• Chinese Journal of Lasers
  • Vol. 50, Issue 24, 2402305 (2023)
Xueping Ding1、*, Qi Zhang2, and Honglin Ma2
Author Affiliations
  • 1School of Material Science and Engineering, Chongqing University of Technology, Chongqing 400054, China
  • 2Chongqing Key Laboratory of Additive Manufacturing Technology and Systems, Chongqing Institute of Green and Intelligent Technology, Chinese Academy of Sciences, Chongqing 400714, China
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    DOI: 10.3788/CJL230634 Cite this Article Set citation alerts
    Xueping Ding, Qi Zhang, Honglin Ma. Effect of Solution‑Aging Treatment on Corrosion Resistance of Ti6Al4V via Laser Wire Vacuum Additive Manufacturing[J]. Chinese Journal of Lasers, 2023, 50(24): 2402305 Copy Citation Text show less
    Experimental equipment for laser wire vacuum additive manufacturing. (a) Overall equipment; (b) equipment in vacuum chamber; (c) wire feeding system; (d) laser and wire arrangement
    Fig. 1. Experimental equipment for laser wire vacuum additive manufacturing. (a) Overall equipment; (b) equipment in vacuum chamber; (c) wire feeding system; (d) laser and wire arrangement
    Additive manufacturing of thin-wall part. (a) Figure of liquid bridge transfer; (b) sample
    Fig. 2. Additive manufacturing of thin-wall part. (a) Figure of liquid bridge transfer; (b) sample
    Polarization curves of different samples in NaCl solution with mass fraction of 3.5%
    Fig. 3. Polarization curves of different samples in NaCl solution with mass fraction of 3.5%
    EIS measurement results. (a) Nyquist plots; (b)(c) Bode plots; (d) equivalent circuit model
    Fig. 4. EIS measurement results. (a) Nyquist plots; (b)(c) Bode plots; (d) equivalent circuit model
    XPS full spectra of passive films formed on different sample surfaces
    Fig. 5. XPS full spectra of passive films formed on different sample surfaces
    High-resolution XPS spectra of passive films formed on different sample surfaces. (a)(d)(g) Ti 2p; (b)(e)(h) O 1s; (c)(f)(i) Al 2p
    Fig. 6. High-resolution XPS spectra of passive films formed on different sample surfaces. (a)(d)(g) Ti 2p; (b)(e)(h) O 1s; (c)(f)(i) Al 2p
    Valence distributions of Ti elements in passive films formed on different sample surfaces
    Fig. 7. Valence distributions of Ti elements in passive films formed on different sample surfaces
    IPFs of different samples. (a) AM; (b) SAT500; (c) SAT600
    Fig. 8. IPFs of different samples. (a) AM; (b) SAT500; (c) SAT600
    Phase distributions in different samples
    Fig. 9. Phase distributions in different samples
    Grain size distributions in different samples. (a) AM; (b) SAT500; (c) SAT600
    Fig. 10. Grain size distributions in different samples. (a) AM; (b) SAT500; (c) SAT600
    KAM maps of different samples. (a) AM; (b) SAT500; (c) SAT600
    Fig. 11. KAM maps of different samples. (a) AM; (b) SAT500; (c) SAT600
    Grain boundary distributions and statistics results in different samples. (a)(d) AM; (b)(e) SAT500; (c)(f) SAT600
    Fig. 12. Grain boundary distributions and statistics results in different samples. (a)(d) AM; (b)(e) SAT500; (c)(f) SAT600
    SampleTemperature /°CTime /hCooling method
    SAT5009501Air cooling
    5004Air cooling
    SAT6009501Air cooling
    6004Air cooling
    Table 1. Process parameters of solution aging heat treatment
    SampleEcorr /Vicorr /(μA/cm2
    AM-0.2132.595
    SAT500-0.1750.035
    SAT600-0.2380.351
    Table 2. Corrosion potential and corrosion current density values of different samples
    Sample

    Rs /

    (Ω·cm2

    CPE1 /

    S·sn1/cm2

    n1

    Rf /

    (104 Ω·cm2

    CPE2 /

    S·sn2/cm2

    n2

    Rct /

    (Ω·cm2

    χ2
    AM181.62.999×10-50.48342.3419.797×10-70.6234758.3003.024×10-3
    SAT500172.43.323×10-50.80934.081.223×10-40.83031.461×1053.046×10-4
    SAT60091.021.357×10-40.68673.9753.042×10-50.91999.3287.323×10-4
    Table 3. EIS parameters of equivalent circuit for test samples
    PeakBinding energy /eVChemical state
    AMSAT500SAT600
    Ti 2p453.94454.07Ti
    456.8456.90456.90Ti2O3
    458.46458.43458.80TiO2
    459.94460.07Ti
    462.5462.60462.60Ti2O3
    464.16464.13464.50TiO2
    O 1s530.73530.61530.71Metal oxides
    532.39531.52531.74OH-
    Al 2p74.674.6374.6Al2O3
    Table 4. Results of peak fitting of high-resolution XPS spectra
    Xueping Ding, Qi Zhang, Honglin Ma. Effect of Solution‑Aging Treatment on Corrosion Resistance of Ti6Al4V via Laser Wire Vacuum Additive Manufacturing[J]. Chinese Journal of Lasers, 2023, 50(24): 2402305
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