Author Affiliations
1Institute of Laser Advanced Manufacturing, Zhejiang University of Technology, Hangzhou 310023, Zhejiang, China2School of Mechanical Engineering, Zhejiang University of Technology, Hangzhou 310023, Zhejiang, China3Collaborative Innovation Center of High-End Laser Manufacturing Equipment (National 2011 Plan ), Zhejiang University of Technology, Hangzhou 310023, Zhejiang, China4Department of Mechanical and Aerospace Engineering, Carleton University, Ottawa KIS 5B6, Canadashow less
Fig. 1. Surface and cross-section morphologies of as-sprayed thermal barrier coatings. (a) Surface morphology; (b) surface morphology at high magnification; (c) cross-section morphology; (d) cross-section morphology of 8YSZ ceramic coating at high magnification
Fig. 2. Surface and cross-section morphologies of laser-alloyed thermal barrier coatings. (a) Surface morphology; (b) surface morphology at high magnification; (c) cross-section morphology; (d) cross-section morphology at high magnification
Fig. 3. XRD patterns of 8YSZ powder, as-sprayed thermal barrier coating and laser-alloyed thermal barrier coatings. (a) 8YSZ powder; (b) as-sprayed thermal barrier coating; (c) laser-alloyed thermal barrier coating
Fig. 4. Surface morphology and its high magnification of as-sprayed thermal barrier coatings after 4 h hot corrosion at 900 ℃. (a) 500×; (b) 10000×
Fig. 5. XRD patterns of as-sprayed and laser-alloyed thermal barrier coatings after molten salt corrosion. (a) As-sprayed thermal barrier coating; (b) laser-alloyed thermal barrier coating
Fig. 6. Surface morphology and its high magnification of laser-alloyed thermal barrier coating after 4 h hot corrosion at 900 ℃. (a) 500×; (b) 5000×
Fig. 7. Cross-section morphology and EDS element analysis of as-sprayed thermal barrier coating after 4 h hot corrosion. (a) Cross-section morphology; (b) EDS elemental analysis
Fig. 8. Cross-section morphology and EDS element analysis of laser-alloyed thermal barrier coating after 4 h hot corrosion. (a) Cross-section morphology; (b) EDS elemental analysis
Fig. 9. Schematics of hot corrosion failure of as-sprayed and laser-alloyed thermal barrier coatings. (a) As-sprayed thermal barrier coating before hot corrosion test; (b) as-sprayed thermal barrier coating after hot corrosion test; (c) laser-alloyed thermal barrier coating before hot corrosion test; (d) self-healing process of laser-alloyed thermal barrier coating; (e) laser-alloyed thermal barrier coating after hot corrosion test
Element | Mass fraction /% |
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Ni | 50-55 | Cr | 17-21 | Mo | 2.8-3.3 | Nb | 4.75-5.5 | Al | 1 | Co | 0.08 | C | 0.35 | Mn | 0.35 | Si | 0.015 | S | 0.3 | Cu | 0.2-0.8 | Ti | 0.65-1.15 | Fe | Margin |
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Table 1. Chemical composition of nickel-based superalloy Inconel 718
Layer | Spraying current /A | Argon flow / (L·min-1) | Hydrogen flow / (L·min-1) | Powder feed rate /(g·min-1) | Spraying distance /mm |
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Bonding layer | 550-570 | 45 | 3 | 15 | 120 | Ceramic layer | 690-710 | 45 | 1 | 10 | 90 |
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Table 2. Process parameters of atmospheric plasma spraying
Area in Fig. 4(b) | Atomic fraction /% |
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Zr | O | Y | S | Na |
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A | 30.0 | 62.3 | 2.6 | 1.8 | 3.2 | B | 18.8 | 63.0 | 1.7 | 4.7 | 11.8 | C | 6.4 | 53.5 | 23.6 | 16.5 | - |
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Table 3. Chemical composition of different areas in as-sprayed thermal barrier coating after hot corrosion