• Chinese Journal of Lasers
  • Vol. 51, Issue 10, 1002321 (2024)
Enhao Feng1, Rong Chen2、3, Shixiong Di4, Zhanwei Zhou5, Xiaogang Yin1, Nan Kang6、*, and Xin Lin2、3
Author Affiliations
  • 1Xi an High Voltage Apparatus Research Institute Co., Ltd., Xi an 710077, Shaanxi , China
  • 2State Key Laboratory of Solidification Processing, Xi an 710072, Shaanxi , China
  • 3Key Laboratory of Metal High Performance Additive Manufacturing and Innovative Design, MIIT, Xi an 710072, Shaanxi , China
  • 4AECC Hunan Aviation Powerplant Research Institute, Zhuzhou 412002, Hunan , China
  • 5Beijing Satellite Manufacturing Co., Ltd., Beijing 100094, China
  • 6MSMP Laboratory, Arts et Métiers Institute of Technology, Paris 51000, France
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    DOI: 10.3788/CJL231575 Cite this Article Set citation alerts
    Enhao Feng, Rong Chen, Shixiong Di, Zhanwei Zhou, Xiaogang Yin, Nan Kang, Xin Lin. Effect of Heat Treatment on Microstructure and Mechanical Properties of TC4 Alloy by Selective Laser Melting[J]. Chinese Journal of Lasers, 2024, 51(10): 1002321 Copy Citation Text show less
    Morphology of TC4 titanium alloy powder
    Fig. 1. Morphology of TC4 titanium alloy powder
    OM images of SLM TC4 titanium alloy. (a) As-deposited state; (b) annealed state; (c) solution state; (d) solution and aging state
    Fig. 2. OM images of SLM TC4 titanium alloy. (a) As-deposited state; (b) annealed state; (c) solution state; (d) solution and aging state
    Metallographic photographs of SLM TC4 titanium alloy sample at different magnifications. (a) 100 times (parallel to deposition direction); (b) 500 times (parallel to deposition direction); (c) 100 times (perpendicular to deposition direction); (d) 500 times (perpendicular to deposition direction)
    Fig. 3. Metallographic photographs of SLM TC4 titanium alloy sample at different magnifications. (a) 100 times (parallel to deposition direction); (b) 500 times (parallel to deposition direction); (c) 100 times (perpendicular to deposition direction); (d) 500 times (perpendicular to deposition direction)
    OM tissue photos of SLM TC4 titanium alloy sample at different magnifications. (a) 100 times (annealed state); (b) 500 times (annealed state); (c) 100 times (solution state); (d) 500 times (solution state); (e) 100 times (solid solution and aging state); (f) 500 times (solid solution and aging state)
    Fig. 4. OM tissue photos of SLM TC4 titanium alloy sample at different magnifications. (a) 100 times (annealed state); (b) 500 times (annealed state); (c) 100 times (solution state); (d) 500 times (solution state); (e) 100 times (solid solution and aging state); (f) 500 times (solid solution and aging state)
    SEM photos of SLM TC4 titanium alloy sample at different magnifications. (a) 1000 times (as-deposited state); (b) 30000 times (as-deposited state); (c) 1000 times (annealed state); (d) 30000 times (annealed state); (e) 1000 times (solution state); (f) 30000 times (solution state); (g) 1000 times (solid solution and aging state); (h) 30000 times (solid solution and aging state)
    Fig. 5. SEM photos of SLM TC4 titanium alloy sample at different magnifications. (a) 1000 times (as-deposited state); (b) 30000 times (as-deposited state); (c) 1000 times (annealed state); (d) 30000 times (annealed state); (e) 1000 times (solution state); (f) 30000 times (solution state); (g) 1000 times (solid solution and aging state); (h) 30000 times (solid solution and aging state)
    Phase content distribution of SLM TC4 titanium alloy in different states. (a) Deposition state; (b) annealed state; (c) solid solution state; (d) solid solution and aging state; (e) α and β phases content comparison histogram
    Fig. 6. Phase content distribution of SLM TC4 titanium alloy in different states. (a) Deposition state; (b) annealed state; (c) solid solution state; (d) solid solution and aging state; (e) α and β phases content comparison histogram
    EBSD grain orientation diagrams of SLM TC4 titanium alloy in different states. (a) Deposition state; (b) annealed state; (c) solid solution state; (d) solid solution and aging state; (e) α and β phases orientation reference map
    Fig. 7. EBSD grain orientation diagrams of SLM TC4 titanium alloy in different states. (a) Deposition state; (b) annealed state; (c) solid solution state; (d) solid solution and aging state; (e) α and β phases orientation reference map
    KAM diagrams of SLM TC4 titanium alloy samples in different states. (a) Deposition state; (b) annealed state; (c) solid solution state; (d) solid solution and aging state
    Fig. 8. KAM diagrams of SLM TC4 titanium alloy samples in different states. (a) Deposition state; (b) annealed state; (c) solid solution state; (d) solid solution and aging state
    Tensile stress-strain curves of TC4 titanium alloy in different states. (a) Deposition state; (b) annealed state; (c) solid solution state; (d) solid solution and aging state
    Fig. 9. Tensile stress-strain curves of TC4 titanium alloy in different states. (a) Deposition state; (b) annealed state; (c) solid solution state; (d) solid solution and aging state
    Comparison of yield strength and tensile strength of TC4 titanium alloy in different states
    Fig. 10. Comparison of yield strength and tensile strength of TC4 titanium alloy in different states
    Comparison of plastic properties of TC4 titanium alloy in different states
    Fig. 11. Comparison of plastic properties of TC4 titanium alloy in different states
    Fracture morphologies of SLM TC4 titanium alloy tensile sample under different states. (a) 500 times (as deposited state); (b) 5000 times (as deposited state); (c) 500 times (annealed state); (d) 5000 times (annealed state); (e) 500 times (solid solution state); (f) 5000 times (solid solution state); (g) 500 times (solid solution and aging state); (h) 5000 times (solid solution and aging state)
    Fig. 12. Fracture morphologies of SLM TC4 titanium alloy tensile sample under different states. (a) 500 times (as deposited state); (b) 5000 times (as deposited state); (c) 500 times (annealed state); (d) 5000 times (annealed state); (e) 500 times (solid solution state); (f) 5000 times (solid solution state); (g) 500 times (solid solution and aging state); (h) 5000 times (solid solution and aging state)
    ElementAlVFeCNHOTi
    Mass fraction /%6.303.500.200.050.020.010.10Bal.
    Table 1. Composition of TC4 titanium alloy powder
    Sample stateElastic modulus /GPa

    Yield

    strength /MPa

    Tensile

    strength /MPa

    Elongation /%Section shrinkage /%
    As deposited111.751080.01238.758.8530.80
    Annealed118.18881.8990.0014.3452.04
    Solid solution116.97799.4928.4015.6254.06
    Solid solution and aging115.55829.6954.0015.9852.06
    Table 2. Mechanical properties of SLM TC4 titanium alloy in different states
    Enhao Feng, Rong Chen, Shixiong Di, Zhanwei Zhou, Xiaogang Yin, Nan Kang, Xin Lin. Effect of Heat Treatment on Microstructure and Mechanical Properties of TC4 Alloy by Selective Laser Melting[J]. Chinese Journal of Lasers, 2024, 51(10): 1002321
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