310023, Zhejiang , China3High-End Laser Manufacturing Equipment Province and Ministry Jointly Established Collaborative Innovation Center, Hangzhou 310023, Zhejiang , Chinashow less
Fig. 1. Flowchart of laser remelting/electrochemical deposition interaction experiment
Fig. 2. Schematic of electrochemical deposition device
Fig. 3. SEM morphologies of surface after laser treatment. (a) After laser melting pretreatment; (b) after laser remelting
Fig. 4. SEM morphologies of deposited layer surface under laser remelting/electrochemical deposition interaction treatment and conventional electrodeposition process, where the “10” in the figure represents electrodeposition for 10 min and the letter “L” represents laser remelting. (a) Electrodeposition 10 min after laser melting pretreatment; (b) electrodeposition 10 min after the first laser remelting treatment; (c) electrodeposition 10 min after the second laser remelting treatment; (d) conventional electrodeposition for 30 min
Fig. 5. Distribution interval of particle size scale of deposited layer under laser remelting/electrochemical deposition interaction treatment and conventional electrodeposition process. (a) Interactive treatment; (b) conventional electrodeposition
Fig. 6. Surface roughness of deposited layer under laser remelting/electrochemical deposition interaction treatment and conventional electrodeposition process. (a) Interactive treatment; (b) conventional electrodeposition
Fig. 7. Element distribution of cross-section under laser remelting/electrochemical deposition interaction treatment. (a) Electrodeposition 10 min after laser melting pretreatment; (b) electrodeposition 10 min after the first laser remelting treatment; (c) electrodeposition 10 min after the second laser remelting treatment
Fig. 8. Section thickness of deposited layer under laser remelting/electrochemical deposition interaction treatment and traditional electrodeposition process. (a) Electrodeposition 10 min after laser melting pretreatment; (b) electrodeposition 10 min after the first laser remelting treatment; (c) electrodeposition 10 min after the second laser remelting treatment; (d) conventional electrodeposition for 30 min
Fig. 9. XRD phase analysis of composite remelting layer (Ti/Cu composite coating by laser remelting) under laser remelting/electrochemical deposition interaction treatment
Fig. 10. Acoustic emission spectra of deposited layer and composite remelting layer under different laser remelting/electrochemical deposition interaction treatment times
Fig. 11. SEM morphologies of scratches of deposited layer under laser remelting/electrochemical deposition interaction treatment. (a) Electrodeposition 10 min after laser melting pretreatment; (b) electrodeposition 10 min after the first laser remelting treatment; (c) electrodeposition 10 min after the second laser remelting treatment
Fig. 12. SEM morphologies of scratch of composite remelting layer obtained by laser remelting/electrochemical deposition interaction treatment. (a) The first laser remelting treatment after electrodeposition 10 min; (b) the second laser remelting treatment after electrodeposition 20 min; (c) the third laser remelting treatment after electrodeposition 30 min
Fig. 13. Oxidative weight gain of interaction-deposited samples and conventional electrodeposition samples at 600 ℃
Fig. 14. Electrical resistivity of coating samples under laser remelting/electrochemical deposition interaction treatment and conventional electrodeposition process
Fig. 15. Timing potential curves of copper electrodeposition process under laser remelting/electrochemical deposition interaction treatment
Fig. 16. Schematic of laser remelting/electrochemical deposition interaction treatment
Process | Light spot diameter /µm | Power/W | Scan speed/(mm·s-1) | Line spacing/mm |
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Laser melting treatment | 200 | 500 | 300 | 0.05 | Laser remelting | 200 | 500 | 300 | 0.04 |
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Table 1. Process parameters of laser melting treatment and laser remelting
Ingredient | Content |
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Volume of deionized water /mL | 200 | Mass of CuSO4 /g | 45 | Volume of H2SO4 /mL | 13 |
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Table 2. Composition and content of electrodeposition solution
Sample | Critical load /N |
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10 | 44.80 | 10-L-10 | 47.15 | 10-L-10-L-10 | 49.35 | 10-L | 49.60 | 10-L-10-L | 49.80 | 10-L-10-L-10-L | 49.95 |
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Table 3. Critical load of deposited layer and composite remelting layer under different laser remelting/ electrochemical deposition interaction treatment times