• Chinese Journal of Lasers
  • Vol. 49, Issue 12, 1210002 (2022)
Dan Liu1、2, Cong Zhao1、2, Peng Ji1、2, Zhihao Cai1、2, Bozhe Li1、2, Mengqiang Zou1、2, and Changrui Liao1、2、*
Author Affiliations
  • 1Key Laboratory of Optoelectronic Devices and Systems of Ministry of Education/Guangdong Province, College of Physics and Optoelectronic Engineering, Shenzhen University, Shenzhen 518060, Guangdong, China
  • 2Shenzhen Key Laboratory of Photonic Devices and Sensing Systems for Internet of Things, Guangdong and Hong Kong Joint Research Centre for Optical Fibre Sensors, Shenzhen University, Shenzhen 518060, Guangdong, China
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    DOI: 10.3788/CJL202249.1210002 Cite this Article Set citation alerts
    Dan Liu, Cong Zhao, Peng Ji, Zhihao Cai, Bozhe Li, Mengqiang Zou, Changrui Liao. Acetone Gas Sensor Based on Two-Photon Polymerized Micropillar on End Face of Fiber[J]. Chinese Journal of Lasers, 2022, 49(12): 1210002 Copy Citation Text show less
    Principle diagram of acetone gas sensing based on fiber-tip micropillar
    Fig. 1. Principle diagram of acetone gas sensing based on fiber-tip micropillar
    Flow chart of device fabrication. (a) Photoresist solution dropped on end face of single-mode fiber, covered with coverslip; (b) two-photon polymerization for micropillar structure on end face of fiber; (c) coverslip on top of optical fiber removed and uncured photoresist washed away with mixed solution of isopropyl alcohol and acetone; (d) micropillar fabricated on end face of optical fiber
    Fig. 2. Flow chart of device fabrication. (a) Photoresist solution dropped on end face of single-mode fiber, covered with coverslip; (b) two-photon polymerization for micropillar structure on end face of fiber; (c) coverslip on top of optical fiber removed and uncured photoresist washed away with mixed solution of isopropyl alcohol and acetone; (d) micropillar fabricated on end face of optical fiber
    SEM micrograph of polymerized micropillar fabricated on end face of optical fiber by two-photon polymerization. (a) Front view; (b) vertical view; (c) side view
    Fig. 3. SEM micrograph of polymerized micropillar fabricated on end face of optical fiber by two-photon polymerization. (a) Front view; (b) vertical view; (c) side view
    Reflection spectra of polymerized micropillars on end face of optical fiber with different design heights. (a) H1=20 μm; (b) H2=30 μm; (c) H3=40 μm
    Fig. 4. Reflection spectra of polymerized micropillars on end face of optical fiber with different design heights. (a) H1=20 μm; (b) H2=30 μm; (c) H3=40 μm
    Acetone gas sensitivity test. (a) Reflection spectra at different acetone concentrations ; (b) relationship between dip wavelength and acetone concentration
    Fig. 5. Acetone gas sensitivity test. (a) Reflection spectra at different acetone concentrations ; (b) relationship between dip wavelength and acetone concentration
    Variation of dip wavelength in interference spectrum of polymerized micropillar when acetone concentration first decreases and then increases for three times in range of 1×10-9 to 1×10-3
    Fig. 6. Variation of dip wavelength in interference spectrum of polymerized micropillar when acetone concentration first decreases and then increases for three times in range of 1×10-9 to 1×10-3
    Temperature response of sensor; (a) Interference spectral response of polymerized micropillar sensor at different temperatures; (b) relationship between dip wavelength in interference spectrum and ambient temperature
    Fig. 7. Temperature response of sensor; (a) Interference spectral response of polymerized micropillar sensor at different temperatures; (b) relationship between dip wavelength in interference spectrum and ambient temperature
    Dan Liu, Cong Zhao, Peng Ji, Zhihao Cai, Bozhe Li, Mengqiang Zou, Changrui Liao. Acetone Gas Sensor Based on Two-Photon Polymerized Micropillar on End Face of Fiber[J]. Chinese Journal of Lasers, 2022, 49(12): 1210002
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